[go: up one dir, main page]

WO2007033815A3 - Electrochemical method for producing nanoscalar metal compounds - Google Patents

Electrochemical method for producing nanoscalar metal compounds Download PDF

Info

Publication number
WO2007033815A3
WO2007033815A3 PCT/EP2006/009106 EP2006009106W WO2007033815A3 WO 2007033815 A3 WO2007033815 A3 WO 2007033815A3 EP 2006009106 W EP2006009106 W EP 2006009106W WO 2007033815 A3 WO2007033815 A3 WO 2007033815A3
Authority
WO
WIPO (PCT)
Prior art keywords
particles
nanoscalar
producing
electrolyte solution
electrochemical method
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/EP2006/009106
Other languages
German (de)
French (fr)
Other versions
WO2007033815A2 (en
Inventor
Wolfgang Kochanek
Martin Seipenbusch
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Leibniz Institut fuer Neue Materialien Gemeinnuetzige GmbH
Original Assignee
Leibniz Institut fuer Neue Materialien Gemeinnuetzige GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Leibniz Institut fuer Neue Materialien Gemeinnuetzige GmbH filed Critical Leibniz Institut fuer Neue Materialien Gemeinnuetzige GmbH
Publication of WO2007033815A2 publication Critical patent/WO2007033815A2/en
Publication of WO2007033815A3 publication Critical patent/WO2007033815A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B1/00Electrolytic production of inorganic compounds or non-metals
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B82NANOTECHNOLOGY
    • B82YSPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00Nanotechnology for materials or surface science, e.g. nanocomposites

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Nanotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Electrochemistry (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Electrolytic Production Of Metals (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)

Abstract

The invention relates to an electrochemical method for producing nanoscalar particles from a metal compound. In said method, metals are anodically dissolved in an electrolytic cell, the electrolyte solution forming a precipitating component, which produces a poorly soluble compound with the metal ions that are formed and comprising a surface modification agent, which permits surface-modified particles to be formed from the metal compound or a precursor of the latter. The method optionally comprises the isolation of the particles thus formed from the electrolyte solution and the optional calcination of said particles. The method is devoid of waste water and is therefore environmentally friendly and cost-effective. The nanoscalar particles that are produced can be easily redispersed in organic and aqueous media and have a high degree of purity. The particle size can lie significantly below 100 nm. The method is particularly suitable for producing simple metal oxides such as iron oxide and binary metal oxides such as ITO and ATO.
PCT/EP2006/009106 2005-09-20 2006-09-19 Electrochemical method for producing nanoscalar metal compounds Ceased WO2007033815A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE200510044873 DE102005044873A1 (en) 2005-09-20 2005-09-20 Electrochemical process for the production of nanoscale metal compounds
DE102005044873.9 2005-09-20

Publications (2)

Publication Number Publication Date
WO2007033815A2 WO2007033815A2 (en) 2007-03-29
WO2007033815A3 true WO2007033815A3 (en) 2007-09-13

Family

ID=37762352

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/EP2006/009106 Ceased WO2007033815A2 (en) 2005-09-20 2006-09-19 Electrochemical method for producing nanoscalar metal compounds

Country Status (2)

Country Link
DE (1) DE102005044873A1 (en)
WO (1) WO2007033815A2 (en)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009108286A1 (en) * 2008-02-28 2009-09-03 Corning Incorporated Electrochemical methods of making nanostructures
US20110052896A1 (en) * 2009-08-27 2011-03-03 Shrisudersan Jayaraman Zinc Oxide and Cobalt Oxide Nanostructures and Methods of Making Thereof
NL2005112C2 (en) 2010-07-19 2012-01-23 Univ Leiden Process to prepare metal nanoparticles or metal oxide nanoparticles.
CN114725324B (en) * 2022-03-04 2024-04-30 中山大学 Preparation and application of zinc metal anode integrated by coordination supermolecular grid material

