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WO2008126850A1 - 有機配位子を有する複合金属シアン化物錯体触媒、その製造方法およびポリエーテルポリオールの製造方法 - Google Patents

有機配位子を有する複合金属シアン化物錯体触媒、その製造方法およびポリエーテルポリオールの製造方法 Download PDF

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Publication number
WO2008126850A1
WO2008126850A1 PCT/JP2008/056982 JP2008056982W WO2008126850A1 WO 2008126850 A1 WO2008126850 A1 WO 2008126850A1 JP 2008056982 W JP2008056982 W JP 2008056982W WO 2008126850 A1 WO2008126850 A1 WO 2008126850A1
Authority
WO
WIPO (PCT)
Prior art keywords
metal cyanide
producing
composite metal
cyanide complex
organic ligand
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2008/056982
Other languages
English (en)
French (fr)
Inventor
Yoshinobu Kadowaki
Shigeru Ikai
Yasuyuki Sasao
Kazuhiko Yamada
Kenji Yamada
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
AGC Inc
Original Assignee
Asahi Glass Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Asahi Glass Co Ltd filed Critical Asahi Glass Co Ltd
Priority to CN2008800112724A priority Critical patent/CN101652403B/zh
Priority to EP08740085.9A priority patent/EP2135888A4/en
Priority to JP2009509352A priority patent/JP5109093B2/ja
Publication of WO2008126850A1 publication Critical patent/WO2008126850A1/ja
Priority to US12/575,501 priority patent/US20100041864A1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/24—Nitrogen compounds
    • B01J27/26—Cyanides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
    • B01J31/22—Organic complexes
    • B01J31/2204—Organic complexes the ligands containing oxygen or sulfur as complexing atoms
    • B01J31/2208—Oxygen, e.g. acetylacetonates
    • B01J31/2226—Anionic ligands, i.e. the overall ligand carries at least one formal negative charge
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/03—Precipitation; Co-precipitation
    • B01J37/031—Precipitation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Inorganic Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Polyethers (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

　触媒活性が高く、粒子の大きさが小さく、かつ粒子の大きさの均一性が高い、有機配位子を有する複合金属シアン化物錯体触媒を、再現性よく、簡便に製造できる製造方法を提供する。 　（ａ）ハロゲン化金属化合物水溶液とシアン化遷移金属化合物水溶液とを層流状態で接触させ、複合金属シアン化錯体を含む液を得る工程と、（ｂ）前記複合金属シアン化錯体を含む液と、有機配位子とを混合し、有機配位子を有する複合金属シアン化物錯体触媒を含む分散液を得る工程とを有する、有機配位子を有する複合金属シアン化錯体触媒の製造方法。
PCT/JP2008/056982 2007-04-10 2008-04-09 有機配位子を有する複合金属シアン化物錯体触媒、その製造方法およびポリエーテルポリオールの製造方法 Ceased WO2008126850A1 (ja)

Priority Applications (4)

Application Number Priority Date Filing Date Title
CN2008800112724A CN101652403B (zh) 2007-04-10 2008-04-09 具有有机配体的复合金属氰化物配位催化剂、其制造方法及聚醚多元醇的制造方法
EP08740085.9A EP2135888A4 (en) 2007-04-10 2008-04-09 COMPOUND CATALYST OF METAL CYANIDE COMPLEX WITH ORGANIC LIGAND, METHOD OF MANUFACTURING THEREOF, AND METHOD FOR PRODUCING POLYETHEREPOLYOLE
JP2009509352A JP5109093B2 (ja) 2007-04-10 2008-04-09 有機配位子を有する複合金属シアン化物錯体触媒、その製造方法およびポリエーテルポリオールの製造方法
US12/575,501 US20100041864A1 (en) 2007-04-10 2009-10-08 Double metal cyanide complex catalyst having organic ligand, process for its production and method for producing polyether polyol

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007-102507 2007-04-10
JP2007102507 2007-04-10

Related Child Applications (1)

Application Number Title Priority Date Filing Date
US12/575,501 Continuation US20100041864A1 (en) 2007-04-10 2009-10-08 Double metal cyanide complex catalyst having organic ligand, process for its production and method for producing polyether polyol

Publications (1)

Publication Number Publication Date
WO2008126850A1 true WO2008126850A1 (ja) 2008-10-23

Family

ID=39863947

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/056982 Ceased WO2008126850A1 (ja) 2007-04-10 2008-04-09 有機配位子を有する複合金属シアン化物錯体触媒、その製造方法およびポリエーテルポリオールの製造方法

Country Status (6)

