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WO2005007863A2 - Solubles de distillerie tenant lieu de composant principal dans des blocs proteiques pour le betail - Google Patents

Solubles de distillerie tenant lieu de composant principal dans des blocs proteiques pour le betail Download PDF

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Publication number
WO2005007863A2
WO2005007863A2 PCT/US2004/022261 US2004022261W WO2005007863A2 WO 2005007863 A2 WO2005007863 A2 WO 2005007863A2 US 2004022261 W US2004022261 W US 2004022261W WO 2005007863 A2 WO2005007863 A2 WO 2005007863A2
Authority
WO
WIPO (PCT)
Prior art keywords
solubles
distillers
molasses
distillers solubles
mixture
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US2004/022261
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English (en)
Other versions
WO2005007863A3 (fr
Inventor
Tracy Aurora Christine Snider
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NATIONAL CORN GROWERS ASSOCIATION
Original Assignee
NATIONAL CORN GROWERS ASSOCIATION
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NATIONAL CORN GROWERS ASSOCIATION filed Critical NATIONAL CORN GROWERS ASSOCIATION
Publication of WO2005007863A2 publication Critical patent/WO2005007863A2/fr
Anticipated expiration legal-status Critical
Publication of WO2005007863A3 publication Critical patent/WO2005007863A3/fr
Ceased legal-status Critical Current

Links

Classifications

    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K10/00—Animal feeding-stuffs
    • A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
    • A23K10/37—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material
    • A23K10/38—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from waste material from distillers' or brewers' waste
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K10/00—Animal feeding-stuffs
    • A23K10/30—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms
    • A23K10/33—Animal feeding-stuffs from material of plant origin, e.g. roots, seeds or hay; from material of fungal origin, e.g. mushrooms from molasses
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K20/00—Accessory food factors for animal feeding-stuffs
    • A23K20/10—Organic substances
    • A23K20/158—Fatty acids; Fats; Products containing oils or fats
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K20/00—Accessory food factors for animal feeding-stuffs
    • A23K20/20—Inorganic substances, e.g. oligoelements
    • A—HUMAN NECESSITIES
    • A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23K—FODDER
    • A23K40/00—Shaping or working-up of animal feeding-stuffs
    • A23K40/20—Shaping or working-up of animal feeding-stuffs by moulding, e.g. making cakes or briquettes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
    • Y02P60/80—Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
    • Y02P60/87—Re-use of by-products of food processing for fodder production

