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WO2008117665A1 - 硫化腐食防止方法、耐硫化腐食性高温部材及び伝熱管の補修方法 - Google Patents

硫化腐食防止方法、耐硫化腐食性高温部材及び伝熱管の補修方法 Download PDF

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Publication number
WO2008117665A1
WO2008117665A1 PCT/JP2008/054510 JP2008054510W WO2008117665A1 WO 2008117665 A1 WO2008117665 A1 WO 2008117665A1 JP 2008054510 W JP2008054510 W JP 2008054510W WO 2008117665 A1 WO2008117665 A1 WO 2008117665A1
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WIPO (PCT)
Prior art keywords
sulfide corrosion
oxide layer
titanium
transfer tube
resistance
Prior art date
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Ceased
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PCT/JP2008/054510
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English (en)
French (fr)
Inventor
Makoto Kawase
Masahiko Morinaga
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Central Research Institute of Electric Power Industry
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Central Research Institute of Electric Power Industry
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Publication date
Application filed by Central Research Institute of Electric Power Industry filed Critical Central Research Institute of Electric Power Industry
Priority to PL08721926T priority Critical patent/PL2130943T3/pl
Priority to JP2009506280A priority patent/JP5110608B2/ja
Priority to CN2008800090439A priority patent/CN101636524B/zh
Priority to EP08721926.7A priority patent/EP2130943B1/en
Priority to US12/294,536 priority patent/US20100233483A1/en
Publication of WO2008117665A1 publication Critical patent/WO2008117665A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C26/00—Coating not provided for in groups C23C2/00 - C23C24/00
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B18/00—Layered products essentially comprising ceramics, e.g. refractory products
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/1208—Oxides, e.g. ceramics
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/1208—Oxides, e.g. ceramics
    • C23C18/1216—Metal oxides
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
    • C23C18/122—Inorganic polymers, e.g. silanes, polysilazanes, polysiloxanes
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1225—Deposition of multilayers of inorganic material
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1229—Composition of the substrate
    • C23C18/1241—Metallic substrates
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/125—Process of deposition of the inorganic material
    • C23C18/1262—Process of deposition of the inorganic material involving particles, e.g. carbon nanotubes [CNT], flakes
    • C23C18/127—Preformed particles
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C28/00—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D
    • C23C28/04—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D only coatings of inorganic non-metallic material
    • C23C28/042—Coating for obtaining at least two superposed coatings either by methods not provided for in a single one of groups C23C2/00 - C23C26/00 or by combinations of methods provided for in subclasses C23C and C25C or C25D only coatings of inorganic non-metallic material including a refractory ceramic layer, e.g. refractory metal oxides, ZrO2, rare earth oxides
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C8/00—Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C8/02—Pretreatment of the material to be coated
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/30—Self-sustaining carbon mass or layer with impregnant or other layer

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Organic Chemistry (AREA)
  • Metallurgy (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Ceramic Engineering (AREA)
  • Nanotechnology (AREA)
  • Other Surface Treatments For Metallic Materials (AREA)
  • Application Of Or Painting With Fluid Materials (AREA)
  • Chemically Coating (AREA)

Abstract

基材を硫化腐食から保護する硫化腐食防止方法、優れた耐硫化腐食性を有する耐硫化腐食性高温部材、及び亀裂が生じた伝熱管の補修方法であって、基材の表面上にケイ素酸化物層を形成し、ケイ素酸化物層上にチタン金属又はチタン化合物を含有したチタン含有塗布液を塗布し、加熱酸化させて第１のチタン酸化物層を形成し、第１のチタン酸化物層上に炭素層を形成し、炭素層上にチタン含有塗布液を塗布し、加熱酸化させて第２のチタン酸化物層を形成することで、ケイ素酸化物層、第１のチタン酸化物層、炭素層及び第２のチタン酸化物層で基材を保護又は補修する。
PCT/JP2008/054510 2007-03-27 2008-03-12 硫化腐食防止方法、耐硫化腐食性高温部材及び伝熱管の補修方法 Ceased WO2008117665A1 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
PL08721926T PL2130943T3 (pl) 2007-03-27 2008-03-12 Sposób zapobiegania korozji siarczkowej, element wysokotemperaturowy odporny na korozję siarczkową
JP2009506280A JP5110608B2 (ja) 2007-03-27 2008-03-12 硫化腐食防止方法、耐硫化腐食性高温部材及び伝熱管の補修方法
CN2008800090439A CN101636524B (zh) 2007-03-27 2008-03-12 防硫化腐蚀方法、耐硫化腐蚀性高温部件以及导热管的修补方法
EP08721926.7A EP2130943B1 (en) 2007-03-27 2008-03-12 Method of preventing sulfide corrosion, high-temperature member with resistance to sulfide corrosion
US12/294,536 US20100233483A1 (en) 2007-03-27 2008-05-12 Sulfidation Corrosion Preventing Method, Sulfidation Corrosion-Resistant High Temperature Member and Heat Exchanger Tube Repairing Method

