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WO2008151758A3 - Process and apparatus for mixing gases - Google Patents

Process and apparatus for mixing gases Download PDF

Info

Publication number
WO2008151758A3
WO2008151758A3 PCT/EP2008/004510 EP2008004510W WO2008151758A3 WO 2008151758 A3 WO2008151758 A3 WO 2008151758A3 EP 2008004510 W EP2008004510 W EP 2008004510W WO 2008151758 A3 WO2008151758 A3 WO 2008151758A3
Authority
WO
WIPO (PCT)
Prior art keywords
gas flow
converter
heat exchanger
supply pipe
integrated heat
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2008/004510
Other languages
French (fr)
Other versions
WO2008151758A2 (en
Inventor
Karl-Heinz Daum
Wolfram Schalk
Ventosa David Cachero
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Metso Corp
Original Assignee
Outotec Oyj
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Outotec Oyj filed Critical Outotec Oyj
Priority to AU2008261290A priority Critical patent/AU2008261290B2/en
Priority to CN200880019767.1A priority patent/CN101679037B/en
Priority to MX2009013478A priority patent/MX340510B/en
Publication of WO2008151758A2 publication Critical patent/WO2008151758A2/en
Publication of WO2008151758A3 publication Critical patent/WO2008151758A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/69Sulfur trioxide; Sulfuric acid
    • C01B17/74Preparation
    • C01B17/76Preparation by contact processes
    • C01B17/80Apparatus
    • C01B17/803Converters
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/10Mixing gases with gases
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30Injector mixers
    • B01F25/31Injector mixers in conduits or tubes through which the main component flows
    • B01F25/313Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced in the centre of the conduit
    • B01F25/3132Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced in the centre of the conduit by using two or more injector devices
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0461Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical annular shaped beds
    • B01J8/0469Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical annular shaped beds the beds being superimposed one above the other
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0492Feeding reactive fluids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0496Heating or cooling the reactor
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/69Sulfur trioxide; Sulfuric acid
    • C01B17/74Preparation
    • C01B17/76Preparation by contact processes
    • C01B17/765Multi-stage SO3-conversion
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00106Controlling the temperature by indirect heat exchange
    • B01J2208/00168Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00194Tubes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)

Abstract

When mixing two gases of different temperature and/or composition in a converter for producing SO3 from an SO2-containing gas, a first SO2-containing gas flow is introduced into the converter through a central supply pipe and passed through an integrated heat exchanger arranged around the central supply pipe, which is traversed by the first gas flow from the bottom to the top. A second gas flow is supplied via a ring conduit arranged above the integrated heat exchanger, from which the second gas flow is discharged through a plurality of openings and is fed into the first gas flow, so that it mixes with the same. Then, the gas mixture obtained is supplied to a contact stage of the converter, in which the SO2 is at least partly converted to SO3 on a catalyst.
PCT/EP2008/004510 2007-06-13 2008-06-06 Process and apparatus for mixing gases Ceased WO2008151758A2 (en)

Priority Applications (3)

Application Number Priority Date Filing Date Title
AU2008261290A AU2008261290B2 (en) 2007-06-13 2008-06-06 Process and apparatus for mixing gases
CN200880019767.1A CN101679037B (en) 2007-06-13 2008-06-06 Method and device for mixing gases
MX2009013478A MX340510B (en) 2007-06-13 2008-06-06 Process and apparatus for mixing gases.

