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WO2008099929A1 - 非晶化セルロースの製造方法 - Google Patents

非晶化セルロースの製造方法 Download PDF

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Publication number
WO2008099929A1
WO2008099929A1 PCT/JP2008/052553 JP2008052553W WO2008099929A1 WO 2008099929 A1 WO2008099929 A1 WO 2008099929A1 JP 2008052553 W JP2008052553 W JP 2008052553W WO 2008099929 A1 WO2008099929 A1 WO 2008099929A1
Authority
WO
WIPO (PCT)
Prior art keywords
cellulose
raw material
crystallinity
containing raw
noncrystalline
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2008/052553
Other languages
English (en)
French (fr)
Inventor
Naoki Nojiri
Masahiro Umehara
Tomohito Kitsuki
Munehisa Okutsu
Keiichiro Tomioka
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kao Corp
Original Assignee
Kao Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Kao Corp filed Critical Kao Corp
Priority to CA002677870A priority Critical patent/CA2677870A1/en
Priority to ES08711383.3T priority patent/ES2515165T3/es
Priority to US12/527,047 priority patent/US8436165B2/en
Priority to CN2008800047250A priority patent/CN101605816B/zh
Priority to EP08711383.3A priority patent/EP2112169B1/en
Priority to KR1020097016091A priority patent/KR20090110322A/ko
Priority to BRPI0807910-2A2A priority patent/BRPI0807910A2/pt
Publication of WO2008099929A1 publication Critical patent/WO2008099929A1/ja
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B15/00—Preparation of other cellulose derivatives or modified cellulose, e.g. complexes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B1/00—Preparatory treatment of cellulose for making derivatives thereof, e.g. pre-treatment, pre-soaking, activation
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
    • C08B15/00—Preparation of other cellulose derivatives or modified cellulose, e.g. complexes
    • C08B15/08—Fractionation of cellulose, e.g. separation of cellulose crystallites
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
    • C08H8/00—Macromolecular compounds derived from lignocellulosic materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Materials Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)

Abstract

　セルロース含有原料から、セルロースＩ型結晶化度を低下させた非晶化セルロースを効率的に得られる生産性に優れた方法に関する。 　下記計算式で示されるセルロースＩ型結晶化度が３３％を超えるセルロース含有原料から非晶化セルロースを製造する方法であって、該セルロース含有原料が、嵩密度が１００～５００ｋｇ／ｍ3ものであり、かつ該原料から水を除いた残余の成分中のセルロース含有量が２０質量％以上であって、該セルロース含有原料を媒体式粉砕機で処理して、該セルロースＩ型結晶化度を３３％以下に低減する、非晶化セルロースの製造方法である。 　セルロースＩ型結晶化度（％）＝〔（Ｉ22.6－Ｉ18.5）／Ｉ22.6〕×１００ 〔Ｉ22.6はＸ線回折における格子面（００２面）の回折強度、Ｉ18.5はアモルファス部の回折強度を示す〕
PCT/JP2008/052553 2007-02-16 2008-02-15 非晶化セルロースの製造方法 Ceased WO2008099929A1 (ja)

Priority Applications (7)

Application Number Priority Date Filing Date Title
CA002677870A CA2677870A1 (en) 2007-02-16 2008-02-15 Process for producing noncrystalline cellulose
ES08711383.3T ES2515165T3 (es) 2007-02-16 2008-02-15 Proceso para producir celulosa no cristalina
US12/527,047 US8436165B2 (en) 2007-02-16 2008-02-15 Process for producing noncrystalline cellulose
CN2008800047250A CN101605816B (zh) 2007-02-16 2008-02-15 非晶纤维素的制造方法
EP08711383.3A EP2112169B1 (en) 2007-02-16 2008-02-15 Process for producing noncrystalline cellulose
KR1020097016091A KR20090110322A (ko) 2007-02-16 2008-02-15 비결정화 셀룰로오스의 제조 방법
BRPI0807910-2A2A BRPI0807910A2 (pt) 2007-02-16 2008-02-15 Processo para produzir celulose não-cristalina

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
JP2007-036742 2007-02-16
JP2007036742 2007-02-16
JP2007319988 2007-12-11
JP2007-319988 2007-12-11
JP2007322004 2007-12-13
JP2007-322004 2007-12-13

Publications (1)

Publication Number Publication Date
WO2008099929A1 true WO2008099929A1 (ja) 2008-08-21

Family

ID=39690154

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2008/052553 Ceased WO2008099929A1 (ja) 2007-02-16 2008-02-15 非晶化セルロースの製造方法

Country Status (8)

