[go: up one dir, main page]

WO2004060566A1 - Centrifugal separator - Google Patents

Centrifugal separator Download PDF

Info

Publication number
WO2004060566A1
WO2004060566A1 PCT/JP2002/013612 JP0213612W WO2004060566A1 WO 2004060566 A1 WO2004060566 A1 WO 2004060566A1 JP 0213612 W JP0213612 W JP 0213612W WO 2004060566 A1 WO2004060566 A1 WO 2004060566A1
Authority
WO
WIPO (PCT)
Prior art keywords
cleaning liquid
cleaning
fly
liquid receiving
residual layer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/JP2002/013612
Other languages
French (fr)
Japanese (ja)
Inventor
Koji Fujimoto
Atsushi Onodera
Jun Ohashi
Motoki Numata
Takayuki Isogai
Katsunori Fukuda
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsubishi Chemical Corp
Tomoe Engineering Co Ltd
Original Assignee
Mitsubishi Chemical Corp
Tomoe Engineering Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Mitsubishi Chemical Corp, Tomoe Engineering Co Ltd filed Critical Mitsubishi Chemical Corp
Priority to PCT/JP2002/013612 priority Critical patent/WO2004060566A1/en
Priority to AU2002360052A priority patent/AU2002360052A1/en
Priority to US10/540,472 priority patent/US7140494B2/en
Priority to PCT/JP2003/016873 priority patent/WO2004058410A1/en
Priority to EP09008729A priority patent/EP2108458B1/en
Priority to CNB2003801074619A priority patent/CN100337755C/en
Priority to CN200710089696XA priority patent/CN101041145B/en
Priority to EP03768302A priority patent/EP1579918B8/en
Priority to AU2003292669A priority patent/AU2003292669A1/en
Publication of WO2004060566A1 publication Critical patent/WO2004060566A1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B3/00Centrifuges with rotary bowls in which solid particles or bodies become separated by centrifugal force and simultaneous sifting or filtering
    • B04B3/04Centrifuges with rotary bowls in which solid particles or bodies become separated by centrifugal force and simultaneous sifting or filtering discharging solid particles from the bowl by a conveying screw coaxial with the bowl axis and rotating relatively to the bowl
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B04CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
    • B04BCENTRIFUGES
    • B04B15/00Other accessories for centrifuges
    • B04B15/12Other accessories for centrifuges for drying or washing the separated solid particles

