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WO2008111383A1 - アルミ改質コロイダルシリカ及びその製造方法 - Google Patents

アルミ改質コロイダルシリカ及びその製造方法 Download PDF

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Publication number
WO2008111383A1
WO2008111383A1 PCT/JP2008/053095 JP2008053095W WO2008111383A1 WO 2008111383 A1 WO2008111383 A1 WO 2008111383A1 JP 2008053095 W JP2008053095 W JP 2008053095W WO 2008111383 A1 WO2008111383 A1 WO 2008111383A1
Authority
WO
WIPO (PCT)
Prior art keywords
colloidal silica
aluminum
producing
modified colloidal
disclosed
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2008/053095
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English (en)
French (fr)
Inventor
Takao Yanagisawa
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fuso Chemical Co Ltd
Original Assignee
Fuso Chemical Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Fuso Chemical Co Ltd filed Critical Fuso Chemical Co Ltd
Priority to JP2009503952A priority Critical patent/JP5221517B2/ja
Publication of WO2008111383A1 publication Critical patent/WO2008111383A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B33/00—Silicon; Compounds thereof
    • C01B33/113—Silicon oxides; Hydrates thereof
    • C01B33/12—Silica; Hydrates thereof, e.g. lepidoic silicic acid
    • C01B33/14—Colloidal silica, e.g. dispersions, gels, sols
    • C01B33/146—After-treatment of sols
    • C01B33/148—Concentration; Drying; Dehydration; Stabilisation; Purification

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Silicon Compounds (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Abstract

（課題）高純度であるとともに、酸性領域でも安定なアルミ改質コロイダルシリカ及びその製造方法、並びに前記アルミ改質コロイダルシリカを、１００°C以下の低温で製造できる簡便な製造方法を提供すること。 （解決手段）以下の工程（１）～（３）を含むアルカリ金属含有量がそれぞれ５０ｐｐｍ以下であるアルミ改質コロイダルシリカの製造方法とする。 （１）アルコキシド法により得られるコロイダルシリカであって、ｐＨが６～１０であるコロイダルシリカに、Ａｌ２Ｏ３／ＳｉＯ２のモル比が０．００００５～０．０１の範囲になるように、アルミン酸塩水溶液を添加する工程 （２）工程（１）で得られたコロイダルシリカを６０～１００°Cに一定時間維持する工程 （３）工程（２）で得られたコロイダルシリカ中のアルカリイオンを必要に応じて除去してアルミ改質コロイダルシリカを得る工程
PCT/JP2008/053095 2007-03-13 2008-02-22 アルミ改質コロイダルシリカ及びその製造方法 Ceased WO2008111383A1 (ja)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2009503952A JP5221517B2 (ja) 2007-03-13 2008-02-22 アルミ改質コロイダルシリカ及びその製造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007-064094 2007-03-13
JP2007064094 2007-03-13

Publications (1)

Publication Number Publication Date
WO2008111383A1 true WO2008111383A1 (ja) 2008-09-18

Family

ID=39759325

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/053095 Ceased WO2008111383A1 (ja) 2007-03-13 2008-02-22 アルミ改質コロイダルシリカ及びその製造方法

Country Status (3)

Country Link
JP (1) JP5221517B2 (ja)
TW (1) TW200902445A (ja)
WO (1) WO2008111383A1 (ja)

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009197078A (ja) * 2008-02-20 2009-09-03 Jgc Catalysts & Chemicals Ltd ハードコート層形成用塗料組成物および光学物品
WO2010150677A1 (ja) * 2009-06-24 2010-12-29 日揮触媒化成株式会社 シリカ系微粒子分散ゾルの製造方法、シリカ系微粒子分散ゾル、該分散ゾルを含む塗料組成物、硬化性塗膜および硬化性塗膜付き基材
JP2012162426A (ja) * 2011-02-08 2012-08-30 Jgc Catalysts & Chemicals Ltd シリカ系微粒子の分散ゾル、該分散ゾルの製造方法および塗料組成物
WO2013183644A1 (ja) 2012-06-04 2013-12-12 ディップソール株式会社 アルミ変性コロイダルシリカを含有した３価クロム化成処理液
CN105586004A (zh) * 2015-12-31 2016-05-18 江苏天恒纳米科技股份有限公司 一种铝改性的硅溶胶的制备方法
CN111194344A (zh) * 2017-05-15 2020-05-22 沙特阿拉伯石油公司 用于地下地层中的水和气体封堵的组合物和方法
CN111320178A (zh) * 2020-03-02 2020-06-23 正大能源材料(大连)有限公司 一种用于合成sapo-34分子筛的金属改性硅溶胶及其制备方法
CN113135573A (zh) * 2021-05-26 2021-07-20 山东银丰纳米新材料有限公司 一种锆改性的阳离子型硅溶胶及其制备方法
CN115403050A (zh) * 2022-08-17 2022-11-29 苏州博来纳润电子材料有限公司 一种高纯有机铝改性酸性硅溶胶及其制备方法和应用

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101774067B1 (ko) * 2009-11-16 2017-09-01 닛키 쇼쿠바이카세이 가부시키가이샤 실리카·알루미나졸의 제조방법, 실리카·알루미나졸, 상기 졸을 포함하는 투명 피막형성용 도료 및 투명 피막 부착 기재
CN113174234A (zh) * 2020-11-12 2021-07-27 常州泰特耐特新材料科技有限公司 一种增强型芳纶浆粕的制备方法