Country Link
US (1) US8436165B2 (ja)
EP (1) EP2112169B1 (ja)
KR (1) KR20090110322A (ja)
CN (1) CN101605816B (ja)
BR (1) BRPI0807910A2 (ja)
CA (1) CA2677870A1 (ja)
ES (1) ES2515165T3 (ja)
WO (1) WO2008099929A1 (ja)

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009084492A1 (en) * 2007-12-27 2009-07-09 Kao Corporation Process for producing saccharide
JP2010037526A (ja) * 2008-08-08 2010-02-18 Kao Corp 低結晶性セルロースの製造方法
JP2010047622A (ja) * 2008-08-19 2010-03-04 Kao Corp 低結晶性セルロースの製造方法
JP2010144098A (ja) * 2008-12-19 2010-07-01 Kao Corp 低結晶性キチンの製造方法
JP2010193858A (ja) * 2009-02-27 2010-09-09 Kao Corp キチン分解物の製造方法
WO2010134560A1 (ja) * 2009-05-21 2010-11-25 花王株式会社 非晶化セルロースの製造方法
JP2011012134A (ja) * 2009-06-30 2011-01-20 Kao Corp 低結晶性セルロースの製造方法
JP2011137094A (ja) * 2009-12-28 2011-07-14 Kao Corp 樹脂組成物
CN103242542A (zh) * 2013-05-29 2013-08-14 南京农业大学 非晶纤维素分散液的生产方法
JP2014198930A (ja) * 2009-05-15 2014-10-23 イメリーズ ミネラルズ リミテッド 紙填料組成物

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP2307500B1 (en) * 2008-07-22 2014-03-05 Kao Corporation Biodegradable resin composition
ES2348843B1 (es) * 2009-05-14 2011-10-07 Blanver Farmoquimica Ltda. Procedimiento para la preparacion de celulosa microcristalina.
JP5683092B2 (ja) 2009-10-29 2015-03-11 花王株式会社 カチオン化ヒドロキシプロピルセルロースの製造方法
CN102781966B (zh) * 2010-03-02 2015-08-26 花王株式会社 阳离子化纤维素以及阳离子化羟烷基纤维素的制造方法
JP5031054B2 (ja) * 2010-03-18 2012-09-19 信越化学工業株式会社 低置換度ヒドロキシプロピルセルロース及びこれを含む固形製剤
EP2616548A4 (en) * 2010-09-14 2015-01-28 Cellulose Sciences International Inc NANODEAGGREGATED CELLULOSE
EP2706072B1 (en) 2011-05-02 2015-09-09 Kao Corporation Method for producing alkali cellulose
JP6761695B2 (ja) 2016-08-16 2020-09-30 信越化学工業株式会社 低置換度ヒドロキシプロピルセルロース及び固形製剤
US11066558B2 (en) * 2017-07-21 2021-07-20 Kao Corporation Asphalt composition, method for producing same and additive for asphalt
KR102171777B1 (ko) 2019-02-11 2020-10-29 강원대학교산학협력단 나노셀룰로오스 제조용 공융용매 및 이를 이용한 나노셀룰로오스 제조 방법

Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS62236801A (ja) 1986-04-08 1987-10-16 Asahi Chem Ind Co Ltd 可溶性セルロ−スの製造方法
JPH05168969A (ja) 1991-12-24 1993-07-02 Matsushita Electric Works Ltd 布シート材の粉砕方法
JPH06107701A (ja) * 1992-03-23 1994-04-19 Nippon Paper Ind Co Ltd 嵩密度の高いカルボキシメチルセルロースの製造方法
JP2001009316A (ja) * 1999-06-29 2001-01-16 Shin Etsu Chem Co Ltd パルプの粉末化方法及びセルロースエーテルの製造方法
JP2001354701A (ja) 2000-06-14 2001-12-25 Shin Etsu Chem Co Ltd 粉末状パルプの製造方法及びセルロースエーテルの製造方法
JP2003064184A (ja) 2001-08-24 2003-03-05 Toray Ind Inc セルロース溶液及び熱可塑性セルロースエステルの製造方法
JP2004115700A (ja) * 2002-09-27 2004-04-15 Nippon Paper Industries Co Ltd 粉末状セルロースおよびその製造法
JP2004331918A (ja) 2003-05-12 2004-11-25 Asahi Kasei Chemicals Corp 非晶質セルロース微粉体
JP2005068140A (ja) 2003-08-07 2005-03-17 Nippon Paper Chemicals Co Ltd セロオリゴ糖の製造方法