Definitions

  • DISTILLERS SOLUBLES AS THE PRIMARY CONSTITUENT TN PROTEIN BLOCKS FOR LIVESTOCK
  • This invention relates generally to the manufacture of protein feed blocks for livestock and, more particularly, to the use of corn distillers solubles as the primary constituent in this process.
  • Distillers solubles and grains are constituents of the stillage that is a byproduct of ethanol production. These stillage by-products contain many nutrients including high protein levels. While the grain portion of the stillage has been extensively utilized as an animal feed product, the demand for solubles has been limited and thus the price paid to distilleries has been low. Furthermore, the demand for distillers solubles that are the by-products of dry-grind ethanol production has been much lower than the corresponding by-products of wet mill ethanol production. To increase the usefulness, demand, and thus the price paid for dry-grind distillers solubles, herein are described protein blocks for livestock feeding which incorporate distillers solubles as the primary constituent as well as the methods for making such protein blocks.
  • U.S. Patent 6,440,478 Bl to Benton et al. teaches a method of making feed blocks involving heating and evaporation of water from a syrup mixture while under vacuum; the problem of feed blocks absorbing moisture in high humidity environments; the need for physical stability of the feed blocks; the degradation of sugars, vitamins, and other nutrients by heat during processing of the feed block materials; the addition of lipid (lecithin) to the feed block mixture; the control of temperature as a variable in feed block formation, including the effect of temperature on the Maillard reaction; the forming of heated and condensed syrup mixtures into feed blocks for livestock; and the cooling of the formed blocks to produce the final product.
  • U.S. Patent 6,440,478 Bl to Benton et al. teaches a method of making feed blocks involving heating and evaporation of water from a syrup mixture while under vacuum; the problem of feed blocks absorbing moisture in high humidity environments; the need for physical stability of the feed blocks; the degradation of sugars, vitamins, and other nutrients by heat during processing of the
  • Patent 5,260,089 to Thornberg teaches a method of making feed blocks which are substantially free of molasses; and of making feed blocks containing distillers grains and solubles wherein nutritional supplements make up less than half of the total weight of the block.
  • U.S. Patent 4,631,192 to Mommer et al. teaches both continuous flow and batch mixing processes for making feed blocks; pouring of heated material into containers for forming into feed blocks; and addition of vitamins and other nutrients as minor constituents of the feed block material.
  • U.S. Patent 3,961,081 to McKenzie teaches a batch mixing method for making feed blocks; heating of the feed material in the presence of reduced vacuum to remove excess water; and the pouring of heated material into molds with subsequent cooling and hardening into feed blocks.
  • U.S. Patent 4,234,608 to Linehan teaches the addition of tallow to animal feed blocks containing molasses, vitamins, and other nutrients.
  • U.S. Patent 5,789,001 to Klopfenstein et al. teaches the addition of lipids to feed blocks; and the effects of pH, temperature, moisture, and time on the progression of the Maillard reaction in the manufacture of feed blocks.
  • An aspect of the present invention is to provide a method for using distillers solubles as the primary constituent in making protein blocks for livestock feeding.
  • a method for making protein blocks for livestock feeding by mixing together distillers solubles, molasses, and tallow, wherein the distillers solubles constitute the primary ingredient in the protein block and the molasses is only a minor constituent of said protein block; removing water from the mixture of distillers solubles, molasses, and tallow using heat and vacuum, so as to condense the mixture; combining the condensed mixture of distillers solubles, molasses, and tallow with premixtures of vitamins, minerals, and other nutrients; pouring the combination of condensed distillers solubles, molasses, and tallow plus nutrient premixtures into molds while the combination is still hot; and cooling the combination to form a protein block.
  • Figure 1 schematically illustrates the production of various stillage byproducts following the fermentation of grains to make ethanol.
  • Figure 2 schematically illustrates the production of protein blocks.
  • Figure 3 illustrates the steam jacketed kettle used to heat the mixture under reduced pressure.
  • Figure 1 illustrates the steps that are taken in the process in which fermenters 10 ferment grains to the subsequent distillation 12 of ethanol to the production of various by-products from the whole stillage that remains after distillation.
  • centrifuges or screens 14 wet grains are separated from liquid solubles.
  • the liquid solubles may be concentrated in an evaporator 16 so as to remove some of the water content.
  • the resulting condensed distillers solubles (CDS) can then either be used in that form 26, or may be used as inputs to other processes.
  • the CDS may be combined with wet grains from the stillage and then dried in a rotary drier 18 or a drum dryer 20.
  • the products of the drying process may be distillers dried grains with solubles 22 or, in the absence of added grains, distillers dried solubles 24.
  • Figure 2 illustrates the production of protein blocks. Liquid solubles, distillers dried solubles, and condensed distillers solubles (collectively 28) are combined with molasses 30 and tallow 32 and the resulting syrup mixture is dehydrated using techniques that are standard in the block manufacturing industry. This step is indicated at 34 in Figure 2.
  • the standard technique which is well-known in the industry, is as follows.
  • the mixture is heated under reduced pressure 36 so as to promote the evaporation of water and the concentration of the mixture.
  • the mixture is dried to a point where it is thick and viscous with a consistency similar to that of taffy.
  • additional ingredients such as vitamins, minerals, and proteins are added to the concentrated mixture so that such additives constitute less than half of the mixture while the evaporated syrups make up greater than one half of the final mixture.
  • This step is indicated at 38 in Figure 2.
  • the mixture of evaporated syrups plus additives is then poured while hot into containers, indicated at 40 in Figure 2, where it is cooled, indicated at 42 in Figure 2, and formed into blocks, indicated in at 44 in Figure 2.
  • the blocks are preferably between ten and two hundred fifty pounds. This step is indicated at 40 in Figure 2.
  • distillers solubles from dry grind ethanol production serve as a replacement for nearly all or all of the molasses as a block ingredient. Distillers solubles are a good replacement for molasses because such solubles have a consistency that is very similar to that of molasses.
  • Distillers solubles from a variety of sources can be used as starting material for making the protein blocks described herein. Solubles from either wet mill or dry grind ethanol production can be mixed with molasses and tallow, as described above, prior to the dehydration step.
  • the molasses may be virtually any molasses including but not limited to cane molasses and beet molasses.
  • the molasses is preferably beet molasses because it is the most "forgiving", or easily mixed/and palatable, of liquids.
  • the solubles can be by-products of ethanol production either for the beverage industry or from fuel-grade or other industrial-grade ethanol.
  • the solubles can be in the form of liquid solubles, condensed distillers solubles, or distillers dried solubles.
  • solubles from the fermentation of other grains including but not limited to wheat, barley, sorghum, and rice, can be used to make the protein blocks described herein.
  • the depth of vacuum used during the dehydration process can be varied to control the rate and final extent of water loss from the distillers solubles mixture.
  • the process can be varied to accommodate various packaging needs.
  • the physical properties of the protein blocks are important.
  • the blocks must be capable of being stored at ambient conditions for prolonged periods and must also be able to withstand varied weather conditions in the field. Especially under conditions of high temperature and humidity the blocks must not exhibit high levels of deliquescence, that is, absorb excessive amounts of moisture. Nonetheless, the blocks must not be so hardened as to make it difficult for livestock to eat from them: livestock must be able to consume the blocks in sufficient quantities so as to promote adequate feeding.
  • Parameters that can be varied to control the stability and texture of the blocks, as well as the nutritional content include the addition of separator byproducts, including but not limited to lipids, to the syrup mixture; the degree of pressure applied when curing the block; and the relative proportions of distillers solubles, molasses, tallow, and additives such as vitamins, minerals, and protein supplements. Finally, additional components may be added to control the extent of the Maillard reaction and Strecker degradation within the mixture, as these reactions have been known to limit the use of corn- based products in substantial quantities in the manufacture of animal feeds. [0029]
  • the temperature at which the process is carried out can have an impact at various steps. The temperature can be altered during condensation of the syrup mixture to control the rate and extent of water loss.
  • the syrup mixture preferably has a high viscosity.
  • the viscosity of the syrup mixture increases as the moisture level of the mixture decreases.
  • the pH of the solubles may also be adjusted to reduce the viscosity of the syrup mixture to a desired level.
  • the steam jacketed kettle operatures under vacuum or low temperature processing.
  • the finished product included a syrup mixture 48 containing fifty percent (50%) condensed distiller's solubles and fifty percent (50%) beet molasses in the wet basis.
  • the cooked basis included approximately twenty-eight percent (28%) distiller's solubles.
  • the texture, color and physical characteristics of the block after cooling was comparable to blocks in which molasses is the sole ingredient.
  • the animals' preference for the distillers solubles-based blocks compared to other available blocks variability in how much each animal consumes; consumptive behavior as it changes from one day to the next; and the amount of block material that is consumed when the animals are first introduced to the new blocks compared to the amount such animals consume after extended exposure to the new block material.