Country Link
US (1) US20100041864A1 (ja)
EP (1) EP2135888A4 (ja)
JP (1) JP5109093B2 (ja)
CN (1) CN101652403B (ja)
TW (1) TW200911370A (ja)
WO (1) WO2008126850A1 (ja)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2013507241A (ja) * 2009-10-09 2013-03-04 ダウ グローバル テクノロジーズ エルエルシー 断熱栓流反応器及び該断熱栓流反応器を組み込んだプロセス
JP7681766B1 (ja) * 2024-07-05 2025-05-22 Ａｇｃ株式会社 組成物
JP7685099B1 (ja) * 2024-07-05 2025-05-28 Ａｇｃ株式会社 複合金属シアン化物錯体触媒及びポリエーテル化合物の製造方法
JP7751714B1 (ja) * 2024-11-18 2025-10-08 Ａｇｃ株式会社 複合金属シアン化物錯体触媒粉末及びポリエーテル化合物の製造方法

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CN102596387B (zh) 2009-10-09 2015-11-25 陶氏环球技术有限责任公司 生产氯化和/或氟化丙烯和高级烯烃的等温多管反应器和方法
KR20120084729A (ko) 2009-10-09 2012-07-30 다우 글로벌 테크놀로지스 엘엘씨 염화 및/또는 불화 프로펜 및 고급 알켄의 제조 방법
WO2012136658A1 (de) * 2011-04-04 2012-10-11 Henkel Ag & Co. Kgaa Katalysator zur epoxidpolymerisation und zur copolymerisation von epoxid mit kohlendioxid
CA2836493A1 (en) 2011-05-31 2012-12-06 Max Markus Tirtowidjojo Process for the production of chlorinated propenes
EP2714631B1 (en) 2011-05-31 2020-05-13 Blue Cube IP LLC Process for the production of chlorinated propenes
WO2013022676A1 (en) 2011-08-07 2013-02-14 Dow Global Technologies, Llc Process for the production of chlorinated propenes
WO2013022806A1 (en) 2011-08-07 2013-02-14 Dow Global Technologies, Llc Process for the production of chlorinated propenes
WO2013078035A1 (en) 2011-11-21 2013-05-30 Dow Global Technologies, Llc Process for the production of chlorinated alkanes
EP2785670B1 (en) 2011-12-02 2017-10-25 Blue Cube IP LLC Process for the production of chlorinated alkanes
WO2013082410A1 (en) 2011-12-02 2013-06-06 Dow Global Technologies, Llc Process for the production of chlorinated alkanes
CN104024188B (zh) 2011-12-13 2018-05-01 蓝立方知识产权有限责任公司 生产氯化丙烷和丙烯的方法
CA2860203C (en) 2011-12-22 2018-01-30 Dow Global Technologies Llc Process for the production of tetrachloromethane
WO2013096706A1 (en) 2011-12-23 2013-06-27 Dow Global Technologies, Llc Process for the production of alkenes and/or aromatic compounds
WO2014046970A1 (en) 2012-09-20 2014-03-27 Dow Global Technologies, Llc Process for the production of chlorinated propenes
JP2015529247A (ja) 2012-09-20 2015-10-05 ダウ グローバル テクノロジーズ エルエルシー 塩素化プロペンの生成のためのプロセス
CN104718020A (zh) 2012-09-30 2015-06-17 陶氏环球技术有限公司 堰式骤冷器和并入所述堰式骤冷器的工艺
US10065157B2 (en) 2012-10-26 2018-09-04 Blue Cube Ip Llc Mixer and processes incorporating the same
JP6247311B2 (ja) 2012-12-18 2017-12-13 ブルー キューブ アイピー エルエルシー 塩素化プロペンを生成するための方法
US9475740B2 (en) 2012-12-19 2016-10-25 Blue Cube Ip Llc Process for the production of chlorinated propenes
JP2016507590A (ja) 2013-02-27 2016-03-10 ブルー キューブ アイピー エルエルシー 塩素化プロペンを生成するための方法
EP2964597B1 (en) 2013-03-09 2017-10-04 Blue Cube IP LLC Process for the production of chlorinated alkanes

