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WO2008105464A1 - カルボン酸クロライドの製造方法 - Google Patents

カルボン酸クロライドの製造方法 Download PDF

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Publication number
WO2008105464A1
WO2008105464A1 PCT/JP2008/053422 JP2008053422W WO2008105464A1 WO 2008105464 A1 WO2008105464 A1 WO 2008105464A1 JP 2008053422 W JP2008053422 W JP 2008053422W WO 2008105464 A1 WO2008105464 A1 WO 2008105464A1
Authority
WO
WIPO (PCT)
Prior art keywords
carboxylic acid
acid chloride
producing
catalyst
type compound
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2008/053422
Other languages
English (en)
French (fr)
Inventor
Takeshi Kobayashi
Kiyomi Kido
Akinori Nagatomo
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Chemicals Inc
Original Assignee
Mitsui Chemicals Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsui Chemicals Inc filed Critical Mitsui Chemicals Inc
Priority to EP08712044.0A priority Critical patent/EP2128122B1/en
Priority to US12/529,307 priority patent/US8198482B2/en
Priority to BRPI0808173A priority patent/BRPI0808173A2/pt
Priority to CN2008800068191A priority patent/CN101627000B/zh
Priority to JP2009501278A priority patent/JP5172820B2/ja
Publication of WO2008105464A1 publication Critical patent/WO2008105464A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/58—Preparation of carboxylic acid halides
    • C07C51/60—Preparation of carboxylic acid halides by conversion of carboxylic acids or their anhydrides or esters, lactones, salts into halides with the same carboxylic acid part
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/58—Preparation of carboxylic acid halides
    • C07C51/64—Separation; Purification; Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

　本発明は、熱安定性に欠けるカルボン酸クロライドや、高沸点で実質的に蒸留困難なカルボン酸クロライド中のヴィルスマイヤー試薬型化合物を効率良く、且つ、簡便な操作で分解し、次工程に悪影響を及ぼす事のない、カルボン酸クロライドの製造方法に関し、より詳しくは、触媒の存在下、塩素化剤とカルボン酸とを反応させ、該反応後に過剰の塩素化剤を系外に除去し、その後、さらに前記触媒に対して１.０～３.０当量の原料カルボン酸を系に添加して、系内に残存するヴィルスマイヤー試薬型化合物を分解することを特徴とする、カルボン酸クロライドの製造方法に関するものである。
PCT/JP2008/053422 2007-03-01 2008-02-27 カルボン酸クロライドの製造方法 Ceased WO2008105464A1 (ja)

Priority Applications (5)

Application Number Priority Date Filing Date Title
EP08712044.0A EP2128122B1 (en) 2007-03-01 2008-02-27 Process for producing carboxylic acid chloride
US12/529,307 US8198482B2 (en) 2007-03-01 2008-02-27 Method for producing carboxylic acid chloride
BRPI0808173A BRPI0808173A2 (pt) 2007-03-01 2008-02-27 método para a produção de cloreto de ácido carboxílico.
CN2008800068191A CN101627000B (zh) 2007-03-01 2008-02-27 酰氯的制备方法
JP2009501278A JP5172820B2 (ja) 2007-03-01 2008-02-27 カルボン酸クロライドの製造方法

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
JP2007051879 2007-03-01
JP2007-051879 2007-03-01

Publications (1)

Publication Number Publication Date
WO2008105464A1 true WO2008105464A1 (ja) 2008-09-04

Family

ID=39721289

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/053422 Ceased WO2008105464A1 (ja) 2007-03-01 2008-02-27 カルボン酸クロライドの製造方法

Country Status (6)

Country Link
US (1) US8198482B2 (ja)
EP (1) EP2128122B1 (ja)
JP (1) JP5172820B2 (ja)
CN (1) CN101627000B (ja)
BR (1) BRPI0808173A2 (ja)
WO (1) WO2008105464A1 (ja)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014058458A (ja) * 2012-09-14 2014-04-03 Nof Corp 脂肪族ジカルボン酸ジクロライドの製造方法
WO2020050368A1 (ja) * 2018-09-06 2020-03-12 国立大学法人神戸大学 ビルスマイヤー試薬の製造方法

