WO2007003283A1 - Sample container, more particularly milk sample bottle, and method for taking a sample, more particularly for taking a milk sample - Google Patents

Abstract

The invention relates to a sample container, more particularly a milk sample bottle, and to a method for taking a sample, more particularly for taking a milk sample, the sample container having a relatively simple design and being inexpensive to produce and yet being exceptionally well-protected against tampering. The sample container has a sealing cap which from fabrication to the analysis stage is held in a sealed closing position and is additionally secured by a securing cap. The securing cap is held in a first locked position corresponding to an empty transporting position or operational position and in a second locking position corresponding to a securing position on the sealing cap and, to allow the taking of a sample, can be opened from the empty transporting position or operational position and brought into the securing position.

Description

Sample container, in particular milk sample bottle, and method for sampling, in particular for milk sampling

The invention relates to a sample container, in particular a milk sample bottle, according to the preamble of claim 1 and a method for sampling, in particular for milk sampling, according to the preamble of claim 26.

More particularly, the invention relates to a tamper-proof sample container and a method of sampling which assure the integrity and assignment of the sample throughout the process of sampling and analysis.

It is known to use containers for materials, e.g. be taken by people or their composition may not be distorted to provide with tamper-resistant caps. The caps are designed so that any unwanted opening before the actual use is recognizable. The known from DE 34 22 547 C2 tamper-resistant cap, which has a pivotally mounted plug with an edge flange for closing an opening is clamped with a closure edge on the container neck of the container and kept substantially non-removable. An inadmissible opening is recognizable.

In DE 202 07 423 Ul a hinged lid closure with tamper-evident for flowable materials is described, which consists of a closure body and a hinged lid and with the closure body can be screwed onto the neck of a container. The hinged lid is connected to the closure body via a film hinge.

From DE 94 18 060 Ul a screwed onto a sample tube end cap made of plastic is known, which is particularly intended for capillary blood withdrawals. The end cap, which has a lead-through opening for a capillary tube and a sealing plug for the sample tube, is provided with a flexible retaining loop as a loss-prevention, which can be applied to the neck of the sample tube detent. The sealing plug and the retaining loop are connected in one piece to the end cap via flexible flat webs.

The known from DE 69 39 265 Ul container closure with a tubular body and a hinged lid part is provided for visualizing an unauthorized opening of the container provided with the container closure with a ring which is connected via a flexible securing strip with predetermined breaking point with the lid part. This ring is held in an annular undercut of the body and the lid can only be opened when the securing strip is broken.

The tubular base body and the container neck are designed such that removal of the base body onto the container is no longer possible.

DE 693 22 515 T2 discloses a test tube for liquids, in particular for blood samples, which has a sealing cap and a locking cap for a friction fit. Test tube and retaining caps can be made in one piece and with flexible hinges and opposite each other be connected to a container edge. The locking cap is folded into the sealing cap placed in the sealing cap, and a detachment of the flap closure can only be done by destroying one of the hinges. Access to the sample material is possible via syringe channels in the sealing cap and in the arresting cap. Both caps also have flanges which extend over the container circumference and in principle allow opening of the container.

From US 5 012 941 A, a sample container is known, which is designed as a molded plastic bottle with a connected lid. The integrity of the contents of the bottle is to be achieved by a closure band formed on the container which is provided with teeth for one-way insertion through aligned openings of a lid and container flange. An opening of the lid leads to a destruction of the closure band, whereby an unauthorized access to the container interior or the sample is visible. Also for the sample analysis, the sealing tape must be destroyed.

With this known sample container, contamination up to sampling can be avoided unless the sealing tape seal has been destroyed. However, contamination is possible immediately before or after sampling because the bottle is no longer sealed. For example, the sampler can touch the container or the lid inside.

If the known sample container is sealed only after sampling with the aid of the sealing tape, contamination may already have taken place until the sample has been taken.

A sample container described in US Pat. No. 5,133,470 A has two destructible means for preventing forgery Tamper protection of a container lid assembly to increase. Containers and lids are commonly made and joined by a first destructible compound formed in the manufacturing process as a result of controlled shrinkage during the cooling phase. The first destructible connection is an arrow-shaped formation on the container, which engages behind a slot in a cover flange when closing the container with the lid. To fill the container, however, the lid must be opened, whereby the first connection or the first seal is destroyed. After filling, a re-sealing of the sample container by means of a disposable tape, which is additionally attached to the bottle or on the lid and is guided by aligned openings on the container and cover flange in a one-way direction.