Definitions

  • a screw conveyor is provided in a bowl, and these are relatively rotatably supported to separate a processed material from a stock solution supplied into the bowl, and an inner peripheral surface on one end side of the bowl.
  • the present invention relates to a centrifugal separator having a washing nozzle for ejecting a washing liquid in the section toward the screen section.
  • Such a centrifuge is used for purifying various crystals in the fields of the chemical industry and the food industry. Background art
  • a cleaning nozzle that jets the cleaning liquid toward the relevant part is provided on the hub of the screw conveyor, and the cleaning part sprays the cleaning liquid all over the crystal being transported. Cleaning was done by doing.
  • Patent Literature 1 Japanese Patent Application Laid-Open No. 2000-3202583.
  • the amount of the crystal is proportional to the amount of the liquid passing through the crystal layer.
  • crystals in an amount proportional to the screen opening cause leakage.
  • the present invention has been made in view of the above-mentioned problems of the prior art.
  • a processed material such as a crystal in a main part of a screen part. It is an object of the present invention to provide a centrifugal separator that can not only reduce the decrease in productivity due to the occurrence of clogging due to clogging, but also reduce the amount of clogging of the processed material in the screen part.
  • the gist of the present invention to achieve the above-mentioned object lies in the following inventions.
  • a screw conveyer is provided in a bowl, and these are relatively rotatably supported to separate a processed material from a stock solution supplied into the bowl, and an inner peripheral surface on one end side of the bowl.
  • a centrifugal separator for washing and dewatering the above-mentioned processed material at a screen portion provided along with a cleaning liquid receiving portion for receiving the cleaning liquid supplied to the hub of the screw conveyor;
  • a centrifugal separator having a cleaning nozzle for ejecting a cleaning liquid in a receiving portion toward the screen portion,
  • a residual layer cleaning liquid receiving portion for receiving a cleaning liquid for cleaning a residual layer processed product generated in a gap between an outer peripheral edge of the screw conveyor and an inner peripheral surface of the screen portion is provided with the cleaning liquid. It is provided separately from the receiving part,
  • a centrifugal separator characterized by forming a washing path for the remaining layer to be ejected.
  • a screw conveyer is provided in the powl, and these are relatively rotatably supported to separate the processed material from the undiluted solution supplied into the bowl and to the inner peripheral surface on one end side of the bowl.
  • a centrifugal separator for cleaning and dewatering the above-mentioned processed material at a screen portion provided along the cleaning portion; a cleaning liquid receiving portion for receiving the cleaning liquid supplied to the hub of the screw conveyor; A washing nozzle for ejecting a washing liquid in the section toward the screen section,
  • a cleaning process is performed for cleaning a residual layer processed product generated in a gap between the outer peripheral edge of the screw of the screw conveyor and the inner peripheral surface of the screen portion.
  • a cleaning liquid receiving section for the remaining layer that receives the cleaning liquid is provided separately from the inside of the cleaning liquid receiving section,
  • a connecting pipe is provided at a position where the inner peripheral edge of the fly is continuous at predetermined intervals along a spiral direction of the fly, at a bottom side of the residual layer cleaning liquid receiving portion, and a hub or fly of the screw conveyor is provided.
  • a cleaning liquid discharge hole extending radially from the inner peripheral side of the hub to the outer peripheral edge of the fly and communicating with the connection pipe,
  • a centrifugal separator characterized in that the cleaning liquid in the cleaning liquid receiving portion for the residual layer is jetted directly from the front end of each of the cleaning liquid discharge holes opened in the outer peripheral edge of the cleaning liquid toward the residual layer processing object.
  • a screw conveyor is provided in the bowl, and these are relatively rotatably supported.
  • the processed material is separated from the stock solution supplied into the bowl, and the inner peripheral surface at one end of the powl is provided.
  • a centrifugal separator for washing and dewatering the processed material in a screen section provided along the line, wherein a cleaning liquid receiving section for receiving the cleaning liquid supplied into the hap of the screw conveyer;
  • a centrifugal separator having a cleaning nozzle for ejecting a cleaning liquid in a receiving portion toward the screen portion,
  • a residual layer cleaning liquid receiving portion for receiving a cleaning liquid for cleaning a residual layer processed product generated in a gap between an outer peripheral edge of the screw conveyor and an inner peripheral surface of the screen portion is provided. It is provided separately from the inside of the washing liquid receiving section,
  • a connection pipe is provided at a position adjacent to a surface of the fly opposite to the processed material transfer surface, at predetermined intervals along a spiral direction of the fly, at a bottom side of the residual layer cleaning liquid receiver, and Providing a washing liquid communication hole through which the connection pipe communicates with the haptic of the screw conveyor;
  • a predetermined distance along the spiral direction of the flight At intervals, a cleaning liquid discharge pipe extending radially from the inner peripheral edge to the outer peripheral edge of the flight and communicating with the cleaning liquid communication hole is attached,
  • a centrifugal separator wherein the cleaning liquid in the cleaning liquid receiving portion for the residual layer is directly discharged from the distal end of the cleaning liquid discharge pipe toward the residual layer processed material.
  • a feed tube for supplying a stock solution extending in the axial direction is inserted into the inside of the hub of the screw conveyor.
  • a cleaning liquid supply path for supplying a cleaning liquid to the cleaning liquid receiving section is formed in the feed tube, and an opening for the cleaning liquid supply path is provided in the middle of the feed tube overlapping the cleaning liquid receiving section in the radial direction.
  • a residual layer cleaning liquid supply path for supplying the residual layer cleaning liquid to the residual layer cleaning liquid receiving part is formed, and in the middle of a feed tube radially overlapping the residual layer cleaning liquid receiving part.
  • the centrifuge described in the above [1] when the stock solution is supplied into the powl, the stock solution is separated into a processed product and a mother liquor in the bowl by centrifugal force, and the processed product is formed on the inner peripheral surface of the bowl.
  • the settled material is conveyed by a screw conveyor provided with a rotation difference from the bowl.
  • the processed material is not sufficiently transported by the conveyor, and is c transported as the remaining layer. Processed material that has been drained on the way is generally free from impurities generated during the manufacturing process.
  • a screen provided along the inner peripheral surface at one end of the bowl is used to clean the screen at the hub of the screw conveyor. Cleaning is performed by spraying the cleaning liquid from the nozzle toward the processing object.
  • the cleaning liquid here is supplied to the cleaning liquid receiving section in the haptic via a cleaning liquid supply path separately provided in a feed tube for supplying the undiluted liquid into the bowl.
  • a remaining layer cleaning liquid receiving portion for receiving a cleaning liquid for cleaning the remaining layer of the processed material is provided separately from the cleaning liquid receiving portion, and the remaining layer cleaning liquid receiving portion is provided.
  • the cleaning liquid supplied to the filter is separated from the cleaning liquid receiving portion by the residual layer cleaning path provided along the spiral direction of the fly, and directly from the outer peripheral edge of the fly toward the residual layer processing object. It is gushing. As a result, it is possible to separately perform the cleaning of the processed material by the cleaning nozzle and the cleaning of the residual layer processed material by the cleaning path for the residual layer, so that the type and amount of the cleaning liquid can be different from each other. .
  • the residual layer processed material generated in the gap between the outer peripheral edge of the screw conveyor and the inner peripheral surface of the screen portion can be particularly directly cleaned, so that the residual layer can be cleaned.
  • the cleaning liquid in the residual layer cleaning liquid receiving portion is provided at a predetermined interval along a spiral direction of the fly at a position where the inner peripheral edge of the fly is continuous. Washing provided inside the hub or flight of the screw conveyor through the connection pipes provided every other Jump out into the bowl from the liquid discharge hole.
  • the cleaning liquid discharge holes radially extend from the inner peripheral side of the hub to the outer peripheral edge of the fly, and are directed toward the residual layer processing object from the front end openings of the respective cleaning liquid discharge holes that open to the outer peripheral edges of the fly. The cleaning liquid can be ejected directly.
  • a groove extending continuously in the spiral direction of the fly and communicating with the distal end port of each of the washing liquid discharge holes is formed on the distal end surface of the outer peripheral edge of the fly. If formed, the cleaning liquid discharged from the tip end of each cleaning liquid discharge hole spreads over the entire outer peripheral edge of the fly along the groove, and is directly jetted toward the remaining layer processing material so as to spread over the entire circumference in the radial direction. That's a thing.
  • the cleaning liquid in the residual layer cleaning liquid receiving portion is subjected to a frying operation at a position adjacent to a surface of the freight opposite to a processing object transport surface.
  • the cleaning liquid discharge pipes that are introduced into the cleaning liquid discharge pipes provided at predetermined intervals along the spiral direction extend radially from the inner peripheral edge to the outer peripheral edge of the fly, and extend along the outer peripheral edge of the fly.
  • the cleaning liquid can be jetted directly from the tip end of each of the cleaning liquid discharge pipes toward the residual layer processed material. According to such a configuration, it is not necessary to provide a hole in the fly itself, and the cleaning liquid discharge pipe can be retrofitted to the fly, so that the manufacture can be performed relatively easily. .
  • the cleaning liquid is similarly introduced into the hub.
  • a part of the feed tube for supplying the undiluted solution can be effectively used.
  • a cleaning liquid supply path for supplying the cleaning liquid to the cleaning liquid receiving section is formed in the feed tube, and an opening for the cleaning liquid supply path is provided in the middle of the feed tube overlapping the cleaning liquid receiving section in the radial direction.
  • a residual layer cleaning liquid supply path for supplying the residual layer cleaning liquid to the residual layer cleaning liquid receiving section is formed in the feed tube, and in the middle of a feed tube radially overlapping the residual layer cleaning liquid receiving section.
  • FIG. 1 is a longitudinal sectional view showing a main part of a centrifuge according to a first embodiment of the present invention.
  • FIG. 2 is a longitudinal sectional view showing the whole of the centrifuge according to the first embodiment of the present invention.
  • FIG. 3 is a sectional view taken along line III-III in FIG.
  • FIG. 4 is a longitudinal sectional view showing a main part of a centrifuge according to a second embodiment of the present invention.
  • FIG. 5 is an enlarged longitudinal sectional view showing a main part of a centrifuge according to a second embodiment of the present invention.
  • FIG. 6 is a sectional view taken along line VI-VI of FIG.
  • FIG. 7 is a longitudinal sectional view showing a main part of a centrifuge according to a third embodiment of the present invention.
  • FIG. 8 is a cross-sectional view taken along the line VIII-VIII of FIG. BEST MODE FOR CARRYING OUT THE INVENTION
  • FIG. 1 to 3 show a first embodiment of the present invention.
  • the centrifugal separator 10 is called a screen bowl type centrifugal separator, and is provided with a screw conveyor 40 in a substantially cylindrical bowl 20. It is supported so as to be relatively rotatable, and is configured such that a processed material to be processed and a mother liquor can be separately separated from a stock solution supplied into the bowl 20.
  • the processed material corresponds to various crystals in the fields of the chemical industry and the food industry, and specifically, for example, terephthalic acid as a raw material for pet bottles and polyester fibers, paraxylene as a raw material for terephthalic acid, and CD.
  • Bisphenol which is a raw material for ROM
  • glutamine soda which is a raw material for chemical seasonings and ingredients.
  • Various solvents correspond to the mother liquor.
  • Each seed crystal has a solvent constituting an unpolymerized substance slurry adhered to the crystal surface during the manufacturing process, and these adhered substances can be washed and replaced with a washing liquid (a specific other solvent or the like).
  • a washing liquid a specific other solvent or the like
  • the bowl 20 and the screw conveyor 40 therein are rotatably supported inside the casing 11 via shafts 12a and 12b.
  • the powl 20 and the screw conveyor 40 are rotationally driven at a slight differential speed by a differential device 14 connected to a bearing 13 on one side.
  • a differential device 14 itself is publicly known, and a detailed description thereof will be omitted.
  • the interior of the casing 11 is partitioned so as to correspond to a discharge port 24, a screen portion 30, a dam portion 26, and the like provided in a bowl 20 described below.
  • a crystal discharge port 15 communicating with the discharge port 24, a cleaning liquid discharge port 16 communicating with the screen section 30, and a mother liquid discharge port 1 communicating with the dam section 26 are provided at a lower portion of the casing 11.
  • One end side of the bowl 20 (right side in Fig. 2) is the direction of crystal discharge, and from the other end side of the pole 20 (left side in Fig. 2), in order from the large-diameter parallel 'cylindrical part 21 and one end. It is divided into a tapered portion 22 whose inner diameter gradually decreases toward the side, and a small-diameter parallel tube portion 23. At the distal end of the small-diameter parallel cylindrical portion 23, a crystal discharge port 24 is opened, and near the distal end of the large-diameter parallel cylindrical portion 21, the liquid depth in the radial direction of the bowl 20 is regulated.
  • a dam 26 is provided which can discharge the mother liquor from which the crystals have been separated out of the bowl 20.
  • the small-diameter parallel cylindrical portion 23 has a large number of filtrate discharge holes 25 formed on the wall surface, and the inner peripheral side is covered with a cylindrical filter medium 31 in the entire circumferential direction, and the screen is screened. Part 30.
  • the size of the filtrate discharge hole 25 does not need to be considered so much in terms of the crystal particle diameter.
  • the filter medium 31 is made of a material having a large number of micropores or slits whose diameter is smaller than the crystal particle diameter. Become. Specifically, for example, edge wire screens, porous ceramic moldings, and the like may be used.
  • the inner peripheral surface of the parallel cylindrical portion 23 is shaved by the thickness of the filter medium 31.
  • the screw conveyor 40 includes a hub 41 serving as a rotating shaft thereof, and a fly 42 provided in a screw-shape on the outer periphery of the hub 41.
  • the fly 42 holds crystals in a bowl 20. It is formed so as to be conveyed to one end (right side in Fig. 2).
  • the screw conveyor 40 and the bowl 20 are different between the outer peripheral edge of the fly 42 and the inner peripheral surface of the parallel tubular portion 23 (the surface of the filter medium 31 of the screen portion 30). Due to the structure that rotates at the speed, it is set so that there is a gap in the radial direction.
  • the hub 41 has a cleaning liquid receiving portion 43 for receiving the cleaning liquid supplied therein, and a cleaning nozzle 4 for jetting the cleaning liquid in the cleaning liquid receiving portion 43 toward the screen portion 30 of the bowl 20. 5 is provided.
  • the cleaning liquid receiving section 43 is located in the entire circumferential direction of the inner peripheral surface of the hub 41! : Specified width in the direction of the beam axis It consists of a part surrounded by a partition that extends to
  • a cleaning liquid communication hole 44 is provided at predetermined intervals on a peripheral wall of the hap 41, which is a bottom side of the cleaning liquid receiving portion 43, and a cleaning communicating with the cleaning liquid communication hole 44 is provided on an outer peripheral surface side of the hap 41.
  • Nozzles 45 are provided.
  • the cleaning nozzle 45 is arranged at a position slightly opposite to the center of the pitch of the fly 42 as shown in FIG. 1 (left side in FIG. 1) and facing the screen portion 30 in the radial direction. I have.
  • a residual layer cleaning liquid receiving section 46 for receiving a cleaning liquid for cleaning residual layer crystals generated in a gap between the outer peripheral edge of the fly 42 and the inner peripheral surface of the screen section 30 is provided. It is provided separately from the inside of the washing liquid receiving section 43.
  • the residual layer cleaning liquid receiving part 46 is provided with a partition extending at a predetermined width in the axial direction over the entire circumferential direction at both ends of the cylindrical member. 7 is provided so as to protrude, and the cleaning liquid receiving portion 46 for the remaining layer is fixed by the respective connection pipes 47 so as to be separated from the inner peripheral surface of the hub 41 in the cleaning liquid receiving portion 43.
  • the connection pipes 47 are arranged at predetermined intervals along the spiral direction of the fly 42 at a position where the inner peripheral edge of the fly 42 is continuous.
  • the outer peripheral edge of the fly 42 from the inner peripheral side of the hub 41.
  • a plurality of cleaning liquid discharge holes 49 are provided extending in the radial direction to communicate with the connection pipes 47.
  • the cleaning liquid discharge holes 49 together with the connection pipes 47 are used to transfer the cleaning liquid in the residual layer cleaning liquid receiving section 46 from the outer periphery of the fly 42 while being separated from the cleaning liquid receiving section 43. It forms a cleaning path for the residual layer that is jetted directly toward the residual layer crystal on the lean part 30.
  • a feed tube for supplying a stock solution extending in the axial direction is provided inside the hub 41.
  • Move 60 has been purchased.
  • the starting end of the feed tube 60 extends outside from the hub 41 and the bowl 20 to become a stock solution supply port 61, and the end of the feed tube 60 is arranged substantially in the center of the hub 41 and has a stock solution outlet 6.
  • the cleaning liquid is supplied to the cleaning liquid supply pipe 71 for supplying the cleaning liquid to the cleaning liquid receiving section 43 in the feed tube 60 and the cleaning liquid receiving section 46 for the residual layer.
  • a residual layer cleaning liquid supply pipe 72 forming a residual layer cleaning liquid supply path.
  • the starting end of the cleaning liquid supply pipe 71 forms a cleaning liquid supply port 71 a that opens substantially perpendicularly to the axial direction on the starting end side of the feed tube 60. Also, in the middle of the feed tube 60 radially overlapping the cleaning liquid receiving portion 43 in the hub 41, an opening 71b of the cleaning liquid supply pipe 71 is opened substantially at right angles to the axial direction. are doing. On the other hand, the beginning of the residual-layer cleaning liquid supply pipe 72 forms a residual-layer cleaning liquid supply port 72 a that opens substantially perpendicularly to the axial direction on the start end side of the feed tube 60.
  • an opening 72b of the cleaning liquid supply pipe 72 for the residual layer is substantially in the axial direction. It opens at right angles.
  • the stock solution is supplied into the bowl 20 via a feed tube 60 using a drive source such as a pump.
  • the undiluted solution sent from the undiluted solution supply port 61 of the feed tube 60 is transferred to the hub of the screw compressor 40.
  • the solution exits from a stock solution outlet 62 located in the vicinity of the center in 41 and is inserted into a dam portion 26 in a bowl 20 to a predetermined depth set in advance.
  • Stock solution is bowl
  • the crystal that settles to the inner peripheral surface side of the bowl 20 due to the action of the centrifugal force is converted into the tapered portion of the powl 20 by the fly 42 of the screw conveyor 40 rotating at a slightly different speed from the bowl 20. Conveyed to 2 and set in advance in dam section 26 The liquid is removed when moving on the inner peripheral surface of the tapered portion 22 to the inner diameter side of the liquid depth, and is further conveyed to the screen portion 30.
  • the washing liquid is generally pure water, acetic acid, pure phenol, sulfuric acid, hydrochloric acid, or the like.
  • the washing liquid is supplied through the washing liquid supply pipe 71 inserted separately into the feed tube 60.
  • the cleaning liquid is supplied to the cleaning liquid receiving part 43 in the hap 41.
  • the cleaning liquid received in the cleaning liquid receiving part 43 is ejected from the cleaning nozzle 45 through the cleaning liquid communication hole 44 in the peripheral wall of the hub 41.
  • the crystal undergoes the washing and dewatering actions in the screen part 30 and is further conveyed to the discharge port 24 side, and the crystal is conveyed to the outer periphery of the fly 42 of the screen conveyor 40.
  • a crystal residual layer is formed in the gap between the screen portion 30 and the inner peripheral surface.
  • the residual layer crystal is directly and locally cleaned by the cleaning liquid sprayed from the outer periphery of the fly 42 in a state of being separated from the cleaning liquid receiving portion 43 by the residual layer cleaning path.
  • the cleaning liquid used here is the same as the liquid ejected from the cleaning nozzle 45.
  • the cleaning liquid is supplied through the residual layer cleaning liquid supply pipe 72 separately inserted into the feed tube 60, and the haptic 4 1 It is supplied to the residual layer cleaning liquid receiving part 46 inside.
  • the cleaning liquid in the residual layer cleaning liquid receiving portion 46 is provided at predetermined intervals along the spiral direction of the fly 42 at a position where the inner peripheral edge of the fly 42 is continuous. It passes through the connecting pipe 47 and jumps out into the bowl 20 from the washing liquid discharge hole 49 provided inside the hub 41 or the fly 42.
  • the cleaning liquid discharge holes 49 extend radially from the inner peripheral side of the hub 4 1 to the outer peripheral edge of the fly 4 2. Do not spray the cleaning solution directly on the remaining crystal. Can be.
  • the residual layer crystal can be particularly locally and directly cleaned by the residual layer cleaning path, so that the residual layer crystal is not fixed and moves. And the permeability of the cleaning solution to the entire crystal being transported is improved. Therefore, the clogging of the crystal in the screen part 30 can be prevented beforehand, and the amount of the cleaning liquid for replacing the original impurity in the crystal can be suppressed. It is possible to reduce the amount of crystal leakage at 30.
  • the cleaning liquid ejected from the cleaning nozzle 45 and the residual layer cleaning path passes through the filter medium 31 after washing the crystals and residual layer crystals, and the filtrate is discharged from the discharge hole 25 to the bowl 2 °. Is discharged to the outside. Further, the crystals washed and drained in the screen section 30 are discharged from the discharge port 24 to the outside of the bowl 20, and finally collected from the crystal discharge port 15 in the casing 11. 4 to 6 show a second embodiment of the present invention.
  • the centrifuge 1 OA extends continuously to the tip end surface of the outer periphery of the fly 42 in the first embodiment described above in the spiral direction of the fly 42, A groove 49a is formed in which the tip end of each cleaning liquid discharge hole 49 communicates.
  • the width of the groove 49a may be set to about 1 to 5 mm, and the depth may be set to about 10 to 25 mm.
  • the cleaning liquid discharged from the tip end of each of the cleaning liquid discharge holes 49 spreads over the entire outer peripheral edge of the fly 42 along the groove 49a, and the remaining layer It can be directly extracted so as to spread all over the circumference in the radial direction toward the processing object.
  • This makes it possible to enhance the permeability of the cleaning liquid to the crystals and the mobility of the remaining layer crystals, as in the above embodiments.
  • the centrifugal separator 10 B includes a connection pipe 47 of the residual-layer washing liquid receiving section 46, and a processing object transport surface 4 of the fly 42. At the position adjacent to the surface 4 2b opposite to 2 a, they are arranged at predetermined intervals along the spiral direction of the fly 42, and the connecting pipe 4 is provided on the peripheral wall of the hub 41. A cleaning liquid communication hole 48 for communicating with 7 is provided.
  • the cleaning liquid in the residual layer cleaning liquid receiving portion 46 is located at a position adjacent to the surface 42 b of the fly 42 opposite to the processing object transport surface 42 a.
  • a connecting pipe 47 provided at a predetermined interval along a spiral direction of the fly 42, and a hub of the screw conveyor 40.
  • Each washing liquid discharge pipe 80 extends from the inner peripheral edge of the fly 42 to the outer peripheral edge.
  • the cleaning liquid can be directly ejected toward the residual layer processing object from the distal end port of each cleaning liquid discharge pipe 80 along the outer periphery of the fly 42. According to such a configuration, it is not necessary to form a hole in the fly 42 itself, and the cleaning liquid discharge pipe 80 can be retrofitted to the fly 42, so that it can be manufactured relatively easily.
  • the cleaning liquid discharge pipes 80 By attaching the cleaning liquid discharge pipes 80 radially at as small an interval as possible, the cleaning liquid can be ejected so as to spread over the remaining layer crystals in all circumferential directions.
  • the cleaning liquid when the cleaning liquid is applied to the entire processed material, the amount of the processed material is proportional to the amount of the cleaning liquid passing through the processed material layer, and the amount of the processed liquid is proportional to the opening of the screen.
  • the cleaning liquid is sprayed directly from the outer peripheral edge of the freight to the remaining layer processing material as described above, thereby preventing the remaining layer processing material from sticking to the processing object being transported. Since the permeability of the cleaning solution is improved, the cleaning solution is intended to replace impurities in the original processed product. This makes it possible to reduce the amount, and it is possible to reduce the total leakage amount of the processed material in the screen part.