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06199515A (ja) * 1992-09-25 1994-07-19 Nissan Chem Ind Ltd 酸性シリカゾルの製造方法
JP2000247625A (ja) * 1999-03-04 2000-09-12 Nippon Chem Ind Co Ltd 高純度シリカゾル及びその製造方法
JP2005162533A (ja) * 2003-12-02 2005-06-23 Fuso Chemical Co Ltd 変性コロイダルシリカの製造方法
JP2006036605A (ja) * 2004-07-29 2006-02-09 Catalysts & Chem Ind Co Ltd 高純度水性シリカゾルの製造方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH06199515A (ja) * 1992-09-25 1994-07-19 Nissan Chem Ind Ltd 酸性シリカゾルの製造方法
JP2000247625A (ja) * 1999-03-04 2000-09-12 Nippon Chem Ind Co Ltd 高純度シリカゾル及びその製造方法
JP2005162533A (ja) * 2003-12-02 2005-06-23 Fuso Chemical Co Ltd 変性コロイダルシリカの製造方法
JP2006036605A (ja) * 2004-07-29 2006-02-09 Catalysts & Chem Ind Co Ltd 高純度水性シリカゾルの製造方法

Cited By (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2009197078A (ja) * 2008-02-20 2009-09-03 Jgc Catalysts & Chemicals Ltd ハードコート層形成用塗料組成物および光学物品
US9441139B2 (en) 2009-06-24 2016-09-13 Jgc Catalysts And Chemicals Ltd. Process for producing silica-based fine particle dispersion sols, silica-based fine particle dispersion sol, coating composition containing the dispersion sol, curable coating film, and substrate having the curable coating film
WO2010150677A1 (ja) * 2009-06-24 2010-12-29 日揮触媒化成株式会社 シリカ系微粒子分散ゾルの製造方法、シリカ系微粒子分散ゾル、該分散ゾルを含む塗料組成物、硬化性塗膜および硬化性塗膜付き基材
JP2011026183A (ja) * 2009-06-24 2011-02-10 Jgc Catalysts & Chemicals Ltd シリカ系微粒子分散ゾルの製造方法、シリカ系微粒子分散ゾル、該分散ゾルを含む塗料組成物、硬化性塗膜および硬化性塗膜付き基材
EP2447211A4 (en) * 2009-06-24 2013-03-06 Jgc Catalysts & Chemicals Ltd METHOD FOR PRODUCING SOLICIDE WITH SILICONE BASED FINE PARTICLE SAMPLE, SOLICIUM BASED FINE PARTICLE SAMPLE METALISATION, SOLICIUM BASED SOLID COATING COMPOSITIONS WITH SOL SOLID BASED SOLVENT DISPERSIBILITY, HARDENABLE COATING FILM AND BASE WITH THE HARDENABLE COATING FILM
US9039828B2 (en) 2009-06-24 2015-05-26 Jgc Catalysts And Chemicals Ltd. Process for producing silica-based fine particle dispersion sols, silica-based fine particle dispersion sol, coating composition containing the dispersion sol, curable coating film, and substrate having the curable coating film
JP2012162426A (ja) * 2011-02-08 2012-08-30 Jgc Catalysts & Chemicals Ltd シリカ系微粒子の分散ゾル、該分散ゾルの製造方法および塗料組成物
WO2013183644A1 (ja) 2012-06-04 2013-12-12 ディップソール株式会社 アルミ変性コロイダルシリカを含有した３価クロム化成処理液
US9206321B2 (en) 2012-06-04 2015-12-08 Dipsol Chemicals Co., Ltd. Trivalent chromium-conversion processing solution containing aluminum-modified colloidal silica
CN105586004A (zh) * 2015-12-31 2016-05-18 江苏天恒纳米科技股份有限公司 一种铝改性的硅溶胶的制备方法
CN111194344A (zh) * 2017-05-15 2020-05-22 沙特阿拉伯石油公司 用于地下地层中的水和气体封堵的组合物和方法
CN111194344B (zh) * 2017-05-15 2022-08-30 沙特阿拉伯石油公司 用于地下地层中的水和气体封堵的组合物和方法
CN111320178A (zh) * 2020-03-02 2020-06-23 正大能源材料(大连)有限公司 一种用于合成sapo-34分子筛的金属改性硅溶胶及其制备方法
CN111320178B (zh) * 2020-03-02 2021-08-27 正大能源材料(大连)有限公司 一种用于合成sapo-34分子筛的金属改性硅溶胶及其制备方法
CN113135573A (zh) * 2021-05-26 2021-07-20 山东银丰纳米新材料有限公司 一种锆改性的阳离子型硅溶胶及其制备方法
CN115403050A (zh) * 2022-08-17 2022-11-29 苏州博来纳润电子材料有限公司 一种高纯有机铝改性酸性硅溶胶及其制备方法和应用
CN115403050B (zh) * 2022-08-17 2024-04-12 浙江博来纳润电子材料有限公司 一种高纯有机铝改性酸性硅溶胶及其制备方法和应用

Also Published As

Publication number Publication date
JP5221517B2 (ja) 2013-06-26
TW200902445A (en) 2009-01-16
JPWO2008111383A1 (ja) 2010-06-24

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