Landscapes

  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Zoology (AREA)
  • Food Science & Technology (AREA)
  • Animal Husbandry (AREA)
  • Health & Medical Sciences (AREA)
  • Botany (AREA)
  • Molecular Biology (AREA)
  • Mycology (AREA)
  • Physiology (AREA)
  • Biotechnology (AREA)
  • Inorganic Chemistry (AREA)
  • Fodder In General (AREA)

Abstract

L'invention concerne un procédé de fabrication de blocs protéiques pour l'alimentation du bétail par le mélange de solubles de distillerie, de mélasses, et de suif, les solubles de distillerie formant l'ingrédient principal du bloc protéique et les mélasses étant uniquement un composant mineur dudit bloc protéique. A cet effet, on élimine l'eau du mélange des solubles de distillerie, des mélasses et du suif au moyen de chaleur et de vide, de manière à condenser le mélange ; on combine le mélange condensé de solubles de distillerie, de mélasses et de suif avec des prémélanges de vitamines, de minéraux et d'autres nutriments ; on verse la combinaison des solubles de distillerie condensés, les mélasses et le suif en plus des prémélanges de nutriments dans des moules alors que la combinaison est encore chaude ; et on refroidit la combinaison afin d'obtenir un bloc protéique.
PCT/US2004/022261 2003-07-10 2004-07-12 Solubles de distillerie tenant lieu de composant principal dans des blocs proteiques pour le betail Ceased WO2005007863A2 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US48649403P 2003-07-10 2003-07-10
US60/486,494 2003-07-10