Landscapes

  • Centrifugal Separators (AREA)

Abstract

A screen-bowl type centrifugal separator capable of eliminating productivity lowering caused by clogging by a material to be processed such as crystals in a screen portion as an essential portion of the separator as well as reducing the leak of the material to be processed in the screen portion. Inside a hub (41) of a screw conveyer (40), a cleaning liquid receiver (43) is provided for receiving the cleaning liquid for a cleaning nozzle (45). Furthermore, inside the cleaning liquid receiver (43), there is provided a remaining layer cleaning liquid receiver (46) separately from the cleaning liquid receiver (43), for receiving a cleaning liquid for cleaning the remaining layered material to be processed in the screen portion (30). The cleaning liquid supplied to the remaining layer cleaning liquid receiver (46) is injected by a remaining layer cleaning path provided along a helical direction of a flight (42), while being separated from the cleaning liquid receiver (43), directly toward the remaining layered material to be processed from the outer periphery of the flight (42).

Description

明細書 遠心分離機 技術分野  Description Centrifuge Technical field

本発明は、 ボウル内にスク リューコンペャを備え、 これらを相対的に 回転可能に支持してなり、 前記ボウル内に供給した原液から処理物を分 離すると共に、 該ボウルの一端側の内周面に沿って設けたスクリーン部 で、 前記処理物の洗浄およぴ脱液を行う遠心分離機において、 前記スク リューコンペャのハブに、 その内部に供給した洗浄液を受け入れる洗浄 液受け部と、 該洗浄液受け部内の洗浄液を前記スクリーン部に向かって 噴出する洗浄ノズルとを有する遠心分離機に関する。 このような遠心分 離機は、 化学工業や食品工業の分野における各種結晶の精製に用いられ るものである。 背景技術  According to the present invention, a screw conveyor is provided in a bowl, and these are relatively rotatably supported to separate a processed material from a stock solution supplied into the bowl, and an inner peripheral surface on one end side of the bowl. A centrifugal separator for washing and dewatering the processing object by means of a screen provided along with a cleaning liquid receiver for receiving the cleaning liquid supplied to the hub of the screw conveyer; The present invention relates to a centrifugal separator having a washing nozzle for ejecting a washing liquid in the section toward the screen section. Such a centrifuge is used for purifying various crystals in the fields of the chemical industry and the food industry. Background art

従来、 スク リーンボウル型の遠心分離機では、 ボウル内に結晶性の固 形物と溶媒からなる原液が供給されると、 遠心力によりボウル内で原液 が処理物である結晶と溶媒とに分けられ、 結晶はボウルの内周面に沈降 して、 ボウルと微少の回転差を与えられているスク リ ューコンペャによ り搬送され、 ポウルの一端側にあるテーパー部にて脱液作用を受ける。 脱液された結晶は、 一般的にその製造過程で生じた不純物や溶媒その ものを結晶表面に付着させており、 これら余分な付着物を洗浄するため に、 テーパー部に続くボウル内周側にスク リーン部を設けると共に、 当 該部位に向かって洗浄液を噴出する洗浄ノズルをスクリユーコンべャの ハブに設けて、 スク リーン部で搬送途中の結晶に洗浄液をくまなく噴射 することで洗浄を行っていた。 例えば、 特許文献 1 (特開 2 0 0 0— 3 2 5 8 3 3号公報) 参照。 ' Conventionally, in a screen bowl type centrifuge, when an undiluted solution consisting of a crystalline solid and a solvent is supplied into the bowl, the undiluted solution is separated into crystals and a solvent in the bowl by centrifugal force. The crystals settle on the inner peripheral surface of the bowl, and are conveyed by a screw con- verter provided with a slight rotation difference from the bowl, and are subjected to a liquid removing action at a tapered portion on one end side of the powl. In general, the dehydrated crystals adhere to the crystal surface impurities and solvents generated during the manufacturing process.In order to clean these extra deposits, the crystals are placed on the inner peripheral side of the bowl following the taper. In addition to providing a screen part, a cleaning nozzle that jets the cleaning liquid toward the relevant part is provided on the hub of the screw conveyor, and the cleaning part sprays the cleaning liquid all over the crystal being transported. Cleaning was done by doing. For example, see Patent Literature 1 (Japanese Patent Application Laid-Open No. 2000-3202583). '

しかしながら、 前述したようなスクリーンボウル型の遠心分離機では. スクリユーコンべャのフライ ト外周縁とスクリーン部内周面との間に形 成される半径方向の隙間において、 結晶はコンペャでは搬送されず、 長 時間の運転によって結晶の残層は移動がなく、 フライ ト外周縁に押し付 けられることにより、 - 固く しまった状態となる。  However, in the screen bowl type centrifuge as described above. In the radial gap formed between the outer peripheral edge of the screw conveyor and the inner peripheral surface of the screen, crystals are not transported by the conveyor. After a long operation, the residual layer of the crystal does not move, and is pressed against the outer periphery of the flight.

このよ うに残層をなす結晶は、 洗浄液の透過性を阻害するばかりでな く、 新しい残層結晶に入れ替わるための移動性も阻害する状態となって しまう という問題がある。 かかる状態は、 一般的にスク リーンの目詰ま り と呼ばれている。 スク リーンの目詰まりを解消するためには、 原液の 供給を一時停止させ、 代わりに一定時間の間、 洗浄液を供給する必要が ある。 そのため、 原液供給の停止時間は生産に寄与できないことになり 生産性を低下させる要因となっていた。  Thus, there is a problem that the crystals forming the remaining layer not only impair the permeability of the cleaning solution, but also impair the mobility for replacement with the new remaining layer crystal. Such a condition is generally called screen clogging. In order to eliminate the clogging of the screen, it is necessary to suspend the supply of the stock solution and to supply the cleaning solution for a certain period of time instead. For this reason, the suspension time of the supply of undiluted solution could not contribute to production, which was a factor that reduced productivity.

