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WO2007062276A3 - Continuous flow biodiesel processor - Google Patents

Continuous flow biodiesel processor Download PDF

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Publication number
WO2007062276A3
WO2007062276A3 PCT/US2006/045743 US2006045743W WO2007062276A3 WO 2007062276 A3 WO2007062276 A3 WO 2007062276A3 US 2006045743 W US2006045743 W US 2006045743W WO 2007062276 A3 WO2007062276 A3 WO 2007062276A3
Authority
WO
WIPO (PCT)
Prior art keywords
continuous flow
biodiesel processor
flow biodiesel
processor
flow
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US2006/045743
Other languages
French (fr)
Other versions
WO2007062276A2 (en
Inventor
Randall Ames
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of WO2007062276A2 publication Critical patent/WO2007062276A2/en
Anticipated expiration legal-status Critical
Publication of WO2007062276A3 publication Critical patent/WO2007062276A3/en
Ceased legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1806—Stationary reactors having moving elements inside resulting in a turbulent flow of the reactants, such as in centrifugal-type reactors, or having a high Reynolds-number
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B01D17/0208—Separation of non-miscible liquids by sedimentation
    • B01D17/0211—Separation of non-miscible liquids by sedimentation with baffles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B01D17/0217—Separation of non-miscible liquids by centrifugal force
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D63/00—Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/02—Hollow fibre modules
    • B01D63/025—Bobbin units
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1812—Tubular reactors
    • B01J19/1818—Tubular reactors in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B01J19/242—Tubular reactors in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/26—Nozzle-type reactors, i.e. the distribution of the initial reactants within the reactor is effected by their introduction or injection through nozzles
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G OR C10K; LIQUIFIED PETROLEUM GAS; USE OF ADDITIVES TO FUELS OR FIRES; FIRE-LIGHTERS
    • C10L1/00—Liquid carbonaceous fuels
    • C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
    • C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
    • C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
    • C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
    • B01F27/271—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator
    • B01F27/2711—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed radially between the surfaces of the rotor and the stator provided with intermeshing elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/27—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices
    • B01F27/272—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed axially between the surfaces of the rotor and the stator, e.g. the stator rotor system formed by conical or cylindrical surfaces
    • B01F27/2721—Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices with means for moving the materials to be mixed axially between the surfaces of the rotor and the stator, e.g. the stator rotor system formed by conical or cylindrical surfaces provided with intermeshing elements
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00004—Scale aspects
    • B01J2219/00006—Large-scale industrial plants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/0009—Coils
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00761—Details of the reactor
    • B01J2219/00763—Baffles
    • B01J2219/00765—Baffles attached to the reactor wall
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/185—Details relating to the spatial orientation of the reactor vertical
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1943—Details relating to the geometry of the reactor round circular or disk-shaped cylindrical
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1946—Details relating to the geometry of the reactor round circular or disk-shaped conical
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Liquid Carbonaceous Fuels (AREA)
  • Apparatus Associated With Microorganisms And Enzymes (AREA)

Abstract

A continuous flow biodiesel processor utilizing high turbulence mixing of oil being processed and a flow-through separation tank with distinct zones and recirculation draw tubes is described, along with methods for using same.
PCT/US2006/045743 2005-11-28 2006-11-28 Continuous flow biodiesel processor Ceased WO2007062276A2 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US74034605P 2005-11-28 2005-11-28
US60/740,346 2005-11-28

Publications (2)

Publication Number Publication Date
WO2007062276A2 WO2007062276A2 (en) 2007-05-31
WO2007062276A3 true WO2007062276A3 (en) 2009-04-23

Family

ID=38067995

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/US2006/045743 Ceased WO2007062276A2 (en) 2005-11-28 2006-11-28 Continuous flow biodiesel processor

Country Status (2)

