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WO2005116166A1 - Procede permettant de separer la cire de materiaux siliceux - Google Patents

Procede permettant de separer la cire de materiaux siliceux Download PDF

Info

Publication number
WO2005116166A1
WO2005116166A1 PCT/IB2005/051742 IB2005051742W WO2005116166A1 WO 2005116166 A1 WO2005116166 A1 WO 2005116166A1 IB 2005051742 W IB2005051742 W IB 2005051742W WO 2005116166 A1 WO2005116166 A1 WO 2005116166A1
Authority
WO
WIPO (PCT)
Prior art keywords
wax
oil
mixture
weight
product
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/IB2005/051742
Other languages
English (en)
Inventor
Francois Jacques Labuschagne
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Publication of WO2005116166A1 publication Critical patent/WO2005116166A1/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C10PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10GCRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G1/00Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal
    • C10G1/04Production of liquid hydrocarbon mixtures from oil-shale, oil-sand, or non-melting solid carbonaceous or similar materials, e.g. wood, coal by extraction

Definitions

  • the present invention relates to a process for material preparation.
  • the present invention relates to a process for material preparation for preparing a natural wax composition.
  • Wax includes esters of monohydric alcohols of the higher homologues; e.g. beeswax is the myricyl (melissyl) ester of palmitic acid.
  • Oils are a group of neutral lipids that are liquid at room temperature.
  • Fixed (fatty) oils from animal, vegetable and marine sources, consist chiefly of glycerides and esters of fatty acids, and also include essential oils (volatile products, mainly hydrocarbons, with characteristics odours, derived from certain plants).
  • Mineral oils, derived from petroleum, coal, shale, etc. consist of hydrocarbons. Waxes and oils are used inter alia in the cosmetic industry.
  • a process for material preparation includes the step of separating wax and/or organics and/or oil from used siliceous material.
  • a material preparation apparatus for separating wax and/or oil from used siliceous material includes separating means for separating wax and/or organics and/or oil from used siliceous material to obtain wax and/or organics and/or oil.
  • the process may be used to recycle used siliceous material.
  • the used siliceous material may include perlite.
  • the used siliceous material may include diatomaceous earth.
  • the oil may be vegetable oil.
  • the unused siliceous material such as unused refined siliceous material may be added to the used siliceous material.
  • the process may include the step of mixing the used siliceous material including the wax and/or organics and/or oil, with water to obtain a first mixture.
  • the first mixture may be subjected to heat up to 100 degrees Celcius.
  • the heat may be provided via steam and/or boilers.
  • the first mixture may be heated for 2-3 hours.
  • the wax and/or oil may form the top layer of the first mixture and the perlite and water the bottom layer of the mixture due to phase separation and left overnight to settle.
  • the wax and/or oil mixture may be pumped off.
  • the perlite and water mixture may have the following composition :
  • the wax/oil mixture may be pumped into retaining tanks.
  • Oil and wax settlement may take place over a period of 30 to 60 days.
  • the wax may settle at the bottom as a grey wax mixture.
  • the oil may settle at the top.
  • the oil may be pumped off on a weekly basis.
  • a grey wax mixture may be obtained including about 40 weight % oil and 2 weight % organic matter.
  • the grey wax mixture may be subjected to boiling.
  • the boiling may take place in a cooking tank having coils.
  • the boiled wax mixture may be passed through a 200-300 micron filtration system at a temperature of 100 degrees Celcius to obtain a wax filtrate product.
  • the wax filtrate product may have the following composition :
  • the wax filtrate product may include no organic matter due to the filtration.
  • the wax filtrate product may be used in the cosmetic industry as a basis, for lipsticks, eyeliners, base creams and other body and facial lather applications.
  • the wax filtrate product may be used in the fruit industry for coating of fruits.
  • the wax filtrate product may be used in the pharmaceutical industry in the coating of capsules.
  • the wax filtrate product may be a natural product.
  • the invention also extends to any product obtained by means of the aforesaid process.
  • Tablel typical physical characteristics of raw perlite
  • Table 5 chemical analysis of wax filtrate product
  • Table 6 protein composition of wax filtrate product and carbon structure single and double bond compositions.
  • One embodiment of a process for material preparation in accordance with the invention includes the step of separating wax and/or oil from used siliceous material which generally includes perlite and is unused refined siliceous material.
  • the process includes the steps
  • the perlite and water mixture has the following composition : (a) Perlite 58 weight %
  • the grey wax/oil/organic mixture Before separation, the grey wax/oil/organic mixture has a composition of about 40 weight % oil and 2 weight % organic matter.
  • the wax filtrate product has the following composition :
  • the wax filtrate product includes no organic matter due to the filtration.
  • the wax filtrate product once developed to specification can be used in the cosmetic industry as a basis, for lipsticks, and eyeliners.
  • the wax filtrate product can be used in the fruit industry for coating of fruits.
  • the wax filtrate product can be used in the pharmaceutical industry in the coating of capsules.
  • the wax filtrate product is a natural product as no chemicals are added during the process.
  • Table 1 provides the typical physical characteristics of raw perlite
  • Table 2 provides the typical chemical analysis of raw perlite
  • Table 3 provides the physical characteristics of treated perlite
  • Table 4 provides the chemical analysis of treated perlite
  • Table 5 provides the chemical analysis of the wax filtrate product
  • Table 6 provides protein composition of wax filtrate product.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Medicinal Preparation (AREA)
  • Cosmetics (AREA)
  • Fats And Perfumes (AREA)