さらにまた、 スク リ ーン部での目漏れについても、 フライ トで搬送さ れている結晶全体にくまなく洗浄液を噴出した場合には、 結晶層を通過 する液量に比例した量の結晶と、 スク リーンの目開きに比例した量の結 晶が目漏れを生じてしまう という問題があった。  Furthermore, regarding the leakage at the screen part, when the cleaning liquid is jetted all over the crystal transported by the fly, the amount of the crystal is proportional to the amount of the liquid passing through the crystal layer. However, there has been a problem that crystals in an amount proportional to the screen opening cause leakage.

本発明は、 以上のような従来技術が有する問題点に着目してなされた もので、 スク リーンボウル型の遠心分離機 おいて、 その要部であるス クリーン部での特に結晶等の処理物による目詰まりの発生に伴う生産性 の低下を解消させるだけでなく、 スク リーン部における処理物の目漏れ 量を減少させることができる遠心分離機を提供することを目的としてい る。 ' 発明の開示 前述した目的を達成するための本発明の要旨とするところは、 次の各 項の発明に存する。 SUMMARY OF THE INVENTION The present invention has been made in view of the above-mentioned problems of the prior art. In a screen bowl type centrifugal separator, a processed material such as a crystal in a main part of a screen part is provided. It is an object of the present invention to provide a centrifugal separator that can not only reduce the decrease in productivity due to the occurrence of clogging due to clogging, but also reduce the amount of clogging of the processed material in the screen part. '' Disclosure of the Invention The gist of the present invention to achieve the above-mentioned object lies in the following inventions.

[ 1 ] ボウル内にスクリューコンペャを備え、 これらを相対的に回転可 能に支持してなり、 前記ボウル内に供給した原液から処理物を分離する と共に、 該ボウルの一端側の内周面に沿って設けたスク リーン部で、 前 記処理物の洗浄および脱液を行う遠心分離機において、 前記スクリュー コンべャのハブに、 その内部に供給した洗浄液を受け入れる洗浄液受け 部と、 該洗浄液受け部内の洗浄液を前記スクリーン部に向かって噴出す る洗浄ノズルとを有する遠心分離機であって、  [1] A screw conveyer is provided in a bowl, and these are relatively rotatably supported to separate a processed material from a stock solution supplied into the bowl, and an inner peripheral surface on one end side of the bowl. A centrifugal separator for washing and dewatering the above-mentioned processed material at a screen portion provided along with a cleaning liquid receiving portion for receiving the cleaning liquid supplied to the hub of the screw conveyor; A centrifugal separator having a cleaning nozzle for ejecting a cleaning liquid in a receiving portion toward the screen portion,

前記洗浄液受け部内に、 前記スク リ ューコンペャのフライ ト外周縁と 前記スクリーン部内周面との間の隙間に生じる残層処理物を洗浄する洗 浄液を受け入れる残層用洗浄液受け部を、 前記洗浄液受け部内とは独立 に区画して設け、  In the cleaning liquid receiving portion, a residual layer cleaning liquid receiving portion for receiving a cleaning liquid for cleaning a residual layer processed product generated in a gap between an outer peripheral edge of the screw conveyor and an inner peripheral surface of the screen portion is provided with the cleaning liquid. It is provided separately from the receiving part,

前記フライ トのらせん方向に沿って、 前記残層用洗浄液受け部内の洗 浄液を、 前記洗浄液受け部とは仕切られた状態で前記フライ ト外周縁よ り前記残層処理物に向けて直接噴出させる残層用洗浄経路を形成したこ とを特徴とする遠心分離機。  Along the spiral direction of the flight, the cleaning liquid in the cleaning liquid receiving portion for the residual layer is directly separated from the cleaning liquid receiving portion toward the residual layer processed material from the outer peripheral edge of the flight. A centrifugal separator characterized by forming a washing path for the remaining layer to be ejected.

[ 2 ] ポウル内にスク リューコンペャを備え、 これらを相対的に回転可 能に支持してなり、 前記ボウル内に供給した原液から処理物を分離する と共に、 該ボウルの一端側の内周面に沿って設けたスク リーン部で、 前 記処理物の洗浄および脱液を行う遠心分離機において、 前記スクリュー コンべャのハブに、 その内部に供給した洗浄液を受け入れる洗浄液受け 部と、 該洗浄液受け部内の洗浄液を前記スクリーン部に向かって噴出す る洗浄ノズルとを有する遠心分離機であって、  [2] A screw conveyer is provided in the powl, and these are relatively rotatably supported to separate the processed material from the undiluted solution supplied into the bowl and to the inner peripheral surface on one end side of the bowl. A centrifugal separator for cleaning and dewatering the above-mentioned processed material at a screen portion provided along the cleaning portion; a cleaning liquid receiving portion for receiving the cleaning liquid supplied to the hub of the screw conveyor; A washing nozzle for ejecting a washing liquid in the section toward the screen section,

前記洗浄液受け部内に、 前記スク リューコンペャのフライ ト外周縁と 前記スクリーン部内周面との間の隙間に生じる残層処理物を洗浄する洗 浄液を受け入れる残層用洗浄液受け部を、 前記洗浄液受け部内とは独立 に区画して設け、 In the cleaning liquid receiving portion, a cleaning process is performed for cleaning a residual layer processed product generated in a gap between the outer peripheral edge of the screw of the screw conveyor and the inner peripheral surface of the screen portion. A cleaning liquid receiving section for the remaining layer that receives the cleaning liquid is provided separately from the inside of the cleaning liquid receiving section,

前記フライ トの内周縁が連なる位置にて、 フライ トのらせん方向に沿 つて所定間隔おきに、 前記残層用洗浄液受け部の底側に接続管を設ける と共に、 前記スクリューコンペャのハブないしフライ ト内部に、 ハブ内 周側よりフライ ト外周縁にかけて放射方向に延びて前記接続管が連通す る洗浄液排出孔を設け、 ·  A connecting pipe is provided at a position where the inner peripheral edge of the fly is continuous at predetermined intervals along a spiral direction of the fly, at a bottom side of the residual layer cleaning liquid receiving portion, and a hub or fly of the screw conveyor is provided. A cleaning liquid discharge hole extending radially from the inner peripheral side of the hub to the outer peripheral edge of the fly and communicating with the connection pipe,

前記残層用洗浄液受け部内の洗浄液を、 前記フライ ト外周縁に開口す る前記各洗浄液排出孔の先端口より、 前記残層処理物に向けて直接噴出 させることを特徴とする遠心分離機。  A centrifugal separator characterized in that the cleaning liquid in the cleaning liquid receiving portion for the residual layer is jetted directly from the front end of each of the cleaning liquid discharge holes opened in the outer peripheral edge of the cleaning liquid toward the residual layer processing object.

[ 3 ] ボウル内にスク リ ューコンペャを備え、 これらを相対的に回転可 能に支持してなり、 前記ボウル内に供給した原液から処理物を分離する と共に、 該ポウルの一端側の内周面に沿って設けたスク リーン部で、 前 記処理物の洗浄およぴ脱液を行う遠心分離機において、 前記スクリュー コンペャのハプに、 その内部に供給した洗浄液を受け入れる洗浄液受け 部と、 該洗浄液受け部内の洗浄液を前記スクリーン部に向かって噴出す る洗浄ノズルとを有する遠心分離機であって、  [3] A screw conveyor is provided in the bowl, and these are relatively rotatably supported. The processed material is separated from the stock solution supplied into the bowl, and the inner peripheral surface at one end of the powl is provided. A centrifugal separator for washing and dewatering the processed material in a screen section provided along the line, wherein a cleaning liquid receiving section for receiving the cleaning liquid supplied into the hap of the screw conveyer; A centrifugal separator having a cleaning nozzle for ejecting a cleaning liquid in a receiving portion toward the screen portion,

前記洗浄液受け部内に、 前記スクリユーコンべャのフライ ト外周縁と 前記スクリーン部内周面との間の隙間に生じる残層処理物を洗浄する洗 浄液を受け入れる残層用洗浄液受け部を、 前記洗浄液受け部内とは独立 に区画して設け、  In the cleaning liquid receiving portion, a residual layer cleaning liquid receiving portion for receiving a cleaning liquid for cleaning a residual layer processed product generated in a gap between an outer peripheral edge of the screw conveyor and an inner peripheral surface of the screen portion is provided. It is provided separately from the inside of the washing liquid receiving section,

前記フライ トの処理物搬送面と反対側の面に隣接する位置にて、 前記 フライ トのらせん方向に沿って所定間隔おきに、 前記残層用洗浄液受け 部の底側に接続管を設けると共に、 前記スクリユーコンべャのハプに前 記接続管が連通する洗浄液連通孔を設け、  A connection pipe is provided at a position adjacent to a surface of the fly opposite to the processed material transfer surface, at predetermined intervals along a spiral direction of the fly, at a bottom side of the residual layer cleaning liquid receiver, and Providing a washing liquid communication hole through which the connection pipe communicates with the haptic of the screw conveyor;

前記フライ トの反対側の面に、 フライ トのらせん方向に沿って所定間 隔おきに、 フライ トの内周縁より外周縁にかけて放射方向に延びて前記 洗浄液連通孔が連通する洗浄液排出パイプを取り付け、 A predetermined distance along the spiral direction of the flight At intervals, a cleaning liquid discharge pipe extending radially from the inner peripheral edge to the outer peripheral edge of the flight and communicating with the cleaning liquid communication hole is attached,

前記残層用洗浄液受け部内の洗浄液を、 前記洗浄液排出パイプの先端 口より、 前記残層処理物に向けて直接嘖出させること'を特徴とする遠心 分離機。 - A centrifugal separator, wherein the cleaning liquid in the cleaning liquid receiving portion for the residual layer is directly discharged from the distal end of the cleaning liquid discharge pipe toward the residual layer processed material. -

[ 4 ] 前記フライ ト外周縁の先端面に、 フライ トのらせん方向に連続し て延び、 前記各洗浄液排出孔の先端口が連通する溝を形成したことを特 徴とする , [ 2 ] 記載の遠心分離機。 [4] The method according to [2], wherein a groove extending continuously in a spiral direction of the fly and formed in a distal end surface of the outer peripheral edge of the fly and communicating with a distal end of each of the cleaning liquid discharge holes is formed. Centrifuge.

[ 5 ] 前記スクリューコンペャのハブ内部に、 その軸方向に延びる原液 供給用のフィードチューブを揷入し、  [5] A feed tube for supplying a stock solution extending in the axial direction is inserted into the inside of the hub of the screw conveyor.