Neither the first nor the second destructible connection between lid and sample container can ensure the necessary manipulation protection. The arrow-like first connector can be manipulated by squeezing the arrow and then inserting it back into the slot to open the lid. In addition, the bottle contents or the container receiving space is accessible during sampling, so that it can lead to contamination.

WO 02/21425 A2 describes a method for sampling and a sample container with a sealable and hermetically sealed cover and an RFID (Radio Frequency Identification) TAG. The TAG is located on the sample container and can only be removed and reused with destruction of at least one destructible.

For tamper-proof design of the sample container and arrangement of the TAG no further versions are included. In the German patent application DE 10 2004 043 883.8, a sample bottle, which is particularly suitable for milk samples and has a high security against manipulation, has been proposed. The milk sample bottle has first and second lids, each having a through-hole for filling a milk sample. The second cover is at least partially adjustable on the first cover, in particular displaceable and / or rotatable, so that the passage openings can be brought into a filling position. A further adjustment leads to an offset arrangement of the passage openings and thus to a tamper-proof closure of the sample container. A locking device ensures that the second lid can not be accidentally moved into the filling position.

The proposed sample container is extremely tamper-proof and easy to handle. Due to the displaceable or rotatable parts in the second cover, however, the production costs for this sample container are relatively high.

The invention is based on the invention to provide a sample container and a method for sampling, in particular for use in the dairy industry, which allow a high security against manipulation during the entire sampling with a relatively simple construction and cost-effective production of the sample container.

According to the invention the object with respect to the sample container by the features of claim 1 and in relation to the method for sampling by the features of claim 26 is achieved. Advantageous and expedient embodiments are contained in the respective subclaims and in the description of the figures. The invention is based on a sample container with a first lid and a second lid, which are produced together with the container. The sample container with the two integrated lids consists of a single piece. Additional tools and machine run times for a separately manufacturable lid eliminated, which leads to a reduction in manufacturing costs.

The sample container, which has as a first lid a closure lid with a filling opening for filling a sample, wherein the closure lid can be formed as a hinged lid and still folded during the manufacturing process on the container opening, so that an integrated one-way closure device operated as tamper protection and the sample container is sealed , as well as having a further lid, which, like the first closure lid, is designed as a hinged lid and can be produced with the container and the closure lid, is provided according to the invention for increasing the manipulation protection with a securing lid as the second lid.

According to the invention the closure lid is cap-shaped and has an inner pot with a lid base and a lid side wall, wherein the lid side wall is provided on the outside with a latching step, on which the fuse cover, which is cap-like and complementary to the inner pot of the closure lid, in a first detent position for a Empty transport or operating position is held. In the first detent position or empty transport or operating position of the fuse cover is arranged according to the invention with protrusion in the inner pot of the closure lid and can be pressed into a second detent position, which represents a securing position, further into the inner drip, so that the fuse cover flush or with Shelter is received in the inner pot of the closure lid.

It is advantageous that the securing cover, such as the closure lid, can be connected to the container by means of a connecting band or to the closure lid via a connecting band. The other connection band may be formed as a film hinge like the first connecting band between the closure lid and the container and allow a folding of the fuse cover from a manufacturing or open position into an operating position and subsequent securing position.

Under operating position, the sample container is to be understood in the delivery state, in which the closure lid is folded under cover of the container opening and sealed. In addition, the fuse cover is folded onto the closure lid and held in the first detent position, which is the transport position to sampling.

It is advantageous that in this first detent position of the fuse cover can be easily opened, the sample container, however, at the same time formed compact and completely secured against contamination, since an opening of the cap is not required even when sampling.

It is advantageous that the cap-like closure lid is designed to be complementary to the container opening and to the lid-side container rim and has an annular groove between an inner pot and an overlapping lid edge. The inner pot is formed by a horizontal lid base and a vertical lid side wall and protrudes into the container. The filling or injection opening is formed centrally in the lid base and coaxial with a lid side wall and provided with a membrane with a predetermined breaking point.

