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WO2010001025A3 - Process for the purification of 2,3,3,3-tetrafluoro-1-propene (hfo-1234yf) - Google Patents

Process for the purification of 2,3,3,3-tetrafluoro-1-propene (hfo-1234yf) Download PDF

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Publication number
WO2010001025A3
WO2010001025A3 PCT/FR2009/051074 FR2009051074W WO2010001025A3 WO 2010001025 A3 WO2010001025 A3 WO 2010001025A3 FR 2009051074 W FR2009051074 W FR 2009051074W WO 2010001025 A3 WO2010001025 A3 WO 2010001025A3
Authority
WO
WIPO (PCT)
Prior art keywords
tetrafluoro
propene
purification
hfo
molecular sieves
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/FR2009/051074
Other languages
French (fr)
Other versions
WO2010001025A2 (en
Inventor
Michel Devic
Anne Pigamo
Laurent Wendlinger
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Original Assignee
Arkema France SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Arkema France SA filed Critical Arkema France SA
Priority to ES09772707.7T priority Critical patent/ES2473468T3/en
Priority to CN200980124282.3A priority patent/CN102076645B/en
Priority to EP09772707.7A priority patent/EP2303819B1/en
Priority to US13/001,663 priority patent/US8252964B2/en
Publication of WO2010001025A2 publication Critical patent/WO2010001025A2/en
Publication of WO2010001025A3 publication Critical patent/WO2010001025A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/38—Separation; Purification; Stabilisation; Use of additives
    • C07C17/389—Separation; Purification; Stabilisation; Use of additives by adsorption on solids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)

Abstract

The subject of the invention is a process for the purification of 2,3,3,3-tetrafluoro-1-propene (HFO-1234yf). More particularly, it relates to a purification process in which 2,3,3,3-tetrafluoro-1-propene, comprising impurities based on halogen compounds, is brought into contact with an adsorbent, preferably molecular sieves and advantageously molecular sieves having a pore opening with an average diameter between 5 and 11 Å, preferably between 5 and 9 Å.
PCT/FR2009/051074 2008-07-03 2009-06-08 Process for the purification of 2,3,3,3-tetrafluoro-1-propene (hfo-1234yf) Ceased WO2010001025A2 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
ES09772707.7T ES2473468T3 (en) 2008-07-03 2009-06-08 Purification procedure of 2,3,3,3-tetrafluoro-1-propene (HFO1234yf)
CN200980124282.3A CN102076645B (en) 2008-07-03 2009-06-08 Method for purifying 2,3,3,3-tetrafluoro-1-propene (HFO-1234yf)
EP09772707.7A EP2303819B1 (en) 2008-07-03 2009-06-08 Process for the purification of 2,3,3,3-tetrafluoro-1-propene (hfo-1234yf)
US13/001,663 US8252964B2 (en) 2008-07-03 2009-06-08 Process for the purification of 2,3,3,3-tetrafluoro-1-propene (HFO-1234yf)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0854514A FR2933402B1 (en) 2008-07-03 2008-07-03 PROCESS FOR PURIFYING 2,3,3,3-TETRAFLUORO-1-PROPENE (HFO1234YF)
FR08.54514 2008-07-03

Publications (2)

Publication Number Publication Date
WO2010001025A2 WO2010001025A2 (en) 2010-01-07
WO2010001025A3 true WO2010001025A3 (en) 2010-03-11

Family

ID=40297685

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/FR2009/051074 Ceased WO2010001025A2 (en) 2008-07-03 2009-06-08 Process for the purification of 2,3,3,3-tetrafluoro-1-propene (hfo-1234yf)

Country Status (6)

Country Link
US (1) US8252964B2 (en)
EP (1) EP2303819B1 (en)
CN (1) CN102076645B (en)
ES (1) ES2473468T3 (en)
FR (1) FR2933402B1 (en)
WO (1) WO2010001025A2 (en)