前記フィードチューブ内に、 前記洗浄液受け部に洗浄液を供給する洗 浄液供給経路を形成すると共に、 前記洗浄液受け部に対して半径方向に 重なるフィードチューブの途中に前記洗浄液供給経路の開放口を設け、 前記フィードチューブ内に、 前記残層用洗浄液受け部に洗浄液を供給 する残層用洗浄液供給経路を形成すると共に、 前記残層用洗浄液受け部 に対して半径方向に重なるフィ一ドチューブの途中に前記残層用洗浄液 供給経路の開放口を設けたことを特徴とする [ 1 ] > . [ 2 ] , [ 3 ] ま たは [ 4 ] 記載の遠心分離機。  A cleaning liquid supply path for supplying a cleaning liquid to the cleaning liquid receiving section is formed in the feed tube, and an opening for the cleaning liquid supply path is provided in the middle of the feed tube overlapping the cleaning liquid receiving section in the radial direction. In the feed tube, a residual layer cleaning liquid supply path for supplying the residual layer cleaning liquid to the residual layer cleaning liquid receiving part is formed, and in the middle of a feed tube radially overlapping the residual layer cleaning liquid receiving part. The centrifuge according to [1], [2], [3], or [4], wherein an opening for the supply path of the residual layer cleaning liquid is provided.

次に本発明の作用を説明する。  Next, the operation of the present invention will be described.

前記 [ 1 ] に記載の遠心分離機によれば、 ポウル内に原液が供給され ると、 遠心力によりボウル内で原液が処理物と母液とに分けられ、 処理 物はボウルの内周面に沈降し、 かかる処理物は、 ボウルと回転差を与え られているスク リ ューコンペャにより搬送される。 ただし、 スク リ ュー コンペャのフライ ト外周縁とスク リ ーン部内周面との間に形成される半 径方向の隙間では、 処理物はコンペャで十分には搬送されず残層をなす c 搬送途中で脱液された処理物は、 一般にその製造過程で生じた不純物 や母液そのものを表面に付着させており、 これら余分な付着物を洗浄す るために、 ボウルの一端側の内周面に沿って設けたスクリーン部におい て、 スクリユーコンべャのハブにある洗浄ノズルより処理物に向かって 洗浄液を噴出して洗浄を行う。 ここでの洗浄液は、 例えば、 ボウル内に 原液を供給するフィードチューブ中に別途設けた洗浄液供給経路を介し て、 前記ハプ内にある洗浄液受け部に供給される。 According to the centrifuge described in the above [1], when the stock solution is supplied into the powl, the stock solution is separated into a processed product and a mother liquor in the bowl by centrifugal force, and the processed product is formed on the inner peripheral surface of the bowl. The settled material is conveyed by a screw conveyor provided with a rotation difference from the bowl. However, in the radial gap formed between the outer peripheral edge of the screw of the screw conveyor and the inner peripheral surface of the screen part, the processed material is not sufficiently transported by the conveyor, and is c transported as the remaining layer. Processed material that has been drained on the way is generally free from impurities generated during the manufacturing process. And the mother liquor itself are adhered to the surface, and in order to wash out these extraneous substances, a screen provided along the inner peripheral surface at one end of the bowl is used to clean the screen at the hub of the screw conveyor. Cleaning is performed by spraying the cleaning liquid from the nozzle toward the processing object. The cleaning liquid here is supplied to the cleaning liquid receiving section in the haptic via a cleaning liquid supply path separately provided in a feed tube for supplying the undiluted liquid into the bowl.

前記洗浄液受け部内には、 前記処理物の残層を洗浄する洗浄液を受け 入れる残層用洗浄液受け部が、 洗浄液受け部内とは独立に区画して設け られており、 この残層用洗浄液受け部に供給された洗浄液は、 フライ ト のらせん方向に沿って設けられた残層用洗浄経路により、 前記洗浄液受 け部とは仕切られた状態でフライ ト外周縁より残層処理物に向けて直接 噴出される。 それにより、 洗浄ノズルによる処理物の洗浄と、 残層用洗 浄経路による残層処理物の洗浄を別々に行うことができ、 それぞれの洗 浄液の種類や液量を互いに異ならせることもできる。  In the cleaning liquid receiving portion, a remaining layer cleaning liquid receiving portion for receiving a cleaning liquid for cleaning the remaining layer of the processed material is provided separately from the cleaning liquid receiving portion, and the remaining layer cleaning liquid receiving portion is provided. The cleaning liquid supplied to the filter is separated from the cleaning liquid receiving portion by the residual layer cleaning path provided along the spiral direction of the fly, and directly from the outer peripheral edge of the fly toward the residual layer processing object. It is gushing. As a result, it is possible to separately perform the cleaning of the processed material by the cleaning nozzle and the cleaning of the residual layer processed material by the cleaning path for the residual layer, so that the type and amount of the cleaning liquid can be different from each other. .

このように、 処理物全体とは別に、 前記スクリューコンペャのフライ ト外周縁と前記スク リーン部内周面との間の隙間に生じた残層処理物を 特に直接洗浄することができるので、 残層処理物の固着がなくなり移動 性も高まり、 搬送中の処理物全体に対する洗浄液の透過性も向上する。 従って、 スクリーン部における処理物の目詰まりを未然に防ぐことがで きると共に、 本来の処理物中の不純物の置換用としての洗浄液量を抑制 することが可能になり、 スク リーン部における処理物の目漏れ量を減少 させることが可能となる。  As described above, separately from the entire processed material, the residual layer processed material generated in the gap between the outer peripheral edge of the screw conveyor and the inner peripheral surface of the screen portion can be particularly directly cleaned, so that the residual layer can be cleaned. This eliminates sticking of the layer processing material, improves mobility, and improves the permeability of the cleaning liquid to the entire processing material being transported. Therefore, clogging of the processed material in the screen portion can be prevented beforehand, and the amount of the cleaning liquid for replacing impurities in the original processed material can be suppressed. The amount of eye leakage can be reduced.

また、 前記 [ 2 ] に記載の遠心分離機によれば、 前記残層用洗浄液受 け部内の洗浄液は、 前記フライ トの内周縁が連なる位置にて、 フライ ト のらせん方向に沿って所定間隔おきに設けられている接続管を通り、 前 記スク リユーコンべャのハブないしフライ ト内部に設けられている洗浄 液排出孔からボウル内に飛び出す。 洗浄液排出孔は、 ハブ内周側よりフ ライ ト外周縁にかけて放射方向に延ぴており、 フライ ト外周縁に開口す る前記各洗浄液排出孔の先端口より、 前記残層処理物に向けて洗浄液を 直接噴出させることができる。 Further, according to the centrifuge described in the above [2], the cleaning liquid in the residual layer cleaning liquid receiving portion is provided at a predetermined interval along a spiral direction of the fly at a position where the inner peripheral edge of the fly is continuous. Washing provided inside the hub or flight of the screw conveyor through the connection pipes provided every other Jump out into the bowl from the liquid discharge hole. The cleaning liquid discharge holes radially extend from the inner peripheral side of the hub to the outer peripheral edge of the fly, and are directed toward the residual layer processing object from the front end openings of the respective cleaning liquid discharge holes that open to the outer peripheral edges of the fly. The cleaning liquid can be ejected directly.

ここで前記 [ 4 ] に記載の遠心分離機のように、 前記フライ ト外周縁 の先端面に、 フライ トのらせん方向に連続して延び、 前記各洗浄液排出 孔の先端口が連通する溝を形成すれば、 前記各洗浄液排出孔の先端口よ り出る洗浄液は溝に沿ってフライ ト外周縁の全域に行き渡り、 前記残層 処理物に向けて半径方向の全周に広がるように直接噴出させることがで さる。  Here, as in the centrifugal separator according to the above [4], a groove extending continuously in the spiral direction of the fly and communicating with the distal end port of each of the washing liquid discharge holes is formed on the distal end surface of the outer peripheral edge of the fly. If formed, the cleaning liquid discharged from the tip end of each cleaning liquid discharge hole spreads over the entire outer peripheral edge of the fly along the groove, and is directly jetted toward the remaining layer processing material so as to spread over the entire circumference in the radial direction. That's a thing.

また、 前記 [ 3 ] に記載の遠心分離機によれば、 前記残層用洗浄液受 け部内の洗浄液は、 前記フライ トの処理物搬送面と反対側の面に隣接す る位置にて、 フライ トのらせん方向に沿って所定間隔おきに設けられて いる接続管と、 前記スクリユーコンべャのハブに設けられている洗浄液 連通孔どを通り、 前記フライ トの反対側の面に、 フライ トのらせん方向 に沿って所定間隔おきに設けられている洗浄液排出パイプに導入される 各洗浄液排出パイプは、 フライ トの内周縁より外周縁にかけて放射方 向に延びており、 フライ ト外周縁に沿った各洗浄液排出パイプの先端口 より、 前記残層処理物に向けて洗浄液を直接噴出させることができる。 このような構成によれば、 フライ ト自体に孔を設ける加工は不要となり 洗浄液排出パイプをフライ トに後付けすることができ、 比較的容易に製 作することができる。 .  Further, according to the centrifuge described in the above [3], the cleaning liquid in the residual layer cleaning liquid receiving portion is subjected to a frying operation at a position adjacent to a surface of the freight opposite to a processing object transport surface. Through the connecting pipes provided at predetermined intervals along the spiral direction of the nozzle and the cleaning liquid communication holes provided in the hub of the screw conveyor, and to the face on the opposite side of the flight, The cleaning liquid discharge pipes that are introduced into the cleaning liquid discharge pipes provided at predetermined intervals along the spiral direction extend radially from the inner peripheral edge to the outer peripheral edge of the fly, and extend along the outer peripheral edge of the fly. The cleaning liquid can be jetted directly from the tip end of each of the cleaning liquid discharge pipes toward the residual layer processed material. According to such a configuration, it is not necessary to provide a hole in the fly itself, and the cleaning liquid discharge pipe can be retrofitted to the fly, so that the manufacture can be performed relatively easily. .

さらにまた、 前記スグリユーコンべャのハプ内にある前記洗浄液受け 部と前記残層用洗浄液受け部とに洗浄液を供給するには、 前記 [ 5 ] に 記載したように、 同じくハブ内に揷入する原液供給用のフィードチュー プの一部を有効に利用することができる。 すなおち、 フィードチューブ内に、 前記洗浄液受け部に洗浄液を供給 する洗浄液供給経路を形成し、 前記洗浄液受け部に対して半径方向に重 なるフィードチューブの途中に洗浄液供給経路の開放口を設ける。 Furthermore, in order to supply the cleaning liquid to the cleaning liquid receiving portion and the residual layer cleaning liquid receiving portion in the haptic of the squirrel conveyor, as described in the above [5], the cleaning liquid is similarly introduced into the hub. A part of the feed tube for supplying the undiluted solution can be effectively used. In other words, a cleaning liquid supply path for supplying the cleaning liquid to the cleaning liquid receiving section is formed in the feed tube, and an opening for the cleaning liquid supply path is provided in the middle of the feed tube overlapping the cleaning liquid receiving section in the radial direction.