On the outside, the lid side wall is provided with the latching step, which holds the folded-over securing cover in the first latching position, namely in the empty transport or operating position. From this first detent position of the fuse cover can be easily reopened, whereby the injection port of the closure cap is accessible without affecting the sterility of the closed with the closure cap receiving space of the sample container.

Conveniently, the cap-like fuse cover is complementary to the closure lid and has a horizontal cover and a circumferential, vertical side wall. In operating position, i. in the first detent position and also when fully pressing the fuse cover into the inner pot of the closure lid, the side wall of the fuse cover is located on the lid side wall of the closure lid, and an inside sleeve which surrounds an injection opening of the fuse cover is in the operating position coaxial with the sleeve-like injection opening of the closure lid and arranged around them.

After sampling, the safety cover can be completely pressed into the cap or in its inner pot. It is advantageous that the inner sides of the fuse cover are not touched, since a pressure on the outside cover sufficient. It is also advantageous locking elements on the adjacent walls and / or sleeves the closure lid and the fuse cover, which act as locking means and prevent removal of the fuse cover from the closure lid or opening. This further increases the integrity of the sample in the sample container.

It may be expedient to provide a mechanical closing device which presses the securing cover in the closure lid in the securing position, that is, in the transport position after sampling.

Due to the complementary design of the fuse cover this is added in the depressed position without any protrusion and possibly under it in the inner pot of the closure cap. Opening the fuse cover without a tool is not possible. Since in this position, the injection opening of the closure lid is completely surrounded by the injection sleeve of the fuse cover and the fuse cover has no opening to the outside, the sample container is still tightly sealed and fully transportable. Shaking, tilting or throwing can not affect the integrity of the sample in the sample container.

A second injection opening can be provided centrally in the securing cover and, in particular, can be designed as a material dilution. This injection opening of the safety cover makes it possible to inject substances into the examination laboratory without having to open the entire sample bottle or the sample container.

Conveniently, this injection port can be visually inspected for any damage, similar to a possible visual inspection of the one-way closure device of the cap on the container. The closure device or the seal are first broken in the analysis laboratory so that the closure lid can be opened together with the safety cover accommodated in the closure lid.

Expediently, an RFID tag is arranged reusable on the sample container, for example in the bottom region of the container or else in the closure lid. The tag can be fixed in the bottom area simply by snapping it on and can be broken out again by means of a tool which acts on recesses in the container. It is also possible to fix a TAG when spraying the sample container.

The arrangement of a TAG in the cap results in a saving of height and material. Advantageously, the TAG provided for the closure lid is provided with a central hole and can be snapped onto the filling sleeve of the injection opening of the closure lid.

The connection of the securing cover can advantageously be arranged on the closure lid, for example between the closure opening for the one-way closure device and the flexible container-side connecting band.

It is also possible to mold the securing cover or its connecting band in the region of the container flap with the closure opening of the disposable closure device on the closure lid. It is also advantageous to form a gripping tab on the security cover, for example with respect to the connecting band to the closure lid or to the container. The fuse cover can then be opened more easily. Conveniently, the grip tab can be used analogously to the connection be provided with a predetermined breaking point, preferably in the region of the lid edge.

A further increase in the protection against tampering is achieved if the grip tab can be positively received and countersunk in the closure lid after sampling and in the sealed arrangement of the fuse cover in the second detent position.

The sample container is expediently arranged for sampling in a receiving device. After releasing the fuse cover from the first detent position or operating position into an open position, rotation of the receptacle and locking takes place and then lifting of the sample container or lowering of the filling device with injection cannula in the filling tube, wherein a membrane ruptures at a predetermined breaking point. After filling the sample, the locking position is released, the fuse cover completely pressed into the inner pot of the cap and then removed the sample bottle or the sample container and arrives, usually in a transport magazine to the examination laboratory.

