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WO2009060793A1 - 炭素繊維ストランド及びその製造方法 - Google Patents

炭素繊維ストランド及びその製造方法 Download PDF

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Publication number
WO2009060793A1
WO2009060793A1 PCT/JP2008/069852 JP2008069852W WO2009060793A1 WO 2009060793 A1 WO2009060793 A1 WO 2009060793A1 JP 2008069852 W JP2008069852 W JP 2008069852W WO 2009060793 A1 WO2009060793 A1 WO 2009060793A1
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WO
WIPO (PCT)
Prior art keywords
strand
carbon fiber
carbon
fiber
fiber strand
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2008/069852
Other languages
English (en)
French (fr)
Inventor
Hidekazu Yoshikawa
Taro Oyama
Hiroshi Kimura
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Teijin Ltd
Original Assignee
Toho Tenax Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Toho Tenax Co Ltd filed Critical Toho Tenax Co Ltd
Priority to ES08848147T priority Critical patent/ES2389967T3/es
Priority to US12/740,043 priority patent/US8129017B2/en
Priority to EP08848147A priority patent/EP2208813B1/en
Publication of WO2009060793A1 publication Critical patent/WO2009060793A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • DTEXTILES; PAPER
    • D02YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02JFINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
    • D02J1/00Modifying the structure or properties resulting from a particular structure; Modifying, retaining, or restoring the physical form or cross-sectional shape, e.g. by use of dies or squeeze rollers
    • D02J1/08Interlacing constituent filaments without breakage thereof, e.g. by use of turbulent air streams
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F11/00Chemical after-treatment of artificial filaments or the like during manufacture
    • D01F11/10Chemical after-treatment of artificial filaments or the like during manufacture of carbon
    • D01F11/16Chemical after-treatment of artificial filaments or the like during manufacture of carbon by physicochemical methods
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01FCHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/20Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products
    • D01F9/21Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D01F9/22Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from polyaddition, polycondensation or polymerisation products from macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from polyacrylonitriles
    • DTEXTILES; PAPER
    • D02YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02JFINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
    • D02J1/00Modifying the structure or properties resulting from a particular structure; Modifying, retaining, or restoring the physical form or cross-sectional shape, e.g. by use of dies or squeeze rollers
    • D02J1/22Stretching or tensioning, shrinking or relaxing, e.g. by use of overfeed and underfeed apparatus, or preventing stretch
    • DTEXTILES; PAPER
    • D02YARNS; MECHANICAL FINISHING OF YARNS OR ROPES; WARPING OR BEAMING
    • D02JFINISHING OR DRESSING OF FILAMENTS, YARNS, THREADS, CORDS, ROPES OR THE LIKE
    • D02J1/00Modifying the structure or properties resulting from a particular structure; Modifying, retaining, or restoring the physical form or cross-sectional shape, e.g. by use of dies or squeeze rollers
    • D02J1/22Stretching or tensioning, shrinking or relaxing, e.g. by use of overfeed and underfeed apparatus, or preventing stretch
    • D02J1/222Stretching in a gaseous atmosphere or in a fluid bed
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10TTECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00Stock material or miscellaneous articles
    • Y10T428/29Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2913Rod, strand, filament or fiber
    • Y10T428/2918Rod, strand, filament or fiber including free carbon or carbide or therewith [not as steel]

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Fluid Mechanics (AREA)
  • Inorganic Fibers (AREA)

Abstract

 本発明により、炭素繊維の繊維軸方向に平行な複数の皺をその表面に有し、走査型プローブ顕微鏡を用いて測定する炭素繊維の表面の前記皺の間隔が120~160nmで、表面の皺の深さが12~23nm未満で、平均繊維直径が4.5~6.5μmで、比表面積が0.9~2.3m2/gで、密度が1.76g/cm3以上の炭素繊維が20000~30000本収束されてなる炭素繊維ストランドであって、前記炭素ストランドのストランド引張り強度が5900MPa以上、ストランド引張り弾性率が300GPa以上、張力9.8Nで巻取ったボビン上のストランドのストランド幅が5.5mm以上、走行中の炭素繊維ストランドに張力9.8Nを付加して3本のステンレス棒を通過させるストランド割れ評価方法においてストランド割れが観察されない炭素繊維ストランドが開示される。   
PCT/JP2008/069852 2007-11-06 2008-10-31 炭素繊維ストランド及びその製造方法 Ceased WO2009060793A1 (ja)

