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WO2007031876A3 - Templated carbon monolithic tubes with shaped micro-channels and method for making the same - Google Patents

Templated carbon monolithic tubes with shaped micro-channels and method for making the same Download PDF

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Publication number
WO2007031876A3
WO2007031876A3 PCT/IB2006/003344 IB2006003344W WO2007031876A3 WO 2007031876 A3 WO2007031876 A3 WO 2007031876A3 IB 2006003344 W IB2006003344 W IB 2006003344W WO 2007031876 A3 WO2007031876 A3 WO 2007031876A3
Authority
WO
WIPO (PCT)
Prior art keywords
channels
making
same
shaped micro
templated carbon
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/IB2006/003344
Other languages
French (fr)
Other versions
WO2007031876A2 (en
Inventor
Lixin Luke Xue
Shuzhong Zhuang
Liqun Yu
John B Paine Iii
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Philip Morris Products SA
Original Assignee
Philip Morris Products SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Philip Morris Products SA filed Critical Philip Morris Products SA
Priority to JP2008519019A priority Critical patent/JP5384107B2/en
Priority to KR1020087000162A priority patent/KR101334430B1/en
Priority to EP06831593A priority patent/EP1917210A2/en
Priority to EA200800166A priority patent/EA013275B1/en
Publication of WO2007031876A2 publication Critical patent/WO2007031876A2/en
Publication of WO2007031876A3 publication Critical patent/WO2007031876A3/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/16Use of materials for tobacco smoke filters of inorganic materials
    • A24D3/163Carbon
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/02Manufacture of tobacco smoke filters
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/04Tobacco smoke filters characterised by their shape or structure
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/04Tobacco smoke filters characterised by their shape or structure
    • A24D3/048Tobacco smoke filters characterised by their shape or structure containing additives
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/20Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising free carbon; comprising carbon obtained by carbonising processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28042Shaped bodies; Monolithic structures
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/305Addition of material, later completely removed, e.g. as result of heat treatment, leaching or washing, e.g. for forming pores
    • B01J20/3057Use of a templating or imprinting material ; filling pores of a substrate or matrix followed by the removal of the substrate or matrix
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30Processes for preparing, regenerating, or reactivating
    • B01J20/3078Thermal treatment, e.g. calcining or pyrolizing
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/05Preparation or purification of carbon not covered by groups C01B32/15, C01B32/20, C01B32/25, C01B32/30
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B32/00Carbon; Compounds thereof
    • C01B32/30Active carbon
    • C01B32/354After-treatment
    • C01B32/382Making shaped products, e.g. fibres, spheres, membranes or foam
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/515Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics
    • C04B35/52Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite
    • C04B35/524Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on non-oxide ceramics based on carbon, e.g. graphite obtained from polymer precursors, e.g. glass-like carbon material
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/622Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/626Preparing or treating the powders individually or as batches ; preparing or treating macroscopic reinforcing agents for ceramic products, e.g. fibres; mechanical aspects section B
    • C04B35/62605Treating the starting powders individually or as mixtures
    • C04B35/6269Curing of mixtures
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B38/00Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof
    • C04B38/0051Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof characterised by the pore size, pore shape or kind of porosity
    • C04B38/0054Porous mortars, concrete, artificial stone or ceramic ware; Preparation thereof characterised by the pore size, pore shape or kind of porosity the pores being microsized or nanosized
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2111/00Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
    • C04B2111/00474Uses not provided for elsewhere in C04B2111/00
    • C04B2111/00793Uses not provided for elsewhere in C04B2111/00 as filters or diaphragms
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/60Aspects relating to the preparation, properties or mechanical treatment of green bodies or pre-forms
    • C04B2235/602Making the green bodies or pre-forms by moulding
    • C04B2235/6028Shaping around a core which is removed later
    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/70Aspects relating to sintered or melt-casted ceramic products
    • C04B2235/94Products characterised by their shape

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Analytical Chemistry (AREA)
  • Structural Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Nanotechnology (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
  • Ceramic Products (AREA)
  • Inorganic Fibers (AREA)