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101863753B (zh) * 2010-06-17 2013-03-06 广东广益科技实业有限公司 一种棕榈酰氯的制备方法
CN102942470B (zh) * 2012-11-02 2015-06-24 常州大学 医药级正戊酰氯的生产工艺
CN105294421A (zh) * 2015-10-20 2016-02-03 安徽广信农化股份有限公司 一种硬酯酰氯的精制方法
US9914880B2 (en) 2015-12-04 2018-03-13 Uop Llc Method of increasing the yield of aviation fuel from renewable feedstocks
JP2020059678A (ja) * 2018-10-11 2020-04-16 京セラドキュメントソリューションズ株式会社 ナフタレンジカルボン酸ジクロリドの製造方法
CN112321419A (zh) * 2020-11-10 2021-02-05 安徽海顺化工有限公司 一种用于制备2-4-（氯苯基）-3-甲基丁酰氯的中间体的分离干燥工艺
CN114644558A (zh) * 2022-03-31 2022-06-21 福州大学 一种以己二酸单乙酯为原料的多步连续合成6-羟基-8-氯辛酸乙酯的方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS56104837A (en) * 1980-01-23 1981-08-20 Mitsui Toatsu Chem Inc Preparation of carboxylic acid chloride
US5200560A (en) 1990-04-21 1993-04-06 Basf Aktiengesellschaft Preparation of carboxylic chlorides
JPH0769970A (ja) * 1993-07-22 1995-03-14 Basf Ag カルボン酸塩化物の連続的製造方法
JPH10130198A (ja) * 1996-10-29 1998-05-19 Asahi Pen Chem Kk 塩化アシルの精製方法
JP2003509392A (ja) * 1999-09-13 2003-03-11 ビーエーエスエフ アクチェンゲゼルシャフト 塩化カルボニルを精製する方法

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3184506A (en) * 1961-07-19 1965-05-18 Du Pont Preparation of carboxylic acid chlorides
DE3039999A1 (de) * 1980-10-23 1982-05-27 Bayer Ag, 5090 Leverkusen N-alkylierte formamide, verfahren zu ihrer herstellung und ihre verwendung
DE19943844A1 (de) 1999-09-13 2001-03-15 Basf Ag Verfahren zur Herstellung von Carbonsäurechloriden
JP2002363130A (ja) 2001-05-31 2002-12-18 Asahi-Penn Chemical Co Ltd 着色の少ないカルボン酸クロライドの製造方法

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS56104837A (en) * 1980-01-23 1981-08-20 Mitsui Toatsu Chem Inc Preparation of carboxylic acid chloride
US5200560A (en) 1990-04-21 1993-04-06 Basf Aktiengesellschaft Preparation of carboxylic chlorides
JPH0769970A (ja) * 1993-07-22 1995-03-14 Basf Ag カルボン酸塩化物の連続的製造方法
JPH10130198A (ja) * 1996-10-29 1998-05-19 Asahi Pen Chem Kk 塩化アシルの精製方法
JP2003509392A (ja) * 1999-09-13 2003-03-11 ビーエーエスエフ アクチェンゲゼルシャフト 塩化カルボニルを精製する方法

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
See also references of EP2128122A4

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2014058458A (ja) * 2012-09-14 2014-04-03 Nof Corp 脂肪族ジカルボン酸ジクロライドの製造方法
WO2020050368A1 (ja) * 2018-09-06 2020-03-12 国立大学法人神戸大学 ビルスマイヤー試薬の製造方法
JPWO2020050368A1 (ja) * 2018-09-06 2021-08-30 国立大学法人神戸大学 ビルスマイヤー試薬の製造方法
JP7344518B2 (ja) 2018-09-06 2023-09-14 国立大学法人神戸大学 ビルスマイヤー試薬の製造方法

Also Published As

Publication number Publication date
JP5172820B2 (ja) 2013-03-27
US8198482B2 (en) 2012-06-12
JPWO2008105464A1 (ja) 2010-06-03
US20100099911A1 (en) 2010-04-22
CN101627000B (zh) 2012-12-26
EP2128122A1 (en) 2009-12-02
EP2128122B1 (en) 2014-01-22
CN101627000A (zh) 2010-01-13
BRPI0808173A2 (pt) 2018-11-13
EP2128122A4 (en) 2011-08-31

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