Abstract

La présente invention concerne un procédé permettant de préparer une matière, lequel procédé comprend une étape qui consiste à séparer la cire et/ou des matières organiques et/ou de l'huile d'un matériau siliceux usagé.
PCT/IB2005/051742 2004-05-27 2005-05-27 Procede permettant de separer la cire de materiaux siliceux Ceased WO2005116166A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
ZA2004/1620 2004-05-27
ZA200401620 2004-05-27

Publications (1)

Publication Number Publication Date
WO2005116166A1 true WO2005116166A1 (fr) 2005-12-08

Family

ID=35450879

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/IB2005/051742 Ceased WO2005116166A1 (fr) 2004-05-27 2005-05-27 Procede permettant de separer la cire de materiaux siliceux

Country Status (2)

Country Link
WO (1) WO2005116166A1 (fr)
ZA (1) ZA200609045B (fr)

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4415432A (en) * 1980-11-19 1983-11-15 Standard Oil Company (Indiana) Hydrocarbon recovery method and apparatus
US4448669A (en) * 1983-03-16 1984-05-15 Phillips Petroleum Company Hydrocarbon recovery from diatomite
DE3323770A1 (de) * 1983-07-01 1985-01-03 Metallgesellschaft Ag, 6000 Frankfurt Verfahren zum trocknen und erhitzen von oelhaltigen feststoffen
US4495058A (en) * 1983-06-06 1985-01-22 Chevron Research Company Process for generating superheated steam using retorted solids
US4539093A (en) * 1982-12-16 1985-09-03 Getty Oil Company Extraction process and apparatus for hydrocarbon containing ores
CA1196594A (fr) * 1982-04-08 1985-11-12 Guy Savard Extraction du petrole present dans les sables bitumineux
US4571294A (en) * 1984-07-02 1986-02-18 Getty Oil Company Process for extracting hydrocarbons from hydrocarbon bearing ores
WO2004101461A1 (fr) * 2003-05-19 2004-11-25 Francois Jacques Labuschagne Procede de traitement de materiau

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4415432A (en) * 1980-11-19 1983-11-15 Standard Oil Company (Indiana) Hydrocarbon recovery method and apparatus
CA1196594A (fr) * 1982-04-08 1985-11-12 Guy Savard Extraction du petrole present dans les sables bitumineux
US4539093A (en) * 1982-12-16 1985-09-03 Getty Oil Company Extraction process and apparatus for hydrocarbon containing ores
US4448669A (en) * 1983-03-16 1984-05-15 Phillips Petroleum Company Hydrocarbon recovery from diatomite
US4495058A (en) * 1983-06-06 1985-01-22 Chevron Research Company Process for generating superheated steam using retorted solids
DE3323770A1 (de) * 1983-07-01 1985-01-03 Metallgesellschaft Ag, 6000 Frankfurt Verfahren zum trocknen und erhitzen von oelhaltigen feststoffen
US4571294A (en) * 1984-07-02 1986-02-18 Getty Oil Company Process for extracting hydrocarbons from hydrocarbon bearing ores
WO2004101461A1 (fr) * 2003-05-19 2004-11-25 Francois Jacques Labuschagne Procede de traitement de materiau

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
DATABASE WPI Week 198525, Derwent World Patents Index; Class Q76, AN 1985-007340 *

Also Published As

Publication number Publication date
ZA200609045B (en) 2008-04-30

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