同様にフィードチューブ内に、 前記残層用洗浄液受け部に洗浄液を供 給する残層用洗浄液供給経路を形成し、 前記残層用洗浄液受け部に対し て半径方向に重なるフィ一ドチューブの途中に残層用洗浄液供給経路の 開放口を設ければ、 洗浄液受け部および残層用洗浄液受け部に対して、 別々に洗浄液を効率よく供給することが可能となる。 図面の簡単な説明  Similarly, a residual layer cleaning liquid supply path for supplying the residual layer cleaning liquid to the residual layer cleaning liquid receiving section is formed in the feed tube, and in the middle of a feed tube radially overlapping the residual layer cleaning liquid receiving section. By providing an opening for the residual layer cleaning liquid supply path, it is possible to efficiently supply the cleaning liquid separately to the cleaning liquid receiving section and the residual layer cleaning liquid receiving section. BRIEF DESCRIPTION OF THE FIGURES

図 1は、 本発明の第 1実施の形態に係る遠心分離機の要部を示す縦断 面図である。  FIG. 1 is a longitudinal sectional view showing a main part of a centrifuge according to a first embodiment of the present invention.

図 2は、 本発明の第 1実施の形態に係る遠心分離機の全体を示す縦断 面図である。  FIG. 2 is a longitudinal sectional view showing the whole of the centrifuge according to the first embodiment of the present invention.

図 3は、 図 1の III一 III線断面図である。  FIG. 3 is a sectional view taken along line III-III in FIG.

図 4は、 本発明の第 2実施の形態に係る遠心分離機の要部を示す縦断 面図である。  FIG. 4 is a longitudinal sectional view showing a main part of a centrifuge according to a second embodiment of the present invention.

図 5は、 本発明の第 2実施の形態に係る遠心分離機の要部を拡大して 示す縦断面図である。  FIG. 5 is an enlarged longitudinal sectional view showing a main part of a centrifuge according to a second embodiment of the present invention.

図 6は、 図 4の VI— VI線断面図である。  FIG. 6 is a sectional view taken along line VI-VI of FIG.

図 7は、 本発明の第 3実施の形態に係る遠心分離機の要部を示す縦断 面図である。  FIG. 7 is a longitudinal sectional view showing a main part of a centrifuge according to a third embodiment of the present invention.

図 8は、 図 7の VII I— VI I I線断面図である。 発明を実施するための最良の形態  FIG. 8 is a cross-sectional view taken along the line VIII-VIII of FIG. BEST MODE FOR CARRYING OUT THE INVENTION

以下、 図面に基づき本発明を代表する各種の実施の形態を説明する。 図 1〜図 3は本発明の第 1実施の形態を示している。 Hereinafter, various embodiments representing the present invention will be described with reference to the drawings. 1 to 3 show a first embodiment of the present invention.

本実施の形態に係る遠心分離機 1 0は、 スク リーンボウル型遠心分離 機と称されるものであり、 '略円筒型のボウル 2 0内にスク リ ユーコンべ ャ 4 0を備え、 これらを相対的に回転可能に支持してなり、 前記ボウル 2 0内に供給される原液から処理対象である処理物と母液を別々に分離 することができるように構成されている。  The centrifugal separator 10 according to the present embodiment is called a screen bowl type centrifugal separator, and is provided with a screw conveyor 40 in a substantially cylindrical bowl 20. It is supported so as to be relatively rotatable, and is configured such that a processed material to be processed and a mother liquor can be separately separated from a stock solution supplied into the bowl 20.

ここで処理物とは、 化学工業や食品工業の分野における各種結晶等が 該当し、 具体的には例えば、 ペッ トボトルやポリエステル繊維の原料と なるテレフタル酸、 テレフタル酸の原料となるパラキシレン、 C D— R O Mの原料となるビスフエノール、 その他、 化学調味,料の原料となるグ ルタミンソーダ等が該当する。 また母液には各種の溶媒が該当する。 各 種結晶は、 その製造過程において未重合物質ゃスラリ一を構成する溶媒 を結晶表面に付着しており、 これらの付着物は洗浄液 (特定の別な溶媒 等) により洗浄置換することができる。 以下、 処理物として結晶に適用 した場合を例に説明する。  Here, the processed material corresponds to various crystals in the fields of the chemical industry and the food industry, and specifically, for example, terephthalic acid as a raw material for pet bottles and polyester fibers, paraxylene as a raw material for terephthalic acid, and CD. — Bisphenol, which is a raw material for ROM, and glutamine soda, which is a raw material for chemical seasonings and ingredients. Various solvents correspond to the mother liquor. Each seed crystal has a solvent constituting an unpolymerized substance slurry adhered to the crystal surface during the manufacturing process, and these adhered substances can be washed and replaced with a washing liquid (a specific other solvent or the like). Hereinafter, an example in which the present invention is applied to a crystal as a processed material will be described.

図 2に示すように、 ボウル 2 0とその内部のスクリユーコンべャ 4 0 は、 ケーシング 1 1 の内部にシャフト 1 2 a , 1 2 bを介して回転可能 に軸支されている。 ポウル 2 0およびスク リ ューコンペャ 4 0は、 片側 の軸受け 1 3に連設.された差動装置 1 4によって微少差速で回転駆動さ れる。 かかる差動装置 1 4自体は公知であり詳細な説明は省略する。 ケーシング 1 1 の内部は、 次述するボウル 2 0に設けられている排出 口 2 4、 スク リーン部 3 0、 ダム部 2 6等にそれぞれ対応するように区 画されている。 そして、 ケーシング 1 1 の下部には、 前記排出口 2 4に 連通する結晶排出口 1 5、 前記スクリーン部 3 0に連通する洗浄液排出 口 1 6、 前記ダム部 2 6に連通する母液排出口 1 7がそれぞれ設けられ ている。 ボウル 2 0の一端側 (図 2中で右側) が結晶の排出方向となっており ポウル 2 0の他端側 (図 2中で左側) から順に、 大径の平行'筒部 2 1 と 一端側に向かって内径が漸次縮小するテーパー部 2 2と、 小径の平行筒 部 2 3とに区分けされている。 小径の平行筒部 2 3の先端側には、 結晶 の排出口 2 4が開設され、 大径の平行筒部 2 1の先端側にほ、 ボウル 2 0の半径方向の液深を規制すると共に、 結晶を分離した母液をボウル 2 0外へ排出可能なダム部 2 6が設けられている。 As shown in FIG. 2, the bowl 20 and the screw conveyor 40 therein are rotatably supported inside the casing 11 via shafts 12a and 12b. The powl 20 and the screw conveyor 40 are rotationally driven at a slight differential speed by a differential device 14 connected to a bearing 13 on one side. Such a differential device 14 itself is publicly known, and a detailed description thereof will be omitted. The interior of the casing 11 is partitioned so as to correspond to a discharge port 24, a screen portion 30, a dam portion 26, and the like provided in a bowl 20 described below. A crystal discharge port 15 communicating with the discharge port 24, a cleaning liquid discharge port 16 communicating with the screen section 30, and a mother liquid discharge port 1 communicating with the dam section 26 are provided at a lower portion of the casing 11. 7 are provided respectively. One end side of the bowl 20 (right side in Fig. 2) is the direction of crystal discharge, and from the other end side of the pole 20 (left side in Fig. 2), in order from the large-diameter parallel 'cylindrical part 21 and one end. It is divided into a tapered portion 22 whose inner diameter gradually decreases toward the side, and a small-diameter parallel tube portion 23. At the distal end of the small-diameter parallel cylindrical portion 23, a crystal discharge port 24 is opened, and near the distal end of the large-diameter parallel cylindrical portion 21, the liquid depth in the radial direction of the bowl 20 is regulated. A dam 26 is provided which can discharge the mother liquor from which the crystals have been separated out of the bowl 20.

図 1に示すように、 小径の平行筒部 2 3は、 その壁面に多数の濾液排 出孔 2 5が形成され、 内周側が円筒状の濾材 3 1で全周方向に覆われて スク リーン部 3 0をなしている。 濾液排出孔 2 5の大きさは、 結晶の粒 子径をさほど考慮する必要はないが、 濾材 3 1は、 結晶の粒子径より小 径サイズの多数の微小孔ないしスリ ッ トを有する素材から成る。 具体的 には例えば、 ゥヱッジワイヤースクリーンゃ多孔質セラミック成形体等 を用いるとよい。 なお、 平行筒部 2 3の内周面は濾材 3 1 の厚さ分だけ 表面が削られている。  As shown in Fig. 1, the small-diameter parallel cylindrical portion 23 has a large number of filtrate discharge holes 25 formed on the wall surface, and the inner peripheral side is covered with a cylindrical filter medium 31 in the entire circumferential direction, and the screen is screened. Part 30. The size of the filtrate discharge hole 25 does not need to be considered so much in terms of the crystal particle diameter.However, the filter medium 31 is made of a material having a large number of micropores or slits whose diameter is smaller than the crystal particle diameter. Become. Specifically, for example, edge wire screens, porous ceramic moldings, and the like may be used. The inner peripheral surface of the parallel cylindrical portion 23 is shaved by the thickness of the filter medium 31.

スクリユーコンべャ 4 0は、 その回転軸となるハブ 4 1 と、 該ハブ 4 1の外周にスクリユー状に設けられるフライ ト 4 2とからなり、 フライ ト 4 2は、 結晶をボウル 2 0の一端側 (図 2中で右側) へ搬送するよう に形成されている。 なお、 フライ ト 4 2の外周縁と平行筒部 2 3の内周 面 (スク リーン部 3 0の濾材 3 1表面) との間には、 スク リ ューコンペ ャ 4 0とボウル 2 0とが異なる速度で回転する構造上、 半径方向に隙間 が生じるように設定されている。  The screw conveyor 40 includes a hub 41 serving as a rotating shaft thereof, and a fly 42 provided in a screw-shape on the outer periphery of the hub 41. The fly 42 holds crystals in a bowl 20. It is formed so as to be conveyed to one end (right side in Fig. 2). The screw conveyor 40 and the bowl 20 are different between the outer peripheral edge of the fly 42 and the inner peripheral surface of the parallel tubular portion 23 (the surface of the filter medium 31 of the screen portion 30). Due to the structure that rotates at the speed, it is set so that there is a gap in the radial direction.

