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WO2010111995A3 - Method for the hydrolysis of cellulose raw materials - Google Patents

Method for the hydrolysis of cellulose raw materials Download PDF

Info

Publication number
WO2010111995A3
WO2010111995A3 PCT/DE2010/000320 DE2010000320W WO2010111995A3 WO 2010111995 A3 WO2010111995 A3 WO 2010111995A3 DE 2010000320 W DE2010000320 W DE 2010000320W WO 2010111995 A3 WO2010111995 A3 WO 2010111995A3
Authority
WO
WIPO (PCT)
Prior art keywords
hydrolysis
raw materials
cellulose raw
cellulose
depolymerization
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/DE2010/000320
Other languages
German (de)
French (fr)
Other versions
WO2010111995A2 (en
Inventor
Ferdi SCHÜTH
Roberto Rinaldi
Philip Engel
Antje Spiess
Jochen Büchs
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Studiengesellschaft Kohle gGmbH
Rheinisch Westlische Technische Hochschuke RWTH
Original Assignee
Studiengesellschaft Kohle gGmbH
Rheinisch Westlische Technische Hochschuke RWTH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Studiengesellschaft Kohle gGmbH, Rheinisch Westlische Technische Hochschuke RWTH filed Critical Studiengesellschaft Kohle gGmbH
Publication of WO2010111995A2 publication Critical patent/WO2010111995A2/en
Publication of WO2010111995A3 publication Critical patent/WO2010111995A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00—Preparation of compounds containing saccharide radicals
    • C12P19/02—Monosaccharides
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B1/00—Preparatory treatment of cellulose for making derivatives thereof, e.g. pre-treatment, pre-soaking, activation
    • C08B1/003—Preparation of cellulose solutions, i.e. dopes, with different possible solvents, e.g. ionic liquids
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P19/00—Preparation of compounds containing saccharide radicals
    • C12P19/14—Preparation of compounds containing saccharide radicals produced by the action of a carbohydrase (EC 3.2.x), e.g. by alpha-amylase, e.g. by cellulase, hemicellulase
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13K—SACCHARIDES OBTAINED FROM NATURAL SOURCES OR BY HYDROLYSIS OF NATURALLY OCCURRING DISACCHARIDES, OLIGOSACCHARIDES OR POLYSACCHARIDES
    • C13K1/00—Glucose; Glucose-containing syrups
    • C13K1/02—Glucose; Glucose-containing syrups obtained by saccharification of cellulosic materials
    • C—CHEMISTRY; METALLURGY
    • C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12P—FERMENTATION OR ENZYME-USING PROCESSES TO SYNTHESISE A DESIRED CHEMICAL COMPOUND OR COMPOSITION OR TO SEPARATE OPTICAL ISOMERS FROM A RACEMIC MIXTURE
    • C12P2201/00—Pretreatment of cellulosic or lignocellulosic material for subsequent enzymatic treatment or hydrolysis

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Microbiology (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • General Engineering & Computer Science (AREA)
  • Biotechnology (AREA)
  • Genetics & Genomics (AREA)
  • Materials Engineering (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Emergency Medicine (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)

Abstract

A method for the depolymerization of cellulose is claimed, wherein a solution made of cellulose is brought in contact with a solid acid catalyst in an ionic fluid and in a subsequent step, the depolymerized cellulose obtained in this way is subjected to enzymatic hydrolysis.
PCT/DE2010/000320 2009-04-02 2010-03-23 Method for the hydrolysis of cellulose raw materials Ceased WO2010111995A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE200910016001 DE102009016001A1 (en) 2009-04-02 2009-04-02 Process for the hydrolysis of cellulose raw materials
DE102009016001.9 2009-04-02

Publications (2)

Publication Number Publication Date
WO2010111995A2 WO2010111995A2 (en) 2010-10-07
WO2010111995A3 true WO2010111995A3 (en) 2011-03-03

Family

ID=42674990

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/DE2010/000320 Ceased WO2010111995A2 (en) 2009-04-02 2010-03-23 Method for the hydrolysis of cellulose raw materials

Country Status (2)