Priority Applications (3)

Application Number Priority Date Filing Date Title
ES08848147T ES2389967T3 (es) 2007-11-06 2008-10-31 Cable de fibras de carbono y proceso para su producción
US12/740,043 US8129017B2 (en) 2007-11-06 2008-10-31 Carbon fiber strand and process for producing the same
EP08848147A EP2208813B1 (en) 2007-11-06 2008-10-31 Carbon fiber strand and process for producing the same

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007-288170 2007-11-06
JP2007288170A JP5264150B2 (ja) 2007-11-06 2007-11-06 炭素繊維ストランド及びその製造方法

Publications (1)

Publication Number Publication Date
WO2009060793A1 true WO2009060793A1 (ja) 2009-05-14

Family

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Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/069852 Ceased WO2009060793A1 (ja) 2007-11-06 2008-10-31 炭素繊維ストランド及びその製造方法

Country Status (5)

Country Link
US (1) US8129017B2 (ja)
EP (1) EP2208813B1 (ja)
JP (1) JP5264150B2 (ja)
ES (1) ES2389967T3 (ja)
WO (1) WO2009060793A1 (ja)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014115762A1 (ja) * 2013-01-25 2014-07-31 東レ株式会社 サイジング剤塗布炭素繊維束、炭素繊維束の製造方法およびプリプレグ
JP2014159564A (ja) * 2013-01-25 2014-09-04 Toray Ind Inc プリプレグおよびサイジング剤塗布炭素繊維
JP2014159664A (ja) * 2013-01-25 2014-09-04 Toray Ind Inc サイジング剤塗布炭素繊維
JP2014159665A (ja) * 2013-01-25 2014-09-04 Toray Ind Inc 炭素繊維束の製造方法ならびに炭素繊維束
JP2015010290A (ja) * 2013-06-27 2015-01-19 東レ株式会社 炭素繊維束およびその製造方法

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5264150B2 (ja) * 2007-11-06 2013-08-14 東邦テナックス株式会社 炭素繊維ストランド及びその製造方法
EP2208812B1 (en) * 2007-11-06 2012-05-02 Toho Tenax Co., Ltd. Carbon fiber strand and process for producing the same
JP5419768B2 (ja) * 2010-03-25 2014-02-19 東邦テナックス株式会社 炭素繊維の表面処理方法、及び同処理方法により製造する炭素繊維
DE102011079506A1 (de) * 2011-07-20 2013-01-24 Sgl Carbon Se Ultradünne Fasern
JP6020201B2 (ja) * 2013-01-25 2016-11-02 東レ株式会社 炭素繊維束およびその製造方法
JP6040786B2 (ja) * 2013-01-25 2016-12-07 東レ株式会社 炭素繊維束
DE102013206984A1 (de) * 2013-04-18 2014-10-23 Bayerische Motoren Werke Aktiengesellschaft Verfahren zum Herstellen von Kohlefasern
JP6211881B2 (ja) * 2013-10-08 2017-10-11 東邦テナックス株式会社 炭素繊維及びその製造方法
US10570536B1 (en) 2016-11-14 2020-02-25 CFA Mills, Inc. Filament count reduction for carbon fiber tow
JP7341648B2 (ja) 2018-10-05 2023-09-11 帝人株式会社 前駆体繊維束の製造方法及び炭素繊維束の製造方法並びに炭素繊維束
TWI767796B (zh) * 2021-07-22 2022-06-11 臺灣塑膠工業股份有限公司 碳纖維的製造方法和碳纖維複合瓶