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4067788A (en) * 1976-09-20 1978-01-10 Electromedia, Inc. Electrochemical production of finely divided metal oxides, metal hydroxides and metals
JPS63195101A (en) * 1987-02-09 1988-08-12 Tosoh Corp Production of metallic oxide
US5417816A (en) * 1992-12-09 1995-05-23 Nikko Kyodo, Ltd. Process for preparation of indium oxide-tin oxide powder
WO2000014302A1 (en) * 1998-09-07 2000-03-16 Henkel Kommanditgesellschaft Auf Aktien Electrochemical production of amorphous or crystalline metal oxides with particle sizes in the nanometer range
WO2004031449A2 (en) * 2002-09-27 2004-04-15 Sustech Gmbh & Co. Kg Electrochemical method for controlling the particle size during the production of nanoparticulate metal oxides

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4067788A (en) * 1976-09-20 1978-01-10 Electromedia, Inc. Electrochemical production of finely divided metal oxides, metal hydroxides and metals
JPS63195101A (en) * 1987-02-09 1988-08-12 Tosoh Corp Production of metallic oxide
US5417816A (en) * 1992-12-09 1995-05-23 Nikko Kyodo, Ltd. Process for preparation of indium oxide-tin oxide powder
WO2000014302A1 (en) * 1998-09-07 2000-03-16 Henkel Kommanditgesellschaft Auf Aktien Electrochemical production of amorphous or crystalline metal oxides with particle sizes in the nanometer range
WO2004031449A2 (en) * 2002-09-27 2004-04-15 Sustech Gmbh & Co. Kg Electrochemical method for controlling the particle size during the production of nanoparticulate metal oxides

Also Published As

Publication number Publication date
DE102005044873A1 (en) 2007-03-29
WO2007033815A2 (en) 2007-03-29

Similar Documents

Publication Publication Date Title
Babar et al. Evolution of waste iron rust into magnetically separable g-C3N4–Fe2O3 photocatalyst: an efficient and economical waste management approach
Kumar et al. From lab to field: Prussian blue frameworks as sustainable cathode materials
Weng et al. Surfactant-free porous nano-Mn 3 O 4 as a recyclable Fenton-like reagent that can rapidly scavenge phenolics without H 2 O 2
CA3097307C (en) A method for the manufacture of graphene oxide and reduced graphene oxide from kish graphite
Itakura et al. Resource recovery from Nd–Fe–B sintered magnet by hydrothermal treatment
Lopez-Tejedor et al. Iron nanostructured catalysts: design and applications
Zhuang et al. Treatment of nanowaste via fast crystal growth: With recycling of nano-SnO2 from electroplating sludge as a study case
CA3057958C (en) A method for the manufacture of reduced graphene oxide from kish graphite
Sun et al. Chitosan modified Fe 0 nanowires in porous anodic alumina and their application for the removal of hexavalent chromium from water
WO2008099773A1 (en) Methods of recovering valuable metal from scrap containing electrically conductive oxide
Hong et al. A short review on electrochemically self-doped TiO2 nanotube arrays: Synthesis and applications
WO2008136818A3 (en) Suspensions of titanium (iv) oxide particles and process for their production
AU2002247658A1 (en) Electrochemical production of nanoscale metal (mixed) oxides
CN104307516A (en) Preparation method of three-dimensional graphene-tannic acid-nano gold composite material
CN106381492A (en) Method for preparing super-amphiphobic aluminum surface
Ramamoorthy et al. Effect of surfactants assisted Co3O4 nanoparticles and its structural, optical, magnetic and electrochemical properties
CN101642714A (en) Preparation method of core-shell Fe/Pd bimetallic nano-catalyst
US20140034514A1 (en) Electrolyte for removing metal-carbide/nitride coatings or metal-carbide-nitride coatings and removing method using same
WO2007033815A3 (en) Electrochemical method for producing nanoscalar metal compounds
CN105886781B (en) Method for recovering manganese dioxide from electrolytic manganese anode mud
CN103143368B (en) A kind of process chemical industrial organic wastewater Catalysts and its preparation method
Guo et al. Rapid remediation of Cd (II)-contaminated water using a magnetically collectable iron-based primary battery
Zhan et al. Template-free synthesis of alkaline earth vanadate nanomaterials from leaching solutions of oil refinery waste
JP5909125B2 (en) Method for producing metal particles using solvothermal reaction
Li et al. Recent developments of iron oxide-based photocatalysts in water treatment technology: a review

Legal Events

Date Code Title Description
121 Ep: the epo has been informed by wipo that ep was designated in this application
122 Ep: pct application non-entry in european phase

Ref document number: 06792149

Country of ref document: EP

Kind code of ref document: A2