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US9926244B2 (en) 2008-10-28 2018-03-27 Honeywell International Inc. Process for drying HCFO-1233zd
US9540296B2 (en) 2015-03-19 2017-01-10 Honeywell International Inc. Process for drying HCFO-1233zd
GB0918069D0 (en) * 2009-10-15 2009-12-02 Ineos Fluor Holdings Ltd Process
AU2013204796B2 (en) * 2009-10-15 2014-09-11 Mexichem Amanco Holding S.A. De C.V. Process for purifying (hydro) fluoroalkenes
WO2011077191A1 (en) * 2009-12-23 2011-06-30 Arkema France Catalytic gas phase fluorination of 1230xa to 1234yf
US9890096B2 (en) 2011-01-19 2018-02-13 Honeywell International Inc. Methods of making 2,3,3,3-tetrafluoro-2-propene
EP2671860B2 (en) * 2011-02-04 2024-05-29 AGC Inc. Method for purifying 2,3,3,3-tetrafluoropropene
US8337595B2 (en) * 2011-04-20 2012-12-25 Honeywell International Inc. Purification of trans-1,3,3,3-tetrafluoropropene
US8796493B2 (en) * 2011-09-30 2014-08-05 Honeywell International Inc. Methods to separate halogentated olefins from 2-chloro-1,1,1,2-tetrafluoropropane using a solid adsorbent
ES2791768T3 (en) * 2011-10-14 2020-11-05 Honeywell Int Inc Process to produce 2,3,3,3-tetrafluoropropene
WO2013184865A1 (en) * 2012-06-06 2013-12-12 E.I. Du Pont De Nemours And Company PROCESS FOR THE REDUCTION OF RfCCX IMPURITIES IN FLUOROOLEFINS
FR3000096B1 (en) * 2012-12-26 2015-02-20 Arkema France COMPOSITION COMPRISING 2,3,3,3-TETRAFLUOROPROPENE
JP2016519053A (en) 2013-03-13 2016-06-30 アーケマ・インコーポレイテッド Process for purifying and stabilizing hydrofluoroolefins and hydrochlorofluoroolefins
US20150259267A1 (en) 2014-03-14 2015-09-17 E.I. Du Pont De Nemours And Company PROCESS FOR THE REDUCTION OF RfC=CX IMPURITIES IN FLUOROOLEFINS
EP3412647B2 (en) * 2013-03-15 2024-02-14 The Chemours Company FC, LLC Process for the reduction of alkyne impurities in fluoroolefins
KR20250152674A (en) * 2013-03-15 2025-10-23 허니웰 인터내셔날 인코포레이티드 Methods for removing halogenated ethylene impurities in 2,3,3,3-tetrafluoropropene product
US10995047B2 (en) 2013-03-15 2021-05-04 The Chemours Company Fc, Llc Process for the reduction of RƒC≡CX impurities in fluoroolefins
CN106170476A (en) 2014-04-16 2016-11-30 默克专利有限公司 Materials for Electronic Devices
GB201410174D0 (en) * 2014-06-09 2014-07-23 Mexichem Amanco Holding Sa Process
EP3286160A4 (en) 2015-04-24 2019-01-16 Honeywell International Inc. PROCESS FOR REDUCING 1233xf CONCENTRATION IN 244bb
JP2018513786A (en) * 2015-04-24 2018-05-31 ハネウェル・インターナショナル・インコーポレーテッドＨｏｎｅｙｗｅｌｌ Ｉｎｔｅｒｎａｔｉｏｎａｌ Ｉｎｃ． Method for regenerating solid adsorbent
CN107635955A (en) 2015-05-21 2018-01-26 科慕埃弗西有限公司 Hydrofluorination of 1233xf to 244bb by SbF5
GB2540427B (en) 2015-07-17 2017-07-19 Mexichem Fluor Sa De Cv Process for the preparation of 2,3,3,3-tetrafluoropropene (1234yf)
RU2736125C2 (en) 2015-08-19 2020-11-11 Сполек Про Хемицкоу А Гутни Виробу, Акциова Сполецност Method of producing c3-chlorinated alkane or alkene compounds
FR3041632B1 (en) * 2015-09-24 2020-01-10 Arkema France PROCESS FOR PURIFYING AND DRYING A FLOW OF HYDROFLUOROOLEFINS
US10239804B2 (en) 2016-01-14 2019-03-26 Srf Limited Process for the preparation of 2,3,3,3-tetrafluoropropene from methyl chloride and chlorodifluoromethane
JP6989519B2 (en) 2016-04-13 2022-01-05 スポレク プロ ヘミコウ アー フツニ ブイロブ，アクツィオバ スポレチェノスト process
KR20220061994A (en) * 2019-09-12 2022-05-13 칸토 덴카 코교 가부시키가이샤 A method for purifying a fluoroolefin having a structure of =CF2 or =CHF, and a high-purity fluoroolefin and a method for producing the same
CN111517937B (en) * 2020-04-27 2022-12-09 中国船舶重工集团公司第七一八研究所 Purification method of hexachloroacetone