ハブ 4 1には、 その内部に供給された洗浄液を受け入れる洗浄液受け 部 4 3と、 該洗浄液受け部 4 3内の洗浄液を前記ボウル 2 0のスクリー ン部 3 0に向かって噴出する洗浄ノズル 4 5 とが設けられている。 洗浄 液受け部 4 3は、 ハブ 4 1の内周面の全周方向に!:り軸心方向に所定幅 に延出する仕切りで囲まれた部位からなる。 The hub 41 has a cleaning liquid receiving portion 43 for receiving the cleaning liquid supplied therein, and a cleaning nozzle 4 for jetting the cleaning liquid in the cleaning liquid receiving portion 43 toward the screen portion 30 of the bowl 20. 5 is provided. The cleaning liquid receiving section 43 is located in the entire circumferential direction of the inner peripheral surface of the hub 41! : Specified width in the direction of the beam axis It consists of a part surrounded by a partition that extends to

洗浄液受け部 4 3の底側となるハプ 4 1の周壁には、 所定間隔おきに 洗浄液連通孔 4 4が設けられ、 ハプ 4 1の外周面側に、 前記洗浄液連通 孔 4 4に連通する洗浄ノズル 4 5が突設されている。 ここで洗浄ノズル 4 5は、 図 1に示すようにフライ ト 4 2のピッチ中央よりやや他端側 ( 図 1中で左側) で、 スク リーン部 3 0を半径方向に臨む位置に配されて いる。  A cleaning liquid communication hole 44 is provided at predetermined intervals on a peripheral wall of the hap 41, which is a bottom side of the cleaning liquid receiving portion 43, and a cleaning communicating with the cleaning liquid communication hole 44 is provided on an outer peripheral surface side of the hap 41. Nozzles 45 are provided. Here, the cleaning nozzle 45 is arranged at a position slightly opposite to the center of the pitch of the fly 42 as shown in FIG. 1 (left side in FIG. 1) and facing the screen portion 30 in the radial direction. I have.

さらに洗浄液受け部 4 3内には、 フライ ト 4 2外周縁とスクリーン部 3 0内周面との間の隙間に生じる残層結晶を洗浄する洗浄液を受け入れ る残層用洗浄液受け部 4 6が、 洗浄液受け部 4 3内とは独立に区画して 設けられている。 残層用洗浄液受け部 4 6は、 円筒部材の両端に全周方 向に亘り軸心方向に所定幅に延出する仕切りを設けてなり、 その底側に は、 所定間隔おきに接続管 4 7が突設され、 各接続管 4 7によって残層 用洗浄液受け部 4 6は、 前記洗浄液受け部 4 3内にてハブ 4 1の内周面 より離隔した状態に固設されている。 図 1に示すように各接続管 4 7は. 前記フライ ト 4 2の内周縁が連なる位置にて、 フライ ト 4 2のらせん方 向に沿つて所定間隔おきに配されている。  Further, in the cleaning liquid receiving section 43, a residual layer cleaning liquid receiving section 46 for receiving a cleaning liquid for cleaning residual layer crystals generated in a gap between the outer peripheral edge of the fly 42 and the inner peripheral surface of the screen section 30 is provided. It is provided separately from the inside of the washing liquid receiving section 43. The residual layer cleaning liquid receiving part 46 is provided with a partition extending at a predetermined width in the axial direction over the entire circumferential direction at both ends of the cylindrical member. 7 is provided so as to protrude, and the cleaning liquid receiving portion 46 for the remaining layer is fixed by the respective connection pipes 47 so as to be separated from the inner peripheral surface of the hub 41 in the cleaning liquid receiving portion 43. As shown in FIG. 1, the connection pipes 47 are arranged at predetermined intervals along the spiral direction of the fly 42 at a position where the inner peripheral edge of the fly 42 is continuous.

本実施の形態では、 スクリューコンべャ 4 0におけるフライ ト 4 2の 内周縁が連なる位置にて、 ハプ 4 1ないしフライ ト 4 2内部に、 ハブ 4 1内周側よりフライ ト 4 2外周縁にかけて放射方向に延びて、 前記各接 続管 4 7が連通する複数の洗浄液排出孔 4 9が設けられている。 各洗浄 液排出孔 4 9は各接続管 4 7と共に、 前記残層用洗浄液受け部 4 6内の 洗浄液を、 前記洗浄液受け部 4 3 とは仕切られた状態でフライ ト 4 2外 周縁よりスク リーン部 3 0上の残層結晶に向けて直接噴出させる残層用 洗浄経路をなしている。  In the present embodiment, at the position where the inner peripheral edge of the fly 42 in the screw conveyor 40 is continuous, inside the hap 41 or the fly 42, the outer peripheral edge of the fly 42 from the inner peripheral side of the hub 41. A plurality of cleaning liquid discharge holes 49 are provided extending in the radial direction to communicate with the connection pipes 47. The cleaning liquid discharge holes 49 together with the connection pipes 47 are used to transfer the cleaning liquid in the residual layer cleaning liquid receiving section 46 from the outer periphery of the fly 42 while being separated from the cleaning liquid receiving section 43. It forms a cleaning path for the residual layer that is jetted directly toward the residual layer crystal on the lean part 30.

ハブ 4 1の内部には、 その軸方向に延びる原液供給用のフィ一ドチュ ーブ 6 0が揷入されている。 フィードチューブ 6 0の始端は、 ハブ 4 1 やボウル 2 0より外部に延出し原液供給口 6 1 となり、 フィードチュー ブ 6 0の終端は、 ハブ 4 1内部の略中央に配されて原液出口 6 2となる, さらにフィードチューブ 6 0内に、 前記洗浄液受け部 4 3に洗浄液を供 給する洗浄液供給経路をなす洗浄液供給管 7 1 と、 前記残層用洗浄液受 け部 4 6に洗浄液を供給する残層用洗浄液供給経路をなす残層用洗浄液 供給管 7 2とが挿入されている。 Inside the hub 41, a feed tube for supplying a stock solution extending in the axial direction is provided. Move 60 has been purchased. The starting end of the feed tube 60 extends outside from the hub 41 and the bowl 20 to become a stock solution supply port 61, and the end of the feed tube 60 is arranged substantially in the center of the hub 41 and has a stock solution outlet 6. The cleaning liquid is supplied to the cleaning liquid supply pipe 71 for supplying the cleaning liquid to the cleaning liquid receiving section 43 in the feed tube 60 and the cleaning liquid receiving section 46 for the residual layer. And a residual layer cleaning liquid supply pipe 72 forming a residual layer cleaning liquid supply path.

洗浄液供給管 7 1の始端は、 フィードチューブ 6 0の始端側にて軸方 向と略直角に開口する洗浄液供給口 7 1 aをなしている。 また、 ハブ 4 1内において洗浄液受け部 4 3に対して半径方向に重なるフィードチュ ーブ 6 0の途中には、 洗浄液供給管 7 1 の開放口 7 1 bが軸方向と略直 角に開口している。 一方、 残層用洗浄液供給管 7 2の始端は、 フィード チューブ 6 0の始端側にて軸方向と略直角に開口する残層用洗浄液供給 口 7 2 aをなしている。 また、 ハブ 4 1内において残層用洗浄液受け部 4 6に対して半径方向に重なるフィードチューブ 6 0の途中には、 残層 用洗浄液供給管 7 2の開放口 7 2 bが軸方向と略直角に開口している。 次に、 第 1実施の形態に係る遠心分離機 1 0の作用を説明する。  The starting end of the cleaning liquid supply pipe 71 forms a cleaning liquid supply port 71 a that opens substantially perpendicularly to the axial direction on the starting end side of the feed tube 60. Also, in the middle of the feed tube 60 radially overlapping the cleaning liquid receiving portion 43 in the hub 41, an opening 71b of the cleaning liquid supply pipe 71 is opened substantially at right angles to the axial direction. are doing. On the other hand, the beginning of the residual-layer cleaning liquid supply pipe 72 forms a residual-layer cleaning liquid supply port 72 a that opens substantially perpendicularly to the axial direction on the start end side of the feed tube 60. Also, in the middle of the feed tube 60 radially overlapping the cleaning liquid receiving portion 46 for the residual layer in the hub 41, an opening 72b of the cleaning liquid supply pipe 72 for the residual layer is substantially in the axial direction. It opens at right angles. Next, the operation of the centrifuge 10 according to the first embodiment will be described.

図 1 , 図 2において、 原液はフィードチューブ 6 0を介して、 ポンプ 等の駆動源を用いてボウル 2 0内へ供給される。 フィードチューブ 6 0 の原液供給口 6 1から送られた原液は、 スク リ ューコンペャ 4 0のハブ In FIGS. 1 and 2, the stock solution is supplied into the bowl 20 via a feed tube 60 using a drive source such as a pump. The undiluted solution sent from the undiluted solution supply port 61 of the feed tube 60 is transferred to the hub of the screw compressor 40.

4 1内の略中央付近に位置する原液出口 6 2から出て、 ボウル 2 0内の ダム部 2 6で予め設定した所定の深さまで張り込まれる。 原液はボウルThe solution exits from a stock solution outlet 62 located in the vicinity of the center in 41 and is inserted into a dam portion 26 in a bowl 20 to a predetermined depth set in advance. Stock solution is bowl

2 0内で遠心力の作用を受けて、 母液から結晶が沈降分離される。 Under the effect of centrifugal force within 20, the crystals are settled and separated from the mother liquor.

遠心力の作用によりボウル 2 0の内周面側へ沈降した結晶は、 ボウル 2 0と微少差速で回転するスク リユーコンべャ 4 0のフライ ト 4 2によ つて、 ポウル 2 0のテーパー部 2 2へ搬送され、 予めダム部 2 6で設定 されている液深よりも内径側へテーパー部 2 2の内周面上を移動する際 に脱液されて、 さらにスク リーン部 3 0へ搬送される。 The crystal that settles to the inner peripheral surface side of the bowl 20 due to the action of the centrifugal force is converted into the tapered portion of the powl 20 by the fly 42 of the screw conveyor 40 rotating at a slightly different speed from the bowl 20. Conveyed to 2 and set in advance in dam section 26 The liquid is removed when moving on the inner peripheral surface of the tapered portion 22 to the inner diameter side of the liquid depth, and is further conveyed to the screen portion 30.

搬送途中で脱液された結晶は、 その製造過程で生じた不純物や母液そ のものを表面に付着させており、 スク リーン部 3 0に至った結晶は、 ハ プ 4 1にある洗浄ノズル 4 5から噴出される洗浄液によって洗浄される: 洗浄液は、 一般に純水、 酢酸、 純フエノール、 硫酸、 塩酸等が用いられ. フィードチューブ 6 0に別途挿入してある洗浄液供給管 7 1を介して、 ハプ 4 1内にある洗浄液受け部 4 3に供給される。 洗浄液受け部 4 3に 受け入れられた洗浄液は、 ハブ 4 1周壁の洗浄液連通孔 4 4を通り洗浄 ノズル 4 5から噴出される。  Crystals that have been drained during transportation have impurities and mother liquor themselves generated during the manufacturing process attached to the surface, and crystals that have reached the screen part 30 have the cleaning nozzle 4 Washing is performed by the washing liquid ejected from 5: The washing liquid is generally pure water, acetic acid, pure phenol, sulfuric acid, hydrochloric acid, or the like. The washing liquid is supplied through the washing liquid supply pipe 71 inserted separately into the feed tube 60. The cleaning liquid is supplied to the cleaning liquid receiving part 43 in the hap 41. The cleaning liquid received in the cleaning liquid receiving part 43 is ejected from the cleaning nozzle 45 through the cleaning liquid communication hole 44 in the peripheral wall of the hub 41.