The sample container according to the invention is characterized by a relatively simple construction and an extremely efficient and cost-effective production. In that the sample container is provided with a first lid, which is a permanently closed closure lid for the container from manufacture, and with a second lid as a safety lid for the closure lid, which in a first latching position for an operating or empty transport position and after sampling in one second detent position can be arranged for a backup position, there is the possibility of a tamper-proof closure of the container interior already in the manufacturing process and also in the subsequent process stages of a sampling and analysis. The sterile interior or receiving space of the container is accessible without removing the cap only during sampling and only for the sample and is covered immediately after filling by the fuse cover again forgery-proof. A manipulation, for example in the area of material thinning of the safety cover, would be visible or identifiable. After sampling, the fuse cover can only be removed together with the cap.

Another advantage is the protected arrangement of a TAG in the region of the double cover or in the bottom-side container area, such that the TAG is reusable.

According to the method, when sampling, in particular during milk sampling, provision is made for a container which is produced in one piece with an integrated closure lid, an integrated safety lid and an integrated one-way closure device made of a plastic material and whose closure lid is folded onto the container during the production process and brought into a closed position and thereby sealed by means of the one-way closure device is additionally secured with the fuse cover by this is folded before delivery in a first detent position on or in the closure lid and placed in an empty transport or operating position. In this empty transport or operating position, the sample container is transported to a sampling device and set in a receiving device. For sampling the fuse cover is brought without tools from the empty transport or operating position in an open position, whereby an injection port in the cap is accessible. The milk sample is then injected through the injection port into the container. ter filled, and after filling the fuse cover is pressed into the closure lid until the fuse cover is in a second detent position, which represents a securing position for the container and the container closure. In this safety position, the safety cover is completely received in the closure cap, and the container with the milk sample can be transported in the tamper-proof securing position. For analysis, the cap is opened together with the fuse cover received therein.

The invention will be further explained below with reference to a drawing; in this show in a highly schematic representation

1 shows a perspective view of a sample container according to the invention in a production or open position;

2 is a perspective view of the sample container according to the invention with closed and sealed cap and open safety cover,

3 shows a perspective view of the sample container according to the invention with closed and sealed closure lid and a safety lid closed in the operating position;

4 shows a perspective view of the sample container according to the invention with closed and sealed closure lid and securing lid closed in the securing position; 5 shows a view of the sample container according to the invention according to FIGS. 1 to 4;

Fig. 6 is a longitudinal section along the line VI-VI in Fig. 5;

Fig. 7 is a plan view according to arrow VII in Fig. 6;

8 shows a perspective view with a view of the bottom region of the sample container according to the invention;

9 shows a cover-side section of a sample container according to the invention with alternatively arranged TAG;

Fig. 10 u.

11 is an enlarged longitudinal section in the region of the filling opening of a sample container according to the invention during sampling and

12 shows an enlarged longitudinal section through a lid-side region of a sample container with closed and sealed closure lid and with a safety cover during the closing process.

1 to 8 show a sample container 2, which is designed to be counterfeit-proof and is provided on the bottom side with an electromagnetically readable identification device, a so-called RFID tag 9 (see FIGS. 6 and I) ₁ .

For identical features, identical reference numerals are used in all drawing figures.

The sample container 2 is provided with a closure lid 5 arranged as the first lid and with a safety cover 7 securable to the closure lid 5. Fig. 1 shows a possible connection of the closure lid 5 to the container 3 and the fuse cover 7 on the closure lid 5. Container 3, closure lid 5 and fuse cover 7 are integrally formed and can be manufactured in a manufacturing process. Advantageously, a sample container 2 made of a plastic, which can be manufactured in an injection molding machine.

The closure lid 5, which is connected by means of a connecting band 6 to the container 3, and the fuse cover 7, which is connected in this embodiment via a further connecting band 8 with the closure lid 5, are cap-like, but opposite to each other, formed. The closure lid 5 is complementary to a container opening 4 and to a container edge region 14 of the container 3 and extends with an inner pot 24, which has a horizontal lid base 25 and a vertical lid side wall 26, in a closed position 23 in the container opening 4 inside. The closure position 23 of the closure lid 5 shown in FIG. 2 is still reached during the manufacturing process in order to effect a sealing of the still soft plastic material with the aid of a disposable closure device.