Abstract

A method is disclosed for forming an article with template shaped channels 20 by (a) mixing a precursor 18 with a fibrous template 10, (b) forming the mixture into a pre-determined shape, (c) curing the mixture to form a precursor composite 19, (d) carbonizing the precursor composite, and (e) decomposing the fibrous template to yield a shaped carbon article 21 with template shaped channels 20.
PCT/IB2006/003344 2005-06-29 2006-06-26 Templated carbon monolithic tubes with shaped micro-channels and method for making the same Ceased WO2007031876A2 (en)

Priority Applications (4)

Application Number Priority Date Filing Date Title
JP2008519019A JP5384107B2 (en) 2005-06-29 2006-06-26 Template carbon monolithic tube with shaped microchannel and method of making it
KR1020087000162A KR101334430B1 (en) 2005-06-29 2006-06-26 Templated carbon monolithic tubes with shaped micro-channels and method for making the same
EP06831593A EP1917210A2 (en) 2005-06-29 2006-06-26 Templated carbon monolithic tubes with shaped micro-channels and method for making the same
EA200800166A EA013275B1 (en) 2005-06-29 2006-06-26 Template carbon monolithic tubes with shaped micro-channels and a method for making the same

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US11/170,272 US7767134B2 (en) 2005-06-29 2005-06-29 Templated carbon monolithic tubes with shaped micro-channels and method for making the same
US11/170,272 2005-06-29

Publications (2)

Publication Number Publication Date
WO2007031876A2 WO2007031876A2 (en) 2007-03-22
WO2007031876A3 true WO2007031876A3 (en) 2007-07-26

Family

ID=37588046

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/IB2006/003344 Ceased WO2007031876A2 (en) 2005-06-29 2006-06-26 Templated carbon monolithic tubes with shaped micro-channels and method for making the same

Country Status (7)

Country Link
US (2) US7767134B2 (en)
EP (1) EP1917210A2 (en)
JP (1) JP5384107B2 (en)
KR (1) KR101334430B1 (en)
EA (1) EA013275B1 (en)
UA (1) UA94585C2 (en)
WO (1) WO2007031876A2 (en)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB0019417D0 (en) * 2000-08-09 2000-09-27 Mat & Separations Tech Int Ltd Mesoporous carbons
US8591855B2 (en) * 2000-08-09 2013-11-26 British American Tobacco (Investments) Limited Porous carbons
GB0506278D0 (en) 2005-03-29 2005-05-04 British American Tobacco Co Porous carbon materials and smoking articles and smoke filters therefor incorporating such materials
EP2170110A2 (en) * 2007-08-01 2010-04-07 Philip Morris Products S.A. Degradable cigarette filters
FR2957276A1 (en) * 2010-03-15 2011-09-16 Francois Parmentier MULTICAPILLARY MONOLITH
DE102011050769A1 (en) * 2011-05-31 2012-12-06 Sven Pracht Filter element and filter for tobacco products and a method for producing the filter element
GB201109419D0 (en) 2011-06-06 2011-07-20 British American Tobacco Co Filter for a smoking article
GB201407642D0 (en) 2014-04-30 2014-06-11 British American Tobacco Co Aerosol-cooling element and arrangements for apparatus for heating a smokable material
FR3024432B1 (en) * 2014-08-01 2018-02-02 Epsilon Composite HYBRID TYPE STRUCTURE TUBE, IN PARTICULAR FOR AERONAUTICAL SEAT
GB201418817D0 (en) 2014-10-22 2014-12-03 British American Tobacco Co Apparatus and method for generating an inhalable medium, and a cartridge for use therewith
GB201503411D0 (en) 2015-02-27 2015-04-15 British American Tobacco Co Apparatus and method for generating an inhalable medium, and a cartridge for use therewith
CN107529830B (en) 2015-02-27 2021-06-29 尼科创业贸易有限公司 Cartridges, components, and methods for generating inhalable media
EP3081292A1 (en) * 2015-04-15 2016-10-19 Air Products And Chemicals, Inc. Perforated adsorbent particles
US9579628B2 (en) 2015-04-15 2017-02-28 Air Products And Chemicals, Inc. Perforated adsorbent particles
GB201517471D0 (en) 2015-10-02 2015-11-18 British American Tobacco Co Apparatus for generating an inhalable medium
GB201608928D0 (en) 2016-05-20 2016-07-06 British American Tobacco Co Article for use in apparatus for heating smokable material
GB201618481D0 (en) 2016-11-02 2016-12-14 British American Tobacco Investments Ltd Aerosol provision article
GB201812373D0 (en) 2018-07-30 2018-09-12 Nicoventures Trading Ltd Generation of an inhalable medium

