[go: up one dir, main page]

WO2011067386A3 - Method for producing aliphatic aldehydes - Google Patents

Method for producing aliphatic aldehydes Download PDF

Info

Publication number
WO2011067386A3
WO2011067386A3 PCT/EP2010/068865 EP2010068865W WO2011067386A3 WO 2011067386 A3 WO2011067386 A3 WO 2011067386A3 EP 2010068865 W EP2010068865 W EP 2010068865W WO 2011067386 A3 WO2011067386 A3 WO 2011067386A3
Authority
WO
WIPO (PCT)
Prior art keywords
general formula
iii
aliphatic aldehydes
producing aliphatic
hydrogen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2010/068865
Other languages
German (de)
French (fr)
Other versions
WO2011067386A2 (en
Inventor
Jörg Botzem
Andreas Lanver
Klaus Ebel
Karl Beck
Ulrich Griesbach
Ralf Pelzer
Achim Sorg
Nadja Pollmer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of WO2011067386A2 publication Critical patent/WO2011067386A2/en
Publication of WO2011067386A3 publication Critical patent/WO2011067386A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/62—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by hydrogenation of carbon-to-carbon double or triple bonds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/68—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C07C45/72—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups
    • C07C45/74—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups combined with dehydration
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0007—Aliphatic compounds
    • C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

The invention relates to a method for producing aliphatic aldehydes of the general formula (I) by reacting aldehyde of the general formula (II) with an aldehyde of the general formula (III), where R1 is hydrogen or a methyl group, R2 is a straight-chain or branched alkyl radical having 1 to 4 carbon atoms, and the two X are each hydrogen or together are a further C-C bond, in the presence of an aldol condensation catalyst to form the substituted octenal of the general formula (I) and subsequently optionally hydration, either continuously or in batches, to form the corresponding octanal of the formula (I). The invention is characterized in that the aldehydes of the general formula III and II are used in a molar ratio of III:II between 1.4:1 and 0.6:1.
PCT/EP2010/068865 2009-12-04 2010-12-03 Method for producing aliphatic aldehydes Ceased WO2011067386A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP09178052 2009-12-04
EP09178052.8 2009-12-04

Publications (2)

Publication Number Publication Date
WO2011067386A2 WO2011067386A2 (en) 2011-06-09
WO2011067386A3 true WO2011067386A3 (en) 2011-10-13

Family

ID=43911613

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2010/068865 Ceased WO2011067386A2 (en) 2009-12-04 2010-12-03 Method for producing aliphatic aldehydes

Country Status (1)

Country Link
WO (1) WO2011067386A2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8889920B2 (en) 2010-02-12 2014-11-18 Basf Se Process for preparing 4-isopropylcyclohexylmethanol

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8367875B2 (en) 2010-02-11 2013-02-05 Basf Se Process for the preparation of m-substituted alkyltoluenes by isomerization with ionic liquids as catalysts
US8609903B2 (en) 2010-04-01 2013-12-17 Basf Se Process for preparing hydroxy-substituted aromatic aldehydes
US9556108B2 (en) 2014-07-10 2017-01-31 Mallinckrodt Llc Process for preparing substituted phenylalkanes
US20210122693A1 (en) * 2018-05-11 2021-04-29 Takasago International Corporation Dienal compound and flavor composition

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0252378A1 (en) * 1986-07-05 1988-01-13 BASF Aktiengesellschaft Aliphatic aldehydes, method for their production and their application as perfume agents

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19611976A1 (en) 1996-03-26 1997-10-02 Basf Ag Process and reactor for carrying out material conversions with catalysts suspended in liquids
DE10231944A1 (en) 2002-07-15 2004-01-29 Basf Ag Process for the continuous hydrogenation of citral to citronellal

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0252378A1 (en) * 1986-07-05 1988-01-13 BASF Aktiengesellschaft Aliphatic aldehydes, method for their production and their application as perfume agents

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8889920B2 (en) 2010-02-12 2014-11-18 Basf Se Process for preparing 4-isopropylcyclohexylmethanol

Also Published As

Publication number Publication date
WO2011067386A2 (en) 2011-06-09

Similar Documents

Publication Publication Date Title
WO2011067386A3 (en) Method for producing aliphatic aldehydes
MXPA04004241A (en) Method for production of formic acid formates.
UA89674C2 (en) Process for the preparation of product comprising a lower alkyl ester of a lower carboxylic acid
RU2010126906A (en) METHOD FOR PRODUCING INDOLINO DERIVATIVE
SG159475A1 (en) Conjugated diene polymer and conjugated diene polymer composition
EP2682382A3 (en) Method for Producing Phenylacetamide Compound
MY139630A (en) Acrylic acid preparation method
ZA200806683B (en) Acrolein preparation method
IN2014CN04702A (en)
WO2007091697A3 (en) Method for preparing prostaglandin derivative
WO2009063856A1 (en) Method for producing cellulose ether derivative
UA101712C2 (en) Normal;heading 1;heading 2;heading 3;PROCESS FOR MANUFACTURING SUBSTITUTED 5-METHOXYMETHYLPYRIDINE-2,3-DICARBOXYLIC ACID DERIVATIVES
WO2009101947A3 (en) Process for producing carbon material
WO2009066735A1 (en) Method for producing 2-azaadamantane
TW200609210A (en) Preparation of acrylic acid by heterogeneously catalyzed gas phase partial oxidation of at least one c3 hydrocarbon precursor compound
NZ605608A (en) Method of synthesis of ferroquine by convergent reductive amination
WO2009054356A1 (en) PROCESS FOR PRODUCTION OF CYANOHYDRIN COMPOUND, AND PROCESS FOR PRODUCTION OF α-HYDROXYESTER COMPOUND
NZ577081A (en) Synthesis of compounds useful as modulators of amyloid-beta production
SG178864A1 (en) Method for producing a compound with a double bond
TW200710076A (en) Process for producing aldehyde with 2-position branched long-chain alkyl
TW200730535A (en) Method for producing ketimine structure-containing alkoxysilane
WO2008092583A3 (en) Method for producing dihalo acetoacetic alkyl esters
WO2009001819A1 (en) Method for producing fluoroamide and method for producing fluoronitrile
MY143948A (en) Process for producing a naphtahlenesulfonate formaldehyde condensate
WO2009147541A3 (en) Method of preparing glycerol alkyl ethers

Legal Events

Date Code Title Description
121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 10785430

Country of ref document: EP

Kind code of ref document: A1

NENP Non-entry into the national phase

Ref country code: DE

122 Ep: pct application non-entry in european phase

Ref document number: 10785430

Country of ref document: EP

Kind code of ref document: A2