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WO2008078040A3 - Procédé et appareil de séparation d'un mélange comprenant au moins de l'hydrogène, de l'azote et du monoxyde de carbone par distillation cryogénique - Google Patents

Procédé et appareil de séparation d'un mélange comprenant au moins de l'hydrogène, de l'azote et du monoxyde de carbone par distillation cryogénique Download PDF

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Publication number
WO2008078040A3
WO2008078040A3 PCT/FR2007/052486 FR2007052486W WO2008078040A3 WO 2008078040 A3 WO2008078040 A3 WO 2008078040A3 FR 2007052486 W FR2007052486 W FR 2007052486W WO 2008078040 A3 WO2008078040 A3 WO 2008078040A3
Authority
WO
WIPO (PCT)
Prior art keywords
carbon monoxide
separating
nitrogen
column
hydrogen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/FR2007/052486
Other languages
English (en)
Other versions
WO2008078040A2 (fr
Inventor
Arthur Darde
Antoine Hernandez
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Original Assignee
Air Liquide SA
LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Air Liquide SA, LAir Liquide SA pour lEtude et lExploitation des Procedes Georges Claude filed Critical Air Liquide SA
Priority to CN2007800477659A priority Critical patent/CN101568788B/zh
Priority to US12/519,990 priority patent/US8555673B2/en
Priority to EP07871916.8A priority patent/EP2140216B1/fr
Publication of WO2008078040A2 publication Critical patent/WO2008078040A2/fr
Publication of WO2008078040A3 publication Critical patent/WO2008078040A3/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0204—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the feed stream
    • F25J3/0223—H2/CO mixtures, i.e. synthesis gas; Water gas or shifted synthesis gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0252—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of hydrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0257—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of nitrogen
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/0228—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream
    • F25J3/0261—Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream characterised by the separated product stream separation of carbon monoxide
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/70—Refluxing the column with a condensed part of the feed stream, i.e. fractionator top is stripped or self-rectified
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00—Processes or apparatus using separation by rectification
    • F25J2200/74—Refluxing the column with at least a part of the partially condensed overhead gas
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2205/00—Processes or apparatus using other separation and/or other processing means
    • F25J2205/30—Processes or apparatus using other separation and/or other processing means using a washing, e.g. "scrubbing" or bubble column for purification purposes
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2240/00—Processes or apparatus involving steps for expanding of process streams
    • F25J2240/40—Expansion without extracting work, i.e. isenthalpic throttling, e.g. JT valve, regulating valve or venturi, or isentropic nozzle, e.g. Laval
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/02—Internal refrigeration with liquid vaporising loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/04—Internal refrigeration with work-producing gas expansion loop
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2270/00—Refrigeration techniques used
    • F25J2270/24—Quasi-closed internal or closed external carbon monoxide refrigeration cycle
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25J—LIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2280/00—Control of the process or apparatus
    • F25J2280/02—Control in general, load changes, different modes ("runs"), measurements

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Carbon And Carbon Compounds (AREA)

Abstract

Dans un procédé de séparation d' un mélange de monoxyde de carbone, d' azote, d' hydrogène par distillation cryogénique dans un système de moyens de séparation comprenant une colonne de déazotation (C4) et au moins une autre colonne, on sépare le mélange pour obtenir un fluide enrichi en monoxyde de carbone et contenant de l' azote, on sépare ce fluide dans la colonne de déazotation, on comprime un débit de monoxyde de carbone provenant du système de colonnes dans un compresseur (V1,V2) jusqu' à une haute pression, une fraction (7) de débit de monoxyde de carbone à haute pression sert de produit, on détend une quantité variable (57) du débit de monoxyde de carbone à haute pression refroidi dans une vanne (59) avant de l' envoyer en cuve de la colonne de déazotation et on varie le débit détendu dans la vanne en fonction des besoins de rebouillage de la colonne de déazotation.
PCT/FR2007/052486 2006-12-21 2007-12-12 Procédé et appareil de séparation d'un mélange comprenant au moins de l'hydrogène, de l'azote et du monoxyde de carbone par distillation cryogénique Ceased WO2008078040A2 (fr)

Priority Applications (3)

Application Number Priority Date Filing Date Title
CN2007800477659A CN101568788B (zh) 2006-12-21 2007-12-12 通过低温蒸馏分离至少包含氢、氮和一氧化碳的混合物的方法和设备
US12/519,990 US8555673B2 (en) 2006-12-21 2007-12-12 Method and device for separating a mixture of at least hydrogen, nitrogen, and carbon monoxide by cryogenic distillation
EP07871916.8A EP2140216B1 (fr) 2006-12-21 2007-12-12 Procédé et appareil de séparation d'un mélange comprenant au moins de l'hydrogène, de l'azote et du monoxyde de carbone par distillation cryogénique

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR0655770 2006-12-21
FR0655770A FR2910602B1 (fr) 2006-12-21 2006-12-21 Procede et appareil de separation d'un melange comprenant au moins de l'hydrogene, de l'azote et du monoxyde de carbone par distillation cryogenique

Publications (2)

Publication Number Publication Date
WO2008078040A2 WO2008078040A2 (fr) 2008-07-03
WO2008078040A3 true WO2008078040A3 (fr) 2009-05-22