The one-way closure device 10, which is also apparent from FIG. 6 and the enlarged sectional view of FIG. 12, consists of a mushroom-shaped punch 11 with a predetermined breaking point 12 on a lug 16 of a radially projecting container flange 15 and a closure position of the closure lid 5 with the punch 11 aligned closure opening 22 which is formed in a cover flap 21 on an outer lid edge 28 of the closure lid 5. The one-way closure device 10 serves to protect the sample container 2 from tampering by indicating unauthorized opening and associated possible contamination of the container interior or the sample. The punch 11 with predetermined breaking point 12 is formed such that the predetermined breaking point 12 the pressure during penetration of the punch 11 by the aligned and tapered closure opening 22 when folding the closure lid 5 holds on the container opening 4, but tears when opening the closure lid 7. It is therefore intended to leave the sample container 2 according to the invention from the manufacturing process to the analysis laboratory in the sealed closure position 23 (FIG. 2) of the closure lid 5 and additionally cover it with the safety lid 7. The fuse cover 7 is opened only for sampling and immediately after sampling in a securing position on the cap 5 folded.

The disposable closure device 10 is arranged opposite the connecting band 6, which, like the connecting band 8, has a film-hinge-like design. The container edge region 14, which surrounds the container opening 4, is formed bead-like (see also Figs. 6, 9 and 12) and is in the closed position of the closure lid 5 in an annular groove 29 of the closure lid 5, which between the inner pot 24 and the outer lid edge 28th is formed, sealingly received.

A filling or injection opening 20 is arranged centrally in the lid base 25 of the inner pot 24 of the closure lid 5 and is sleeve-shaped, so that a cannula 43 (see FIGS. 10 and 11) of a sampling device (not shown) can reach the region of the filling opening 20 , The sterile sample container 2 is delivered with closed fuse cover 7. Fig. 3 shows the delivery state in which the fuse cover 7 is folded in a first detent position or empty transport position 33 on the closure lid 5. The securing cover 7 has a cover 31, in which a material dilution is formed centrally as an injection opening 30. On the horizontal cover 31, the further connecting band 8, which is provided at the edge with a predetermined breaking point 38, and a gripping tab 39 are formed, which is shown for reasons of clarity only in Fig. 3. In the first detent position or operating position 33 of FIG. 3, in which the fuse cover 7 is held by the latching step 27 on the inner pot 24 and on the outer lid side wall 26 of the closure lid 5, the fuse cover 7 is above the cap 5 and can be tool-free be opened.

For sampling, the securing cover 7 is opened from the empty transport position or first detent position 33 of FIG. 3, so that the filling or injection opening 20 of the closure lid 5, as shown in FIG. 2, is accessible. The sample container 2 is placed and locked in a receiving device (not shown) for sampling. By lowering the injection cannula 43 (see FIGS. 10 and 11) or lifting the sample container 2 or the receiving device, the injection cannula 43 passes into the sleeve-like filling opening 20 and penetrates a membrane 41. If the membrane 41 has a predetermined breaking point 42 and a hinge 47 11, the injection port 20 is released in the manner shown in FIG. 11 and the sample can be filled into the inner space 35 of the sterile sample container 2. It is advantageous that the injection cannula 43 can be inserted relatively deep. Since the container opening 4 or the interior 35 of the container 3 is connected directly to the closure lid 5 with the lid base 25, the risk of contamination, for example due to sample liquid spraying around, is substantially lower.

After filling the sample, the sample container 2 is removed by rotation about its longitudinal axis from the receiving or holding device. The detent positions of the sample container 2 in the holding or receiving device can be designed ergonomically by a tactile resistance, for example a latchable spring mechanism (not shown).

After removal of the sample container 2, a further securing of the sample takes place in the container interior 35 by the securing cover 7 being pressed onto the first closure lid 5 into a second detent position or a securing position 34 (see FIG. 4).

In this securing position 34 closes the cover 31 of the fuse cover 7 flush with the closure lid 5 and the cover edge 28 from or has a shelter, so that opening the fuse cover 7 without tools and without visible destruction is not possible.

The impressions of the securing cover 7 in the closure lid 5 can be made by sliding over the outside of the cover 31. A touch of the inner surface and a concomitant risk of contamination are excluded. Instead of pushing in by hand, a mechanical closing device for pressing in the securing cover 7 into the closure lid 5 and into the securing position 34 may also be provided. Fig. 5 shows a side view of the sample container 2. The flush and up to the connecting band 8 substantially complete recording of the fuse cover 7 in the cap 5 is clearly visible.