Citations (4)

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Publication number Priority date Publication date Assignee Title
WO1995028279A1 (en) * 1994-04-15 1995-10-26 Corning Incorporated Activated carbon honeycombs having varying adsorption capacities and method of making same
US5820967A (en) * 1995-02-27 1998-10-13 Corning Incorporated Extruded structures from thermosetting resins
US5972253A (en) * 1996-09-30 1999-10-26 University Of Kentucky Research Foundation Preparation of monolithic carbon fiber composite material
WO2003086116A1 (en) * 2002-04-12 2003-10-23 Philip Morris Products, S.A. Activated carbon fiber cigarette filter

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US2881770A (en) 1954-05-27 1959-04-14 Eastman Kodak Co Fibrous tobacco smoke filters
US3101723A (en) 1960-11-15 1963-08-27 Philip Morris Inc Fibrous cigarette filter
US3353543A (en) 1964-12-02 1967-11-21 American Filtrona Corp Smoke filter
GB2020158B (en) 1978-04-21 1982-11-24 Cigarette Components Ltd Production of tobacco smoke filters
US4481958A (en) 1981-08-25 1984-11-13 Philip Morris Incorporated Combustible carbon filter and smoking product
GB8617831D0 (en) 1986-07-22 1986-08-28 British Petroleum Co Plc Production of porous shaped articles
US5057368A (en) 1989-12-21 1991-10-15 Allied-Signal Filaments having trilobal or quadrilobal cross-sections
US5510063A (en) * 1994-04-15 1996-04-23 Corning Incorporated Method of making activated carbon honeycombs having varying adsorption capacities
US5891221A (en) * 1994-12-23 1999-04-06 Alliedsignal Inc. Chemical reagent package and method of operation effective at removing a wide range of odors
US5947126A (en) * 1997-05-29 1999-09-07 Eastman Chemical Co. Environmentally disintegratable tobacco smoke filter rod
MY128157A (en) 2000-04-20 2007-01-31 Philip Morris Prod High efficiency cigarette filters having shaped micro cavity fibers impregnated with adsorbent or absorbent materials
MY138902A (en) 2000-04-20 2009-08-28 Philip Morris Prod "cigarette filters of shaped micro cavity fibers impregnated with flavorant materials"
US6857431B2 (en) * 2002-12-09 2005-02-22 Philip Morris Usa Inc. Nanocomposite copper-ceria catalysts for low temperature or near-ambient temperature catalysis and methods for making such catalysts
US6814786B1 (en) * 2003-04-02 2004-11-09 Philip Morris Usa Inc. Filters including segmented monolithic sorbent for gas-phase filtration

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1995028279A1 (en) * 1994-04-15 1995-10-26 Corning Incorporated Activated carbon honeycombs having varying adsorption capacities and method of making same
US5820967A (en) * 1995-02-27 1998-10-13 Corning Incorporated Extruded structures from thermosetting resins
US5972253A (en) * 1996-09-30 1999-10-26 University Of Kentucky Research Foundation Preparation of monolithic carbon fiber composite material
WO2003086116A1 (en) * 2002-04-12 2003-10-23 Philip Morris Products, S.A. Activated carbon fiber cigarette filter

Also Published As

Publication number Publication date
EA200800166A1 (en) 2008-04-28
JP2008544938A (en) 2008-12-11
US7767134B2 (en) 2010-08-03
WO2007031876A2 (en) 2007-03-22
JP5384107B2 (en) 2014-01-08
KR101334430B1 (en) 2013-11-29
EP1917210A2 (en) 2008-05-07
KR20080022177A (en) 2008-03-10
US20100163064A1 (en) 2010-07-01
UA94585C2 (en) 2011-05-25
US20070000508A1 (en) 2007-01-04
EA013275B1 (en) 2010-04-30

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