Family

ID=38326917

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/FR2007/052486 Ceased WO2008078040A2 (fr) 2006-12-21 2007-12-12 Procédé et appareil de séparation d'un mélange comprenant au moins de l'hydrogène, de l'azote et du monoxyde de carbone par distillation cryogénique

Country Status (5)

Country Link
US (1) US8555673B2 (fr)
EP (1) EP2140216B1 (fr)
CN (1) CN101568788B (fr)
FR (1) FR2910602B1 (fr)
WO (1) WO2008078040A2 (fr)

Families Citing this family (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20100251765A1 (en) 2009-04-01 2010-10-07 Air Products And Chemicals, Inc. Cryogenic Separation of Synthesis Gas
FR2959297B1 (fr) * 2010-04-22 2012-04-27 Air Liquide Procede et appareil de production d'azote par distillation cryogenique d'air
EP2562502A1 (fr) * 2011-06-24 2013-02-27 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude Procédé et installation pour la fourniture d'un monoxyde de carbone gazeux par distillation cryogénique
FR3058996B1 (fr) * 2016-11-18 2022-01-07 Air Liquide Procede et installation de separation cryogenique d’un melange gazeux par lavage au methane
IT201700042150A1 (it) * 2017-04-14 2018-10-14 Cristiano Galbiati Separation equipment
CN107084594B (zh) * 2017-04-27 2022-07-26 杭州中泰深冷技术股份有限公司 一种液co循环制冷合成气制甲醇联产lng装置及其使用方法

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4478621A (en) * 1982-04-28 1984-10-23 Linde Aktiengesellschaft Process for the extraction of carbon monoxide from gas streams
DE19541339A1 (de) * 1995-11-06 1997-05-07 Linde Ag Verfahren zum Gewinnen von Kohlenmonoxid
US6062042A (en) * 1998-01-13 2000-05-16 Air Products And Chemicals, Inc. Seperation of carbon monoxide from nitrogen-contaminated gaseous mixtures

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US3756036A (en) * 1971-04-20 1973-09-04 Phillips Petroleum Co Demethanizing method and apparatus
GB1436542A (en) * 1972-05-10 1976-05-19 Air Prod & Chem Separation of gases
US4952223A (en) * 1989-08-21 1990-08-28 The Boc Group, Inc. Method and apparatus of producing carbon dioxide in high yields from low concentration carbon dioxide feeds
FR2718428B1 (fr) * 1994-04-11 1997-10-10 Air Liquide Procédé et installation de production de monoxyde de carbone.
DE4433114A1 (de) * 1994-09-16 1996-03-21 Linde Ag Verfahren zum Gewinnen einer Kohlenmonoxid-Reinfraktion
FR2754541B1 (fr) * 1996-10-15 1998-12-24 Air Liquide Procede et installation pour la separation d'un melange d'hydrogene et/ou d'au moins un hydrocarbure et/ou d'azote et/ou d'oxyde de carbone
US5992175A (en) * 1997-12-08 1999-11-30 Ipsi Llc Enhanced NGL recovery processes
GB9800692D0 (en) * 1998-01-13 1998-03-11 Air Prod & Chem Separation of carbon monoxide from nitrogen-contaminated gaseous mixtures also containing hydrogen and methane
US7107788B2 (en) * 2003-03-07 2006-09-19 Abb Lummus Global, Randall Gas Technologies Residue recycle-high ethane recovery process
EP1479990A1 (fr) * 2003-05-19 2004-11-24 L'Air Liquide Société Anonyme à Directoire et Conseil de Surveillance pour l'Etude et Exploitation des Procédés Georges Claude Procédé et installation pour la production d'un mélange contenant au moins 10% de monoxyde de carbone
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US7617701B2 (en) * 2004-04-07 2009-11-17 L'air Liquide, Societe Anonyme A Directoire Et Conseil De Surveillance Pour L'etude Et L'exploitation Des Procedes Georges Claude Process and installation for providing a fluid mixture containing at least 10% carbon monoxide
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FR2879595A3 (fr) * 2006-01-26 2006-06-23 Air Liquide Procede d'integration d'une unite de deazotation sur une boite froide produisant du monoxyde de carbone
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Publication number Priority date Publication date Assignee Title
US4478621A (en) * 1982-04-28 1984-10-23 Linde Aktiengesellschaft Process for the extraction of carbon monoxide from gas streams
DE19541339A1 (de) * 1995-11-06 1997-05-07 Linde Ag Verfahren zum Gewinnen von Kohlenmonoxid
US6062042A (en) * 1998-01-13 2000-05-16 Air Products And Chemicals, Inc. Seperation of carbon monoxide from nitrogen-contaminated gaseous mixtures

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Title
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BERNINGER R: "FORTSCHRITTE BEI DER H2/CO-TIEFTEMPERATURZERLEGUNG", BERICHTE AUS TECHNIK UND WISSENSCHAFT, LINDE AG. WIESBADEN, DE, vol. 62, 1988, pages 18 - 23, XP001181523, ISSN: 0942-332X *

Also Published As

Publication number Publication date
US8555673B2 (en) 2013-10-15
WO2008078040A2 (fr) 2008-07-03
CN101568788B (zh) 2011-11-02
EP2140216B1 (fr) 2017-11-08
US20100071411A1 (en) 2010-03-25
CN101568788A (zh) 2009-10-28
FR2910602B1 (fr) 2012-12-14
FR2910602A1 (fr) 2008-06-27
EP2140216A2 (fr) 2010-01-06

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