FIG. 6 also shows the predetermined breaking point 12 of the one-way closure device 10 of the closure lid 5, the abutment of the lid side wall 26 of the inner pot 24 of the closure lid 5 on the side wall 36 of the fuse cover 7 and also the second detent position of the fuse cover 7, which end on the side wall 36 has a Abdichtwulst 44. The injection port 20 is sealed and the sample container 2 is transportable.

Fig. 6 also illustrates a first alternative of a TAG attachment in the bottom region of the container 3. For this purpose, the container 3 is extended beyond a container bottom 19 out and provided with bottom-side support members 17, which are designed as a snap mechanism for holding the TAG 9 , In order to be able to remove the TAG 9 from the recyclable sample container 2 after the laboratory examination and to be able to use it again, bottom-side recesses 18 (see also FIGS. 1 to 4 and FIG. 8) are formed, through which a tool for removing the TAG 9 can be inserted ,

A bottom-side container configuration for arranging a reusable TAG is also shown in FIG. 8. The perspective view shows the holder of the TAG 9 with the aid of the bottom-side holding elements 17 and the arrangement of the bottom-side recesses 18 in the wall of the container 3. In this illustration, the area-larger design of the Cover flap 21 in comparison to the container flap 16 and the opposite arrangement of the hinge-like connecting band 6 recognizable. In the area between the cover tab 21 and the connecting band 6, the further connecting band 8 for the connection of the securing cover 7 on the closure lid 5 can be seen.

Fig. 9 shows in an alternative embodiment, the arrangement of a TAG 9 in the region of the double-lid closure 5, 7, here in the inner pot 24 and on the lid base 25 of the closure lid 5 resting. For receiving in the sleeve-shaped injection opening 20 of the closure lid 5 of the TAG 9 is provided with a complementary central opening and can be snapped onto the sleeve-shaped injection port 20 or snapped. The advantage of the arrangement of the TAG 9 according to FIG. 9 is a saving of material, since the bottom extension of the container 3 according to FIGS. 1 to 8 can be dispensed with. In addition, the sample container 3 has a lower height, which may have an advantageous effect on handling and transport.

An enlarged view of the almost pressed onto the closure lid 5 fuse cover 7 is shown in Fig. 12. The connection of the securing cover 7 takes place in this embodiment variant in the region of the cover lug 21 with the closure opening 22 formed therein. The flexible connecting band 8 extends here as far as the cover 31 and is provided with a predetermined breaking point 38.

FIG. 12 shows, in particular, further sealing and blocking elements which, in addition to a first detent position up to sampling, serve in particular for sealing and stably holding or locking the securing cover 7 on the closure lid 5 after sampling. So are outside Tig at the sleeve-shaped filling opening 20 and on the lid side wall 26 of the closure lid 5 locking elements 45 are formed. At the same time 7 opposing locking elements 46 are provided on the side wall 36 of the fuse cover, which effectively prevent loosening of the fuse cover 7 from the cap 5. The material dilution 30, which is formed centrally in the fuse cover 7, serves to be able to inject substances into the examination laboratory without opening the entire sample container 2. For secure manipulation protection, it is expedient to visually inspect the material dilution 30 for damage in order to ensure that the sample container 2 and the sample are intact. A visual check can be carried out analogously for the one-way closure device 10 and the associated sealing of the closed container 3.