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04145123A (ja) 1990-10-05 1992-05-19 Asahi Glass Co Ltd ポリエーテル化合物の製造方法
JPH07196778A (ja) 1993-11-23 1995-08-01 Arco Chem Technol Lp 二金属シアン化物錯体触媒及びその製造方法ならびに前記触媒を用いてエポキシドポリマーを製造する方法
WO2000002951A1 (fr) * 1998-07-10 2000-01-20 Asahi Glass Company Ltd. Catalyseur de polymerisation par decyclisation d'un oxyde d'alkylene, et son procede de fabrication et d'utilisation
JP2003165837A (ja) * 2001-11-30 2003-06-10 Asahi Glass Co Ltd 複合金属シアン化物錯体触媒およびその製造方法
JP2003165836A (ja) * 2001-11-29 2003-06-10 Asahi Glass Co Ltd スラリー状複合金属シアン化物錯体触媒およびその製造方法、ならびにこれを用いたポリエーテルポリオールまたはポリエーテルモノオールの製造方法
JP2004535502A (ja) 2001-07-16 2004-11-25 シエル・インターナシヨネイル・リサーチ・マーチヤツピイ・ベー・ウイ 二重金属錯体触媒
JP2005015786A (ja) 2003-06-04 2005-01-20 Asahi Glass Co Ltd 複合金属シアン化物錯体触媒、その製造方法およびその利用
JP2007102507A (ja) 2005-10-05 2007-04-19 Solute Research Institute Ltd 不整形地の不整形度評価のためのシステム及び方法

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US6605422B2 (en) * 2001-03-16 2003-08-12 Fuji Photo Film Co., Ltd. Process for producing a silver halide photographic emulsion
EP1288244A1 (en) * 2001-08-31 2003-03-05 Asahi Glass Company, Limited Double metal cyanide complex catalyst for ring opening polymerization of alkylene oxide and its production process
DE10156117A1 (de) * 2001-11-15 2003-05-28 Basf Ag Verfahren zur Herstellung von Polyetheralkoholen
EP1908512A1 (en) * 2002-07-15 2008-04-09 Asahi Glass Company, Limited Process for producing inorganic spheres
EP1632517B1 (en) * 2003-06-04 2009-07-22 Asahi Glass Company Ltd. Composite metal cyanide complex catalyst, process for producing the same, and use of the same
DE602004029742D1 (de) * 2003-06-18 2010-12-09 Asahi Glass Co Ltd Verfahren und Vorrichtung zur Herstellung von anorganischen Sphären

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH04145123A (ja) 1990-10-05 1992-05-19 Asahi Glass Co Ltd ポリエーテル化合物の製造方法
JPH07196778A (ja) 1993-11-23 1995-08-01 Arco Chem Technol Lp 二金属シアン化物錯体触媒及びその製造方法ならびに前記触媒を用いてエポキシドポリマーを製造する方法
WO2000002951A1 (fr) * 1998-07-10 2000-01-20 Asahi Glass Company Ltd. Catalyseur de polymerisation par decyclisation d'un oxyde d'alkylene, et son procede de fabrication et d'utilisation
JP2004535502A (ja) 2001-07-16 2004-11-25 シエル・インターナシヨネイル・リサーチ・マーチヤツピイ・ベー・ウイ 二重金属錯体触媒
JP2003165836A (ja) * 2001-11-29 2003-06-10 Asahi Glass Co Ltd スラリー状複合金属シアン化物錯体触媒およびその製造方法、ならびにこれを用いたポリエーテルポリオールまたはポリエーテルモノオールの製造方法
JP2003165837A (ja) * 2001-11-30 2003-06-10 Asahi Glass Co Ltd 複合金属シアン化物錯体触媒およびその製造方法
JP2005015786A (ja) 2003-06-04 2005-01-20 Asahi Glass Co Ltd 複合金属シアン化物錯体触媒、その製造方法およびその利用
JP2007102507A (ja) 2005-10-05 2007-04-19 Solute Research Institute Ltd 不整形地の不整形度評価のためのシステム及び方法

Non-Patent Citations (1)

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Title
See also references of EP2135888A4

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2013507241A (ja) * 2009-10-09 2013-03-04 ダウ グローバル テクノロジーズ エルエルシー 断熱栓流反応器及び該断熱栓流反応器を組み込んだプロセス
JP7681766B1 (ja) * 2024-07-05 2025-05-22 Ａｇｃ株式会社 組成物
JP7685099B1 (ja) * 2024-07-05 2025-05-28 Ａｇｃ株式会社 複合金属シアン化物錯体触媒及びポリエーテル化合物の製造方法
JP7751714B1 (ja) * 2024-11-18 2025-10-08 Ａｇｃ株式会社 複合金属シアン化物錯体触媒粉末及びポリエーテル化合物の製造方法

Also Published As

Publication number Publication date
TW200911370A (en) 2009-03-16
JPWO2008126850A1 (ja) 2010-07-22
JP5109093B2 (ja) 2012-12-26
EP2135888A4 (en) 2014-10-01
EP2135888A1 (en) 2009-12-23
CN101652403B (zh) 2012-11-21
CN101652403A (zh) 2010-02-17
US20100041864A1 (en) 2010-02-18

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