Country Link
DE (1) DE102009016001A1 (en)
WO (1) WO2010111995A2 (en)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103232396B (en) * 2013-04-17 2015-03-04 北京工业大学 Three selective ionic liquids and synthesizing method thereof
JP2016524899A (en) * 2013-07-01 2016-08-22 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ Endoglucanase-induced production of cellulose oligomers
BR112017022096A2 (en) * 2015-04-13 2018-07-03 Basf Corp ? methods for saccharide release and biosynthetic preparation of a product, biosynthetic reaction mixture and pozzolanic material?
CN105949482B (en) * 2016-05-23 2018-01-12 齐鲁工业大学 A kind of method for improving the methylimidazole villaumite of 1 pi-allyl 3 dissolving cellulosic energy
CN105801884B (en) * 2016-05-23 2018-01-12 齐鲁工业大学 A kind of method for improving the methylimidazole villaumite of 1 butyl 3 dissolving cellulosic energy

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090011473A1 (en) * 2007-02-23 2009-01-08 The University Of Toledo Saccharifying cellulose
WO2009115075A1 (en) * 2008-03-18 2009-09-24 Studiengesellschaft Kohle Mbh Method for the depolymerization of cellulose

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US943176A (en) 1908-08-08 1909-12-14 Joseph Henry Burdock Light-extinguisher.
US1943176A (en) 1930-09-27 1934-01-09 Chem Ind Basel Cellulose solution
US6824599B2 (en) 2001-10-03 2004-11-30 The University Of Alabama Dissolution and processing of cellulose using ionic liquids
DE102005017715A1 (en) 2005-04-15 2006-10-19 Basf Ag Solution, useful for physical or chemical treatment of cellulose, comprises cellulose and an ionic liquid containing anions and cations as solvent, where the cation exhibits nitrogen, oxygen, sulfur and phosphorus atoms in protonated form
AU2008208869B2 (en) 2007-01-23 2014-02-13 Basf Se Method for producing glucose by enzymatic hydrolysis of cellulose that can be pretreated with an ionic liquid containing a polyatomic anion
WO2008090156A1 (en) 2007-01-23 2008-07-31 Basf Se Method for producing glucose by enzymatic hydrolysis of cellulose that is obtained from material containing ligno-cellulose using an ionic liquid that comprises a polyatomic anion
KR100887563B1 (en) * 2007-07-06 2009-03-09 한국과학기술연구원 Hydrolysis Method of Cellulose by Solid Acid Catalyst

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20090011473A1 (en) * 2007-02-23 2009-01-08 The University Of Toledo Saccharifying cellulose
WO2009115075A1 (en) * 2008-03-18 2009-09-24 Studiengesellschaft Kohle Mbh Method for the depolymerization of cellulose

Non-Patent Citations (4)

* Cited by examiner, † Cited by third party
Title
CHANGZHI LI ET AL: "Efficient Acid-Catalyzed Hydrolysis of Cellulose in Ionic Liquid", ADVANCED SYNTHESIS & CATALYSIS, WILEY VCH VERLAG, WEINHEIM, DE, vol. 349, 1 January 2007 (2007-01-01), pages 1847 - 1850, XP002534172, ISSN: 1615-4150, DOI: DOI:10.1002/ADSC.200700259 *
DADI A P ET AL: "Mitigation of cellulose recalcitrance to enzymatic hydrolysis by ionic liquid pretreatment", APPLIED BIOCHEMISTRY AND BIOTECHNOLOGY, THE HUMANA PRESS, INC, US, vol. 137, 1 January 2007 (2007-01-01), pages 407 - 421, XP008089078, ISSN: 0273-2289, DOI: DOI:10.1007/S12010-007-9068-9 *
ROBERTO RINALDI ET AL: "Depolymerization of Cellulose Using Solid Catalysts in Ionic Liquids", ANGEWANDTE CHEMIE. INTERNATIONAL EDITION, WILEY VCH VERLAG, WEINHEIM, vol. 47, no. 42, 12 September 2008 (2008-09-12), pages 8047 - 8050, XP009106605, ISSN: 1433-7851, DOI: DOI:10.1002/ANIE.200802879 *
ZHAO H ET AL: "Regenerating cellulose from ionic liquids for an accelerated enzymatic hydrolysis", JOURNAL OF BIOTECHNOLOGY, ELSEVIER SCIENCE PUBLISHERS, AMSTERDAM, NL, vol. 139, no. 1, 1 January 2009 (2009-01-01), pages 47 - 54, XP025796272, ISSN: 0168-1656, [retrieved on 20080905], DOI: DOI:10.1016/J.JBIOTEC.2008.08.009 *

Also Published As

Publication number Publication date
WO2010111995A2 (en) 2010-10-07
DE102009016001A1 (en) 2010-10-07

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