Family Cites Families (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3817983A (en) * 1972-05-01 1974-06-18 Du Pont Process using diverse types of cellulose for preparing viscose
DE3038001A1 (de) * 1980-10-08 1982-05-06 Henkel KGaA, 4000 Düsseldorf Verfahren zur herstellung von mikropulvern aus celluloseether oder cellulose
EP1792930B1 (en) * 2004-08-10 2013-02-13 Idemitsu Technofine Co. Ltd Modified powder, fluid composition containing said modified powder, formed article, and method for producing modified powder
US20100274001A1 (en) * 2007-10-25 2010-10-28 Kao Corporation Method for producing cellulose ether derivative
JP2009120716A (ja) * 2007-11-14 2009-06-04 Kao Corp ヒドロキシエチルセルロースの製造方法
EP2226335B1 (en) * 2007-12-27 2013-09-25 Kao Corporation Method for producing methyl cellulose
CA2710504A1 (en) * 2007-12-27 2009-07-09 Kao Corporation Process for producing saccharide

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS62236801A (ja) 1986-04-08 1987-10-16 Asahi Chem Ind Co Ltd 可溶性セルロ−スの製造方法
JPH05168969A (ja) 1991-12-24 1993-07-02 Matsushita Electric Works Ltd 布シート材の粉砕方法
JPH06107701A (ja) * 1992-03-23 1994-04-19 Nippon Paper Ind Co Ltd 嵩密度の高いカルボキシメチルセルロースの製造方法
JP2001009316A (ja) * 1999-06-29 2001-01-16 Shin Etsu Chem Co Ltd パルプの粉末化方法及びセルロースエーテルの製造方法
JP2001354701A (ja) 2000-06-14 2001-12-25 Shin Etsu Chem Co Ltd 粉末状パルプの製造方法及びセルロースエーテルの製造方法
JP2003064184A (ja) 2001-08-24 2003-03-05 Toray Ind Inc セルロース溶液及び熱可塑性セルロースエステルの製造方法
JP2004115700A (ja) * 2002-09-27 2004-04-15 Nippon Paper Industries Co Ltd 粉末状セルロースおよびその製造法
JP2004331918A (ja) 2003-05-12 2004-11-25 Asahi Kasei Chemicals Corp 非晶質セルロース微粉体
JP2005068140A (ja) 2003-08-07 2005-03-17 Nippon Paper Chemicals Co Ltd セロオリゴ糖の製造方法

Non-Patent Citations (2)

* Cited by examiner, † Cited by third party
Title
"Handbook of Analytical Chemistry", 30 November 1991, MARUZEN CO., LTD., article "Japan Institute of Analytical Chemistry", pages: 1081 - 1082
See also references of EP2112169A4

Cited By (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009084492A1 (en) * 2007-12-27 2009-07-09 Kao Corporation Process for producing saccharide
JP2010037526A (ja) * 2008-08-08 2010-02-18 Kao Corp 低結晶性セルロースの製造方法
JP2010047622A (ja) * 2008-08-19 2010-03-04 Kao Corp 低結晶性セルロースの製造方法
JP2010144098A (ja) * 2008-12-19 2010-07-01 Kao Corp 低結晶性キチンの製造方法
JP2010193858A (ja) * 2009-02-27 2010-09-09 Kao Corp キチン分解物の製造方法
JP2014198930A (ja) * 2009-05-15 2014-10-23 イメリーズ ミネラルズ リミテッド 紙填料組成物
JP2022062145A (ja) * 2009-05-15 2022-04-19 ファイバーリーン テクノロジーズ リミテッド 紙填料組成物
JP2011001547A (ja) * 2009-05-21 2011-01-06 Kao Corp 非晶化セルロースの製造方法
CN102439046A (zh) * 2009-05-21 2012-05-02 花王株式会社 非结晶纤维素的制造方法
WO2010134560A1 (ja) * 2009-05-21 2010-11-25 花王株式会社 非晶化セルロースの製造方法
JP2011012134A (ja) * 2009-06-30 2011-01-20 Kao Corp 低結晶性セルロースの製造方法
JP2011137094A (ja) * 2009-12-28 2011-07-14 Kao Corp 樹脂組成物
CN103242542A (zh) * 2013-05-29 2013-08-14 南京农业大学 非晶纤维素分散液的生产方法

Also Published As

Publication number Publication date
US8436165B2 (en) 2013-05-07
BRPI0807910A2 (pt) 2014-06-24
CN101605816A (zh) 2009-12-16
CN101605816B (zh) 2011-11-09
KR20090110322A (ko) 2009-10-21
EP2112169A4 (en) 2010-12-08
EP2112169B1 (en) 2014-07-30
ES2515165T3 (es) 2014-10-29
CA2677870A1 (en) 2008-08-21
US20100105891A1 (en) 2010-04-29
EP2112169A1 (en) 2009-10-28

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