Claims

PATENT CLAIMS A sample container, in particular a milk sample bottle, with a container (3) for receiving a sample, an integrated closure lid (5) as a first lid, which has an injection opening (20) for filling a sample, an integrated one-way closure device (10), which on Closure cover (5) and container (3) is designed as tamper protection, and with a fuse cover (7), which as a second lid with the container (3) and the closure lid (5) producible, with the container (3) or the closure lid ( 5) connected and under cover of the injection opening (20) on the closure lid (5) is hinged, characterized in that the closure lid (5) is cap-like and an inner pot (24) having a lid base (25) and a lid side wall (26) characterized in that the lid side wall (26), which rests in a sealed closure position (23) on the inside of a container edge region (14), außense it is provided with a latching step (27) and that the securing cover (7), which is cap-shaped and complementary to the inner pot (24) of the closure lid (5), for a Leetransport- or operating position (33) in a first detent position the latching step (27) held and in the inner pot (24) of the closure ceiling (5) is arranged with projection and for a securing position (34) in a second detent position further pressed into the inner pot (24) and is received flush or with shelter in the inner pot (24). 2. Sample container according to claim 1, characterized in that the closure lid (5) by means of a connecting band (6) connected to the container (3) and still during manufacture from an open position (13) by means of the one-way closure device (10) in a Counterfeit-proof, sealed closure position (23) is adjustable. 3. Sample container according to claim 1 or 2, characterized in that the securing cover (7) by means of a further connecting band (8) with the container (3) or the closure lid (5) and from a production or open position (13) in the empty transport or operating position (33) can be folded onto or into the closure lid and can be brought further into a securing position (34) after sampling. 4. Sample container according to one of the preceding claims, characterized in that the closure lid (5) complementary to the container opening (4) and the container edge region (14) is formed and an annular groove (29) between the inner pot (24) and an outer lid edge (28 ) having. 5. Sample container according to one of the preceding claims, characterized in that the injection opening (20) of the closure lid (5) is formed centrally in the lid base surface (25). 6. Sample container according to one of the preceding claims, characterized in that the injection opening (20) is sleeve-like and coaxial with the vertical lid side wall (26) and provided with a membrane (41) with predetermined breaking point (42). 7. Sample container according to one of the preceding claims, characterized in that the one-way closure device (10) having a punch (11) with predetermined breaking point (12) on the container (3) and a closure opening (22) on the closure lid (5) with the container (3) covered by the closure lid (5) is permanently sealed during production and until sample analysis. 8. Sample container according to one of the preceding claims, characterized in that the one-way closure device (10) has a mushroom-shaped punch (11) on a lug (16) of the container (3) and an upwardly tapering closure opening (22) on a Cover flap (21) of the closure lid (5). 9. Sample container according to one of the preceding claims, characterized in that the tab (16) with the punch (11) of the disposable closure device (10) on a container flange (15) and with respect to the connecting band (6) which the container (3) the closure cover (5) connects, is arranged, and that the predetermined breaking point (12), which the pressure upon penetration of the punch (11) through the aligned closure opening (22) when folding the closure lid (5) on the container opening (4) withstands, when opening the closure lid (5) but breaks, at the transition between the punch (11) and the Container flange (15) is formed. 10. Sample container according to one of the preceding claims, characterized in that the connecting band (6) between the container (3) and the closure lid (5) formed like a film hinge and integrally formed on the container flange (15) and the lid edge (28). 11. Sample container according to one of the preceding claims, characterized in that the securing cover (7), which, like the closure lid (5) but in the shape of a cap, has a horizontal cover (31) and a circumferential vertical side wall (36). 12. Sample container according to one of the preceding claims, characterized in that the securing cover (7) in the first latching position and operating position (33) and in the second latching position and securing position (34) with the side wall (36) on the outside of the lid side wall (26 ) of the closure lid (5). 13. A sample container according to one of the preceding claims, characterized in that the fuse cover (7) for sampling to open and from the on the latching step (27) of the closure lid (5) hold operating position (33) up or down bar and after sampling further in the closure lid (5) pressed and in the securing position (34) can be brought. 14. Sample container according to one of the preceding claims, characterized in that the securing cover (7) has an injection opening (30) which is formed centrally in the cover (31) and in operating and securing position (33, 34) with the injection opening (20 ) of the closure lid (5) is arranged in alignment. 15. Sample container according to one of the preceding claims, characterized in that the securing cover (7) as injection opening (30) has a material dilution in the cover (31) and an inside sleeve (32) for grasping the sleeve-like injection opening (20) of the closure lid (20). 