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JP2530767B2 (ja) * 1991-06-04 1996-09-04 東レ株式会社 炭素繊維及びその製造方法
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JP2003064539A (ja) * 2001-08-24 2003-03-05 Toho Tenax Co Ltd 炭素繊維織物、及びその製造方法
JP2003306836A (ja) * 2002-04-17 2003-10-31 Toho Tenax Co Ltd 炭素繊維ストランド及びその製造方法
JP2004107836A (ja) * 2002-09-19 2004-04-08 Toho Tenax Co Ltd 炭素繊維の製造法
JP2004285501A (ja) * 2003-03-20 2004-10-14 Teijin Fibers Ltd 異染性ポリエステル混繊糸およびその製造方法および織編物
JP2005133274A (ja) 2003-10-10 2005-05-26 Mitsubishi Rayon Co Ltd 炭素繊維と同炭素繊維を含む複合材料
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JP2005314830A (ja) * 2004-04-28 2005-11-10 Toho Tenax Co Ltd ポリアクリロニトリル系炭素繊維及びその製造方法
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JP2007177368A (ja) * 2005-12-01 2007-07-12 Toho Tenax Co Ltd 炭素繊維並びにプリカーサー及び炭素繊維の製造方法

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JP2530767B2 (ja) * 1991-06-04 1996-09-04 東レ株式会社 炭素繊維及びその製造方法
JPH1025627A (ja) 1997-04-04 1998-01-27 Mitsubishi Rayon Co Ltd アクリル系炭素繊維
JP2002327339A (ja) 2001-04-27 2002-11-15 Mitsubishi Rayon Co Ltd 炭素繊維及びその製造方法
JP2003064539A (ja) * 2001-08-24 2003-03-05 Toho Tenax Co Ltd 炭素繊維織物、及びその製造方法
JP2003306836A (ja) * 2002-04-17 2003-10-31 Toho Tenax Co Ltd 炭素繊維ストランド及びその製造方法
JP2004107836A (ja) * 2002-09-19 2004-04-08 Toho Tenax Co Ltd 炭素繊維の製造法
JP2004285501A (ja) * 2003-03-20 2004-10-14 Teijin Fibers Ltd 異染性ポリエステル混繊糸およびその製造方法および織編物
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WO2005078173A1 (ja) * 2004-02-13 2005-08-25 Mitsubishi Rayon Co., Ltd. 炭素繊維前駆体繊維束、その製造方法及び製造装置、並びに炭素繊維とその製造方法
JP2005314830A (ja) * 2004-04-28 2005-11-10 Toho Tenax Co Ltd ポリアクリロニトリル系炭素繊維及びその製造方法
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JP2007177368A (ja) * 2005-12-01 2007-07-12 Toho Tenax Co Ltd 炭素繊維並びにプリカーサー及び炭素繊維の製造方法

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014115762A1 (ja) * 2013-01-25 2014-07-31 東レ株式会社 サイジング剤塗布炭素繊維束、炭素繊維束の製造方法およびプリプレグ
JP2014159564A (ja) * 2013-01-25 2014-09-04 Toray Ind Inc プリプレグおよびサイジング剤塗布炭素繊維
JP2014159664A (ja) * 2013-01-25 2014-09-04 Toray Ind Inc サイジング剤塗布炭素繊維
JP2014159665A (ja) * 2013-01-25 2014-09-04 Toray Ind Inc 炭素繊維束の製造方法ならびに炭素繊維束
TWI504791B (zh) * 2013-01-25 2015-10-21 Toray Industries A carbon fiber bundle coated with a sizing agent, a method for producing a carbon fiber bundle, and a prepreg
KR101624839B1 (ko) 2013-01-25 2016-05-26 도레이 카부시키가이샤 사이징제 도포 탄소 섬유 다발, 탄소 섬유 다발의 제조 방법 및 프리프레그
US9435057B2 (en) 2013-01-25 2016-09-06 Toray Industries, Inc. Sizing agent-coated carbon fiber bundle, carbon fiber bundle production method, and prepreg
JP2015010290A (ja) * 2013-06-27 2015-01-19 東レ株式会社 炭素繊維束およびその製造方法

Also Published As

Publication number Publication date
EP2208813B1 (en) 2012-07-25
US8129017B2 (en) 2012-03-06
US20100252439A1 (en) 2010-10-07
JP5264150B2 (ja) 2013-08-14
JP2009114578A (ja) 2009-05-28
EP2208813A1 (en) 2010-07-21
EP2208813A4 (en) 2011-08-10
ES2389967T3 (es) 2012-11-05

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