Publications (2)

Publication Number Publication Date
WO2005007863A2 true WO2005007863A2 (fr) 2005-01-27
WO2005007863A3 WO2005007863A3 (fr) 2006-04-06

Family

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Application Number Title Priority Date Filing Date
PCT/US2004/022261 Ceased WO2005007863A2 (fr) 2003-07-10 2004-07-12 Solubles de distillerie tenant lieu de composant principal dans des blocs proteiques pour le betail

Country Status (2)

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US (1) US20050005863A1 (fr)
WO (1) WO2005007863A2 (fr)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2426425A (en) * 2005-05-25 2006-11-29 Carrs Agriculture Ltd Animal feedstuff preparation using heating and vacuum conditions
EP1927291A1 (fr) * 2006-11-28 2008-06-04 Carrs Agriculture Limited Fabrication de suppléments alimentaires pour animaux

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20120174867A1 (en) * 2010-12-31 2012-07-12 Campbell James W Wildlife feeding block
US20140170748A1 (en) 2012-12-14 2014-06-19 DePuy Synthes Products, LLC Nutrient Enriched Media for hUTC Growth
CN110403072A (zh) * 2018-04-26 2019-11-05 重庆新同连饲料有限公司 一种含糖蜜成分的畜禽饲料配方

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US3961081A (en) * 1972-06-05 1976-06-01 Mckenzie Carl O Molasses feed block for animals and method of making same
US3952115A (en) * 1975-04-02 1976-04-20 The Procter & Gamble Company Fortification of foodstuffs with N-acyl derivatives of sulfur-containing L-amino acid esters
US4089701A (en) * 1976-02-07 1978-05-16 Mitsui Sugar Co., Ltd. Process for solidifying molasses
US4349578A (en) * 1977-09-09 1982-09-14 A. E. Staley Manufacturing Company Condensed vegetable seed solubles animal feed ingredient
NZ188642A (en) * 1977-11-01 1980-04-28 Ici Australia Ltd Manufacture of rigid animal feed supplement block
IE52298B1 (en) * 1980-11-06 1987-09-02 Uniscope Inc Substantially solid animal feed supplement composition and a method of making the same
US4729896A (en) * 1986-06-23 1988-03-08 Pacific Kenyon Corp. Buffered animal feed supplement block
US5068114A (en) * 1989-12-06 1991-11-26 Cargill, Incorporated Animal feed block composition
US5260089A (en) * 1992-01-30 1993-11-09 Harvest Fuel, Inc. Feed supplement composition and method of manufacturing
US6440478B1 (en) * 1993-08-30 2002-08-27 K.E.S. Associates Feed block for animals
WO1995010195A1 (fr) * 1993-10-14 1995-04-20 Westway Trading Corporation Procede de preparation de blocs alimentaires rigides pour animaux
US5789001A (en) * 1995-06-09 1998-08-04 University Of Nebraska Ruminant feed and method for making
US6143335A (en) * 1999-01-26 2000-11-07 Mckenzie International, Inc. Solid nutritional foods and methods of making the same
US6726941B2 (en) * 2001-08-20 2004-04-27 Archer Daniels Midland Company Amorphous solid cast feed product made by solidifying liquid agricultural byproducts
US6793947B2 (en) * 2001-11-30 2004-09-21 Denco Producers Association, Llc Feed supplement and methods of making thereof

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2426425A (en) * 2005-05-25 2006-11-29 Carrs Agriculture Ltd Animal feedstuff preparation using heating and vacuum conditions
EP1726214A1 (fr) * 2005-05-25 2006-11-29 Carrs Agriculture Limited Procédé de fabrication des suppléments de fourrage et l'appareil correspondant
GB2426425B (en) * 2005-05-25 2007-06-06 Carrs Agriculture Ltd Manufacture of animal feed supplements
EP1927291A1 (fr) * 2006-11-28 2008-06-04 Carrs Agriculture Limited Fabrication de suppléments alimentaires pour animaux

Also Published As

Publication number Publication date
WO2005007863A3 (fr) 2006-04-06
US20050005863A1 (en) 2005-01-13

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