Country Link
US (1) US20070175092A1 (en)
WO (1) WO2007062276A2 (en)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100799597B1 (en) * 2006-04-07 2008-01-30 (주)두웰테크놀로지 Alternative fuel production apparatus and method using high efficiency annular reactor
GB2438403B (en) * 2006-05-25 2011-02-23 Viktor Fedorovych Dekhtiaruk Manufacture of biodiesel
EP1920829A1 (en) * 2006-11-07 2008-05-14 Süd-Chemie Ag Amorphous adsorbent, method of obtaining the same and its use in the bleaching of fats and/or oils
EP2102316A1 (en) * 2006-11-07 2009-09-23 Sued-Chemie AG Method for purification of biodiesel
US20080115407A1 (en) * 2006-11-22 2008-05-22 Hoffman Mark A System and method for producing biodiesel
DE102007019379A1 (en) * 2007-04-23 2008-10-30 Bayer Technology Services Gmbh Process for the purification of product mixtures from transesterification reactions
US8052848B2 (en) * 2007-06-26 2011-11-08 The Penn State Research Foundation Ultrasonic and microwave methods for enhancing the rate of a chemical reaction and apparatus for such methods
US8901330B2 (en) * 2007-08-29 2014-12-02 Sauber Llc Method for production of biofuel
AU2014240324B2 (en) * 2007-08-29 2016-06-30 Agron Bioenergy Llc Method for production of biofuel
US20100205853A1 (en) * 2007-10-09 2010-08-19 Council Of Scientific & Industrial Research Process for the Preparation of Biodiesel from Vegetable Oils Containing High FFA
US7452515B1 (en) * 2007-11-06 2008-11-18 Biofuels Allied, Inc. System for creating a biofuel
US9080117B2 (en) * 2008-01-22 2015-07-14 GER Enterprises, LLC Biofuel production method and system
US8097049B2 (en) * 2008-02-07 2012-01-17 The Dallas Group Of America, Inc. Biodiesel purification by a continuous regenerable adsorbent process
CZ305086B6 (en) * 2008-09-16 2015-04-29 Univerzita Pardubice Process for preparing biofuel from vegetable oils, particularly from rapeseed oil
US8232419B2 (en) * 2008-10-02 2012-07-31 The Dallas Group Of America Triacylglycerol purification by a continuous regenerable adsorbent process
WO2010081063A2 (en) * 2009-01-12 2010-07-15 Arisdyne Systems Inc. Process for improved biodiesel fuel
CA2750127A1 (en) * 2009-02-10 2010-08-19 Bio-Alternative Llc Mobile biodiesel production facility
WO2010107446A1 (en) * 2009-03-19 2010-09-23 Green Earth Fuels, Llc Biodiesel cold soak filtering system
AR074573A1 (en) * 2009-12-09 2011-01-26 Biocombustibles Y En Alternativas Als S A A CONTINUOUS PROCEDURE TO PRODUCE BIODIESEL FUEL
WO2012106158A2 (en) * 2011-02-01 2012-08-09 Ohana Investment Works Llc Methods and apparatus for controlling moisture in plant oils and liquid biofuels
CA2768717C (en) * 2011-12-20 2021-03-02 The Biofuel Partnership Limited A biodiesel manufacturing system and apparatus
US8304566B2 (en) 2012-03-09 2012-11-06 Antonio Cantizani Processes and apparatus for small-scale in situ biodiesel production
US9475029B2 (en) * 2013-08-28 2016-10-25 Louisiana Eco Green, L.L.C. Method of manufacturing bio-diesel and reactor
NL2017029B1 (en) * 2016-06-23 2018-01-17 Flowid Holding B V Spinning disc reactor
WO2024205513A1 (en) * 2023-03-28 2024-10-03 Esg Jet (Thailand) Company Limited Method and application for methyl ester and glycerine separation used in biodiesel purification process

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1670593A (en) * 1923-12-03 1928-05-22 Barrett Co Mixing machine and process
US3738492A (en) * 1972-03-17 1973-06-12 Brunswick Corp Oil-water separator
EP0249463A2 (en) * 1986-06-11 1987-12-16 Bio-Energy Technology Ltd. Bio-fuel production
US5514820A (en) * 1989-09-29 1996-05-07 Henkel Kommanditgesellschaft Auf Aktien Continuous process for the production of lower alkyl esters
US6015440A (en) * 1997-10-31 2000-01-18 Board Of Regents Of The University Of Nebraska Process for producing biodiesel fuel with reduced viscosity and a cloud point below thirty-two (32) degrees fahrenheit

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2728457A (en) * 1951-09-14 1955-12-27 Atlantic Refining Co Phase separation process and apparatus
DE4209779C1 (en) * 1992-03-26 1993-07-15 Oelmuehle Leer Connemann Gmbh & Co., 2950 Leer, De
US6174501B1 (en) * 1997-10-31 2001-01-16 The Board Of Regents Of The University Of Nebraska System and process for producing biodiesel fuel with reduced viscosity and a cloud point below thirty-two (32) degrees fahrenheit
PL341110A1 (en) * 1997-11-24 2001-03-26 Energea Umwelttechnologie Gmbh Method of obtaining methyl esters of fatty acids and system therefor
DE59813936D1 (en) * 1998-04-29 2007-04-19 Sulzer Chemtech Ag A method of separating a first from a second liquid
US20030032826A1 (en) * 2001-07-20 2003-02-13 The Board Of Regents Of The University Of Nebraska Transesterification process for production of biodiesel
WO2003022961A1 (en) * 2001-09-09 2003-03-20 Bio-Clean Fuels, Inc. Method and apparatus for making biodiesel fuel
PT1534659E (en) * 2002-08-23 2008-07-03 Richard Gapes Transesterification and esterification of fatty acids and triglycerides by dispersion and dispersion method for the production of fatty acid methylesters
DE10243700A1 (en) * 2002-09-20 2004-04-01 Oelmühle Leer Connemann Gmbh & Co. Method and device for producing biodiesel
US20050027137A1 (en) * 2003-07-29 2005-02-03 Hooker Jeffrey D. Apparatus and method for the production of fatty acid alkyl ester

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1670593A (en) * 1923-12-03 1928-05-22 Barrett Co Mixing machine and process
US3738492A (en) * 1972-03-17 1973-06-12 Brunswick Corp Oil-water separator
EP0249463A2 (en) * 1986-06-11 1987-12-16 Bio-Energy Technology Ltd. Bio-fuel production
US5514820A (en) * 1989-09-29 1996-05-07 Henkel Kommanditgesellschaft Auf Aktien Continuous process for the production of lower alkyl esters
US6015440A (en) * 1997-10-31 2000-01-18 Board Of Regents Of The University Of Nebraska Process for producing biodiesel fuel with reduced viscosity and a cloud point below thirty-two (32) degrees fahrenheit

Also Published As

Publication number Publication date
WO2007062276A2 (en) 2007-05-31
US20070175092A1 (en) 2007-08-02

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