5) is formed. 16. Sample container according to one of the preceding claims, characterized in that the securing cover (7) in the closure lid (5) by pressing on the outside of the cover (31) by hand or by means of a locking device can be pressed. 17. Sample container according to one of the preceding claims, characterized in that it is fully transportable in the securing position of the safety cover (7) and the safety cover (7) only with a tool or together with the cover (5) destroying the Einwegverschlusseinrich- tion (10) is removable or open. 18. Sample container according to one of the preceding claims, characterized in that the securing cover (7) has a predetermined breaking point (38) in the region of the connecting band (8) which holds the securing lid (7) with the closure lid (5) or with the container (3). connects, has. 19. Sample container according to one of the preceding claims, characterized in that the securing cover (7) with the closure lid (5) by an edge on the cover (31) of the fuse cover (7) and on the cover flap (21) of the closure lid (5) molded connecting band (8) or with the container (3) by a with the tab (16) connected to the connecting band is connected. 20. Sample container according to one of the preceding claims, characterized in that the securing cover (7) by a connecting band (8) with the closure lid (5) is connected, which at the edge of the cover (31) of the fuse cover (7) and on the closure lid (5) is arranged in the region between the cover flap (21) and the container-side connecting band (6). 21. Sample container according to one of the preceding claims, characterized in that the closure lid (5) and the securing cover (7) in the region of the side walls (26, 36) and / or the sleeve-shaped injection openings (20, 30, 32) with locking elements (45, 46) are provided, which allow only a destructive removal of the fuse cover (7) from the closure lid (5). 22. A sample container according to one of the preceding claims, characterized in that a TAG (9), in particular an RFID tag, reusable on or below the container bottom (19) or in the closure lid (5) is arranged. 23. A sample container according to claim 22, characterized in that the TAG (9) is arranged during the production of the container (3) or can be fixed after its production. 24. Sample container according to claim 23, characterized in that for fixing the TAG (9), bottom-side holding elements (17) and for removing the TAG (9), bottom-side recesses (18) are formed in the container (3). 25. Sample container according to claim 22, characterized in that the TAG (9) is provided with a centric bore corresponding to the sleeve-shaped injection opening (20) of the closure lid (5) and is arranged in the inner pot (24) of the closure cap (5). 26. Method for sampling, in particular for milk sampling, with the aid of a sample container, in particular according to one of claims 1 to 25, characterized in that a container (3) which is integral with an integrated closure lid (5), an integrated safety lid ( 7) and with an integrated one-way closure device (10) made of a plastic material is produced and the closure lid (5) still in the manufacturing process on the container (3) and placed in a closed position (23) and thereby using the disposable closure device (10) is sealed, in addition to the fuse cover (7) is secured by this is folded into a first detent position on or in the closure lid (7) and brought into an empty transport or operating position (33) before delivery, transported in the empty transport or operating position (33) to a sampling device and set in a receiving device, the safety cover (7) for sampling without tools from the empty transport or operating position (33) is brought into an open position, so that an injection port (20) in the closure lid (5) is accessible, then the milk sample through the injection port (20) into the container (3) is filled and after filling the container (3) of the fuse cover (7) in the lock pressed down to a second detent position (5) and is thereby brought into a securing position (34), in which the securing cover (7) completely in the closure lid (5) is received, and that the container (3) with the milk sample and the closure - (5) and securing cover (7) transported in the tamper-proof securing position (34) and opened for analysis of the closure lid (5) together with the fuse cover (7) received therein. 27. The method according to claim 26, characterized in that the one-way closure device (10) and / or a membrane (41) of the injection opening (20) of the closure lid (5) and / or a material dilution (30) in the Si be checked visually for integrity. 28. The method of claim 26 or 27, characterized in that a TAG (9) during manufacture of the sample container (2) in the closure lid (5) or in the container bottom (19) is introduced, or is subsequently fixed reusable. 29. The method according to any one of claims 26 to 28, characterized in that the sample container (2) with closure lid (5) in the closed position (23) and securing cover (7) in the empty transport or operating position (33) arranged for sampling in a receiving device is after the fuse cover (7) is brought into the open position without tools, after rotation of the receiving device and locking the sample container (2) raised or a filling device is lowered with an injection cannula, and that solved after filling the sample, the locking position of the receiving device, the safety cover (7) is pressed completely into the inner pot (24) of the closure cap (5) and then the sample container (2) is removed and transported to a testing laboratory for analysis in a transport magazine.