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE102007027881.2 2007-06-13
DE102007027881A DE102007027881B4 (en) 2007-06-13 2007-06-13 Method and apparatus for mixing gases

Publications (2)

Publication Number Publication Date
WO2008151758A2 WO2008151758A2 (en) 2008-12-18
WO2008151758A3 true WO2008151758A3 (en) 2009-06-11

Family

ID=39827729

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2008/004510 Ceased WO2008151758A2 (en) 2007-06-13 2008-06-06 Process and apparatus for mixing gases

Country Status (7)

Country Link
CN (1) CN101679037B (en)
AU (1) AU2008261290B2 (en)
CL (1) CL2008001718A1 (en)
DE (1) DE102007027881B4 (en)
MX (1) MX340510B (en)
PE (1) PE20090270A1 (en)
WO (1) WO2008151758A2 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108046221A (en) * 2017-12-12 2018-05-18 中国恩菲工程技术有限公司 A kind of method of metallurgical off-gas acid-making

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102745654A (en) * 2012-07-31 2012-10-24 阳谷祥光铜业有限公司 Conversion device for acid-making with smoke, system and method for heating conversion device for acid-making with smoke
WO2025140972A1 (en) * 2023-12-28 2025-07-03 Metso Metals Oy Process and plant for producing a sulfur trioxide-containing gas

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4152407A (en) * 1977-02-02 1979-05-01 Warren Fuchs Process and apparatus for exothermic reactions
GB2139914A (en) * 1980-09-19 1984-11-21 Chemetics Int Catalytic converter
WO2004037719A1 (en) * 2002-10-24 2004-05-06 Outokumpu Oyj Process and plant for the manufacture of sulphuric acid from gases rich in sulphur dioxide
DE10359744A1 (en) * 2003-12-19 2005-07-14 Uhde Gmbh Method and device for injecting oxygen into a synthesis reactor

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2104858A (en) * 1935-01-23 1938-01-11 Gen Chemical Corp Manufacture of sulphuric acid
DE966833C (en) * 1951-10-10 1957-09-12 Basf Ag Device for the production of gases containing sulfur trioxide
DE1151341B (en) * 1961-03-21 1963-07-11 Schmidt Sche Heissdampf Installation of additional firing systems for introducing and mixing the fresh heating gas into exhaust gas ducts through which low-temperature exhaust gases flow
DE1926239U (en) * 1964-01-31 1965-11-04 Uhde Gmbh Friedrich DEVICE FOR MIXING GASES OF DIFFERENT DENSITY.
US3661165A (en) * 1970-07-21 1972-05-09 Nat Distillers Chem Corp System for mixing gases and sparger valve for accomplishing same
DE7242602U (en) * 1972-11-20 1976-04-29 Hoogovens Ijmuiden B.V., Ijmuiden (Niederlande)
US5480620A (en) * 1994-08-17 1996-01-02 Cameron; Gordon M. Catalytic converter
DE19800800C2 (en) 1998-01-13 2001-05-23 Metallgesellschaft Ag Process for the production of sulfuric acid
DE10023178A1 (en) 2000-05-11 2001-11-15 Mg Technologies Ag Two-stage catalytic production of sulfur trioxide gas with low sulfur dioxide content from high sulfur dioxide-content gas comprises use of two catalyst layers with temperature at each layer controlled

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4152407A (en) * 1977-02-02 1979-05-01 Warren Fuchs Process and apparatus for exothermic reactions
GB2139914A (en) * 1980-09-19 1984-11-21 Chemetics Int Catalytic converter
WO2004037719A1 (en) * 2002-10-24 2004-05-06 Outokumpu Oyj Process and plant for the manufacture of sulphuric acid from gases rich in sulphur dioxide
DE10359744A1 (en) * 2003-12-19 2005-07-14 Uhde Gmbh Method and device for injecting oxygen into a synthesis reactor

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108046221A (en) * 2017-12-12 2018-05-18 中国恩菲工程技术有限公司 A kind of method of metallurgical off-gas acid-making

Also Published As

Publication number Publication date
DE102007027881A1 (en) 2008-12-18
PE20090270A1 (en) 2009-03-19
DE102007027881B4 (en) 2012-02-16
CN101679037A (en) 2010-03-24
WO2008151758A2 (en) 2008-12-18
AU2008261290B2 (en) 2013-07-04
AU2008261290A1 (en) 2008-12-18
CL2008001718A1 (en) 2008-08-01
CN101679037B (en) 2015-03-04
MX2009013478A (en) 2010-01-18
MX340510B (en) 2016-07-11

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