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WO2008128278A3 - Treatment of nickel-containing solutions - Google Patents

Treatment of nickel-containing solutions Download PDF

Info

Publication number
WO2008128278A3
WO2008128278A3 PCT/AU2008/000533 AU2008000533W WO2008128278A3 WO 2008128278 A3 WO2008128278 A3 WO 2008128278A3 AU 2008000533 W AU2008000533 W AU 2008000533W WO 2008128278 A3 WO2008128278 A3 WO 2008128278A3
Authority
WO
WIPO (PCT)
Prior art keywords
nickel
iron
solution
liquor
ferrous
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/AU2008/000533
Other languages
French (fr)
Other versions
WO2008128278A2 (en
Inventor
Andrew Langham Gillies
Patirck Anthony Treasure
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
METALLICA MINERALS Ltd
Original Assignee
METALLICA MINERALS Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from AU2007902050A external-priority patent/AU2007902050A0/en
Application filed by METALLICA MINERALS Ltd filed Critical METALLICA MINERALS Ltd
Priority to AU2008241353A priority Critical patent/AU2008241353A1/en
Publication of WO2008128278A2 publication Critical patent/WO2008128278A2/en
Publication of WO2008128278A3 publication Critical patent/WO2008128278A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00Obtaining nickel or cobalt
    • C22B23/04Obtaining nickel or cobalt by wet processes
    • C22B23/0453Treatment or purification of solutions, e.g. obtained by leaching
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B23/00Obtaining nickel or cobalt
    • C22B23/04Obtaining nickel or cobalt by wet processes
    • C22B23/0453Treatment or purification of solutions, e.g. obtained by leaching
    • C22B23/0461Treatment or purification of solutions, e.g. obtained by leaching by chemical methods
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/22Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/42Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/20Treatment or purification of solutions, e.g. obtained by leaching
    • C22B3/44Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Environmental & Geological Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture And Refinement Of Metals (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)

Abstract

A method for the separation of nickel and iron from an acidic iron-containing nickel solution containing at least some dissolved iron in the ferric [Fe(III)] state comprises conducting a crude precipitation to precipitate some of the iron present in the solution by increasing the pH of the solution, electrochemically reducing the remaining ferric [Fe(III)] content of the iron-containing nickel solution to the ferrous [Fe(II)] state; and selectively separating the soluble nickel and ferrous [Fe(II)] components of the liquor by contacting the liquor with an ion exchange resin to selectively capture nickel. The nickel-loaded resin may be stripped to form a nickel-rich solution and nickel or a nickel product recovered from the nickel rich solution. The substantially nickel-free liquor derived from the ion exchange step may be treated to remove soluble iron therefrom.
PCT/AU2008/000533 2007-04-19 2008-04-16 Treatment of nickel-containing solutions Ceased WO2008128278A2 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU2008241353A AU2008241353A1 (en) 2007-04-19 2008-04-16 Treatment of nickel-containing solutions

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
AU2007902050 2007-04-19
AU2007902050A AU2007902050A0 (en) 2007-04-19 Treatment of Nickel-Containing Solutions

Publications (2)

Publication Number Publication Date
WO2008128278A2 WO2008128278A2 (en) 2008-10-30
WO2008128278A3 true WO2008128278A3 (en) 2008-12-18

Family

ID=39875997

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/AU2008/000533 Ceased WO2008128278A2 (en) 2007-04-19 2008-04-16 Treatment of nickel-containing solutions

Country Status (2)

Country Link
AU (1) AU2008241353A1 (en)
WO (1) WO2008128278A2 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2014025568A1 (en) * 2012-08-06 2014-02-13 Dow Global Technologies Llc Recovery of nickel using integrated continuous ion exchange and electo-winning process
CN112941314B (en) * 2021-01-29 2022-12-13 湖南邦普循环科技有限公司 Method for separating nickel and iron from nickel-iron alloy and application
CN117509760A (en) * 2023-12-04 2024-02-06 九江天赐资源循环科技有限公司 A method for jointly producing battery-grade nickel sulfate and battery-grade iron phosphate

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3450495A (en) * 1966-09-16 1969-06-17 Falconbridge Nickel Mines Ltd Method of precipitating metals as sulphides
AU424095B2 (en) * 1970-11-04 1972-05-11 Electrolytic Zinc Company Of Australasia Limited An improved method of removing dissolvede ferric iron from iron bearing solutions
GB2291870A (en) * 1994-08-01 1996-02-07 Gencor Ltd Recovering nickel from a nickel sulphide concentrate
WO2001032943A2 (en) * 1999-11-03 2001-05-10 Bhp Minerals International, Inc. Atmospheric leach process for the recovery of nickel and cobalt from limonite and saprolite ores
WO2002046481A1 (en) * 2000-12-08 2002-06-13 Outokumpu Oyj Method for the hydrolytic precitpitation of iron

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3450495A (en) * 1966-09-16 1969-06-17 Falconbridge Nickel Mines Ltd Method of precipitating metals as sulphides
AU424095B2 (en) * 1970-11-04 1972-05-11 Electrolytic Zinc Company Of Australasia Limited An improved method of removing dissolvede ferric iron from iron bearing solutions
GB2291870A (en) * 1994-08-01 1996-02-07 Gencor Ltd Recovering nickel from a nickel sulphide concentrate
WO2001032943A2 (en) * 1999-11-03 2001-05-10 Bhp Minerals International, Inc. Atmospheric leach process for the recovery of nickel and cobalt from limonite and saprolite ores
WO2002046481A1 (en) * 2000-12-08 2002-06-13 Outokumpu Oyj Method for the hydrolytic precitpitation of iron

Also Published As

Publication number Publication date
WO2008128278A2 (en) 2008-10-30
AU2008241353A1 (en) 2008-10-30

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