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US3215747A (en) * 1963-05-31 1965-11-02 Pennsalt Chemicals Corp Method of separating trifluoroethylene from tetrafluoroethylene
EP0511612A2 (en) * 1991-04-27 1992-11-04 Hoechst Aktiengesellschaft Method for the purification of chlorofluorohydrocarbons
WO2001083411A1 (en) * 2000-05-04 2001-11-08 Ineos Fluor Holdings Limited Removal of (hydro)haloalkene impurities from product streams
US7084315B2 (en) * 2000-05-04 2006-08-01 Ineos Fluor Holdings Limited Removal of (hydro)haloalkene impurities from product streams
WO2007079431A2 (en) * 2006-01-03 2007-07-12 Honeywell International Inc. Method for producing fluorinated organic compounds
WO2008001844A1 (en) * 2006-06-30 2008-01-03 Showa Denko K.K. Process for producing high-purity hexafluoropropylene and cleaning gas

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JPS6440507A (en) 1987-08-06 1989-02-10 Asahi Chemical Ind Production of fluorine-containing polymer
US5396000A (en) 1993-05-24 1995-03-07 E. I. Du Pont De Nemours And Company Process for the manufacture of 1,1,1,2,3,-pentafluoropropane
TWI288025B (en) 2000-09-14 2007-10-11 Showa Denko Kk Adsorbent for purifying perfluorocarbon, process for producing same, high purity octafluoropropane and octafluorocyclobutane, and use thereof
DE60205083T2 (en) 2001-01-15 2006-06-01 Showa Denko K.K. PROCESS FOR THE PREPARATION OF OCTAFLUOROPROPAN
JP2002226411A (en) 2001-01-30 2002-08-14 Asahi Glass Co Ltd Method for purifying 1,1,1,3,3-pentafluoropropane
CA2564991C (en) 2004-04-29 2013-03-19 Honeywell International Inc. Processes for synthesis of 1,3,3,3-tetrafluoropropene and 2,3,3,3-tetrafluoropropene
GB0611742D0 (en) * 2006-06-14 2006-07-26 Ineos Fluor Holdings Ltd Desiccants for fluids
KR101394583B1 (en) 2006-10-03 2014-05-12 멕시켐 아만코 홀딩 에스.에이. 데 씨.브이. Dehydrogenationhalogenation process for the production of C3-C6(hydro)fluoroalkenes

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3215747A (en) * 1963-05-31 1965-11-02 Pennsalt Chemicals Corp Method of separating trifluoroethylene from tetrafluoroethylene
EP0511612A2 (en) * 1991-04-27 1992-11-04 Hoechst Aktiengesellschaft Method for the purification of chlorofluorohydrocarbons
WO2001083411A1 (en) * 2000-05-04 2001-11-08 Ineos Fluor Holdings Limited Removal of (hydro)haloalkene impurities from product streams
US7084315B2 (en) * 2000-05-04 2006-08-01 Ineos Fluor Holdings Limited Removal of (hydro)haloalkene impurities from product streams
WO2007079431A2 (en) * 2006-01-03 2007-07-12 Honeywell International Inc. Method for producing fluorinated organic compounds
WO2008001844A1 (en) * 2006-06-30 2008-01-03 Showa Denko K.K. Process for producing high-purity hexafluoropropylene and cleaning gas

Also Published As

Publication number Publication date
CN102076645B (en) 2014-02-26
EP2303819B1 (en) 2014-05-07
FR2933402B1 (en) 2010-07-30
FR2933402A1 (en) 2010-01-08
ES2473468T3 (en) 2014-07-07
WO2010001025A2 (en) 2010-01-07
US8252964B2 (en) 2012-08-28
EP2303819A2 (en) 2011-04-06
US20110105809A1 (en) 2011-05-05
CN102076645A (en) 2011-05-25

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