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2007080715 2007-03-27
JP2007-080715 2007-03-27
JP2007-303585 2007-11-22
JP2007303585 2007-11-22

Publications (1)

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WO2008117665A1 true WO2008117665A1 (ja) 2008-10-02

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PCT/JP2008/054510 Ceased WO2008117665A1 (ja) 2007-03-27 2008-03-12 硫化腐食防止方法、耐硫化腐食性高温部材及び伝熱管の補修方法

Country Status (6)

Country Link
US (1) US20100233483A1 (ja)
EP (1) EP2130943B1 (ja)
JP (1) JP5110608B2 (ja)
CN (1) CN101636524B (ja)
PL (1) PL2130943T3 (ja)
WO (1) WO2008117665A1 (ja)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2013019041A (ja) * 2011-07-14 2013-01-31 Toppan Printing Co Ltd 酸化亜鉛皮膜の形成方法
WO2019139008A1 (ja) * 2018-01-11 2019-07-18 日本板硝子株式会社 薄膜付き基材の製造方法及び薄膜付き基材
JP2021194575A (ja) * 2020-06-11 2021-12-27 株式会社東芝 塗膜の形成方法

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5588856B2 (ja) * 2010-12-27 2014-09-10 東京エレクトロン株式会社 カーボン膜上への酸化物膜の成膜方法及び成膜装置
CN104136138B (zh) * 2012-01-30 2018-03-20 赫姆洛克半导体运营有限责任公司 修复和/或保护反应器中表面的方法
US10651034B2 (en) * 2016-03-30 2020-05-12 U.S.A. As Represented By The Administrator Of The National Aeronautics And Space Administration Thermal absorption coating on sapphire for epitaxial process
FR3135316B1 (fr) * 2022-05-06 2024-05-03 Commissariat Energie Atomique Procede de traitement de surface pour ameliorer la performance d’un systeme thermodynamique avec cycle a absorption

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JPH09272990A (ja) 1996-04-05 1997-10-21 Kanmeta Eng Kk 金属表面の腐食等の防止剤及び腐食等の防止方法
JP2007009315A (ja) * 2005-06-01 2007-01-18 Central Res Inst Of Electric Power Ind 耐硫化腐食性高温部材及びその製造方法並びに高温部材の硫化腐食防止方法

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JPS60125375A (ja) * 1983-12-07 1985-07-04 Usui Internatl Ind Co Ltd 金属・セラミツクス接合体及びその製造方法
JPS637379A (ja) * 1986-06-25 1988-01-13 Matsushita Electric Works Ltd 多層薄膜の製法
JPH09272990A (ja) 1996-04-05 1997-10-21 Kanmeta Eng Kk 金属表面の腐食等の防止剤及び腐食等の防止方法
JP2007009315A (ja) * 2005-06-01 2007-01-18 Central Res Inst Of Electric Power Ind 耐硫化腐食性高温部材及びその製造方法並びに高温部材の硫化腐食防止方法

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2013019041A (ja) * 2011-07-14 2013-01-31 Toppan Printing Co Ltd 酸化亜鉛皮膜の形成方法
WO2019139008A1 (ja) * 2018-01-11 2019-07-18 日本板硝子株式会社 薄膜付き基材の製造方法及び薄膜付き基材
JPWO2019139008A1 (ja) * 2018-01-11 2020-12-24 日本板硝子株式会社 薄膜付き基材の製造方法及び薄膜付き基材
JP7186184B2 (ja) 2018-01-11 2022-12-08 日本板硝子株式会社 薄膜付き基材の製造方法及び薄膜付き基材
JP2021194575A (ja) * 2020-06-11 2021-12-27 株式会社東芝 塗膜の形成方法
JP7451311B2 (ja) 2020-06-11 2024-03-18 株式会社東芝 塗膜の形成方法

Also Published As

Publication number Publication date
EP2130943A1 (en) 2009-12-09
CN101636524A (zh) 2010-01-27
EP2130943B1 (en) 2019-09-11
JPWO2008117665A1 (ja) 2010-07-15
JP5110608B2 (ja) 2012-12-26
CN101636524B (zh) 2012-01-04
PL2130943T3 (pl) 2020-05-18
US20100233483A1 (en) 2010-09-16
EP2130943A4 (en) 2015-07-08

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