このようにスク リーン部 3 0で結晶は洗浄およぴ脱液作用を受け、 さ らに排出口 2 4側へ搬送されるが、 スク リ ユーコンべャ 4 0のフライ ト 4 2外周縁とスクリーン部 3 0内周面との間の隙間には結晶の残層が形 成される。 かかる残層結晶は、 残層用洗浄経路によって、 前記洗浄液受 け部 4 3 とは仕切られた状態でフライ ト 4 2外周縁から噴射される洗浄 液により直接的かつ局所的に洗浄される。 ここでの洗浄液は、 前記洗浄 ノズル 4 5から噴出させるものと同じ液を用いる場合が多く、 フィード チューブ 6 0に別途挿入してある残層用洗浄液供給管 7 2を介して、 ハ プ 4 1内にある残層用洗浄液受け部 4 6に供給される。  As described above, the crystal undergoes the washing and dewatering actions in the screen part 30 and is further conveyed to the discharge port 24 side, and the crystal is conveyed to the outer periphery of the fly 42 of the screen conveyor 40. A crystal residual layer is formed in the gap between the screen portion 30 and the inner peripheral surface. The residual layer crystal is directly and locally cleaned by the cleaning liquid sprayed from the outer periphery of the fly 42 in a state of being separated from the cleaning liquid receiving portion 43 by the residual layer cleaning path. In many cases, the cleaning liquid used here is the same as the liquid ejected from the cleaning nozzle 45. The cleaning liquid is supplied through the residual layer cleaning liquid supply pipe 72 separately inserted into the feed tube 60, and the haptic 4 1 It is supplied to the residual layer cleaning liquid receiving part 46 inside.

詳しく言えば、 残層用洗浄液受け部 4 6内の洗浄液は、 前記フライ ト 4 2の内周縁が連なる位置にて、 フライ ト 4 2のらせん方向に沿って所 定間隔おきに設けられている接続管 4 7を通り、 ハブ 4 1ないしフライ ト 4 2内部に設けられている洗浄液排出孔 4 9からボウル 2 0内に飛び 出す。 洗浄液排出孔 4 9は、 ハブ 4 1内周側よりフライ ト 4 2外周縁に かけて放射方向に延びており、 フライ ト 4 2外周縁に開口する各洗浄液 排出孔 4 9の先端口より、 残層結晶に向けて洗浄液を直接噴出させるこ とができる。 More specifically, the cleaning liquid in the residual layer cleaning liquid receiving portion 46 is provided at predetermined intervals along the spiral direction of the fly 42 at a position where the inner peripheral edge of the fly 42 is continuous. It passes through the connecting pipe 47 and jumps out into the bowl 20 from the washing liquid discharge hole 49 provided inside the hub 41 or the fly 42. The cleaning liquid discharge holes 49 extend radially from the inner peripheral side of the hub 4 1 to the outer peripheral edge of the fly 4 2. Do not spray the cleaning solution directly on the remaining crystal. Can be.

以上のように、 洗浄ノズル 4 5による結晶全体の洗浄とは別に、 残層 用洗浄経路により残層結晶を特に局所的かつ直接に洗浄することができ るので、 残層結晶の固着がなくなり移動性も高まり、 搬送中の結晶全体 に対する洗浄液の透過性も向上する。 そのため、 スク リーン部 3 0にお ける結晶の目詰まりを未然に防ぐことができると共に、 本来の結晶中の 不純物の置換用としての洗浄液量を抑制することが可能になり、 スク リ ーン部 3 0における結晶の目漏れ量を減少させることが可能となる。  As described above, apart from cleaning the entire crystal by the cleaning nozzle 45, the residual layer crystal can be particularly locally and directly cleaned by the residual layer cleaning path, so that the residual layer crystal is not fixed and moves. And the permeability of the cleaning solution to the entire crystal being transported is improved. Therefore, the clogging of the crystal in the screen part 30 can be prevented beforehand, and the amount of the cleaning liquid for replacing the original impurity in the crystal can be suppressed. It is possible to reduce the amount of crystal leakage at 30.

しかも、 洗浄液受け部 4 3 と残層用洗浄液受け部 4 6 とには、 互いに 仕切られた状態で別々に洗浄液が供給されるので、 洗浄ノズル 4 5から 噴出させる洗浄液の液量と、 残層用洗浄経路から噴出させる洗浄液の液 量とを外部より別々にコントロールすることができるため、 結晶洗浄の 置換率おょぴ目漏れ量の低減を図るための両方の最適な洗浄液液量の調 整を容易に行うことができる。 "  Moreover, since the cleaning liquid is supplied separately to the cleaning liquid receiving portion 43 and the cleaning liquid receiving portion 46 for the remaining layer while being separated from each other, the amount of the cleaning liquid ejected from the cleaning nozzle 45 and the amount of the remaining liquid Since the amount of the cleaning liquid spouted from the cleaning path can be separately controlled from the outside, adjustment of both the optimum cleaning liquid amount to reduce the replacement rate of crystal cleaning and the amount of leakage Can be easily performed. "

スク リーン部 3 0において、 洗浄ノズル 4 5およぴ残層用洗浄経路か ら噴出された洗浄液は、 結晶や残層結晶の洗浄後に濾材 3 1を通り濾液 棑出孔 2 5からボウル 2 ◦の外部へ排出される。 また、 スク リーン部 3 0で洗浄され脱液された結晶は、 排出口 2 4からボウル 2 0の外部に排 出され、 最後はケーシング 1 1にある結晶排出口 1 5から回収される。 図 4〜図 6は本発明の第 2実施の形態を示している。  In the screen part 30, the cleaning liquid ejected from the cleaning nozzle 45 and the residual layer cleaning path passes through the filter medium 31 after washing the crystals and residual layer crystals, and the filtrate is discharged from the discharge hole 25 to the bowl 2 °. Is discharged to the outside. Further, the crystals washed and drained in the screen section 30 are discharged from the discharge port 24 to the outside of the bowl 20, and finally collected from the crystal discharge port 15 in the casing 11. 4 to 6 show a second embodiment of the present invention.

本実施の形態に係る遠心分離機 1 O Aは、 前述した第 1実施の形態に おける前記フライ ト 4 2外周縁の先端面に、 該フライ ト 4 2のらせん方 向に連続して延び、 前記各洗浄液排出孔 4 9の先端口が連通する溝 4 9 aを形成したものである。 詳しくは例えば、 溝 4 9 aの巾は 1〜 5 m m 程度、 深さは 1 0〜 2 5 m m程度に設定するとよい。 なお、 第 1実施の 形態と同種の部位には同一符号を付して重複した説明を省略する。 このような第 2実施の形態によれば、 前記各洗浄液排出孔 4 9の先端 口より出る洗浄液は、 溝 4 9 aに沿ってフライ ト 4 2外周縁の全域に行 き渡り、 前記残層処理物に向けて半径方向の全周に広がるように直接嘖 出させることができる。 それにより、 前記各種実施の形態と同様に、 結 晶に対する洗浄液の透過性および残層結晶の移動性を高めることができ る。 The centrifuge 1 OA according to the present embodiment extends continuously to the tip end surface of the outer periphery of the fly 42 in the first embodiment described above in the spiral direction of the fly 42, A groove 49a is formed in which the tip end of each cleaning liquid discharge hole 49 communicates. For example, the width of the groove 49a may be set to about 1 to 5 mm, and the depth may be set to about 10 to 25 mm. The same parts as those in the first embodiment are denoted by the same reference numerals, and redundant description will be omitted. According to such a second embodiment, the cleaning liquid discharged from the tip end of each of the cleaning liquid discharge holes 49 spreads over the entire outer peripheral edge of the fly 42 along the groove 49a, and the remaining layer It can be directly extracted so as to spread all over the circumference in the radial direction toward the processing object. This makes it possible to enhance the permeability of the cleaning liquid to the crystals and the mobility of the remaining layer crystals, as in the above embodiments.

図 7および図 8は本発明の第 3実施の形態を示している。  7 and 8 show a third embodiment of the present invention.

本実施の形態に係る遠心分離機 1 0 Bは、 図 7に示すように、 前記残 層用洗浄液受け部 4 6の各接続管 4 7は、 前記フライ ト 4 2の処理物搬 送面 4 2 a と反対側の面 4 2 bに隣接する位置にて、 フライ ト 4 2のら せん方向に沿って所定間隔おきに配されており、 前記ハブ 4 1の周壁に は、 各接続管 4 7が連通する洗浄液連通孔 4 8が設けられている。  As shown in FIG. 7, the centrifugal separator 10 B according to the present embodiment includes a connection pipe 47 of the residual-layer washing liquid receiving section 46, and a processing object transport surface 4 of the fly 42. At the position adjacent to the surface 4 2b opposite to 2 a, they are arranged at predetermined intervals along the spiral direction of the fly 42, and the connecting pipe 4 is provided on the peripheral wall of the hub 41. A cleaning liquid communication hole 48 for communicating with 7 is provided.

そして、 スク リューコンべャ 4 0に けるフライ ト 4 2の処理物搬送 面 4 2 a と反対側の面 4 2 bには、 フライ ト 4 2のらせん方向に沿って 所定間隔おきに、 フライ ト 4 2の内周縁より外周縁にかけて放射方向に 延びて、 前記各洗浄液連通孔 4 8にそれぞれ連通する複数の洗浄液排出 パイプ 8 0が取り付けられている。 かかる洗浄液排出パイプ 8 0は、 接 続管 4 7や洗浄液連通孔 4 8と共に残層用洗浄経路をなしている。  The surface 42 b of the screw 42 on the opposite side of the processed material transfer surface 42 a of the fly 42 is arranged at predetermined intervals along the spiral direction of the fly 42. A plurality of cleaning liquid discharge pipes 80 extending radially from the inner peripheral edge to the outer peripheral edge of 42 and communicating with the respective cleaning liquid communication holes 48 are attached. The cleaning liquid discharge pipe 80 forms a residual layer cleaning path together with the connection pipe 47 and the cleaning liquid communication hole 48.

このような第 3実施の形態によればく 前記残層用洗浄液受け部 4 6内 の洗浄液は、 前記フライ ト 4 2の処理物搬送面 4 2 a と反対側の面 4 2 bに隣接する位置にて、 フライ ト 4 2のらせん方向に沿って所定間隔お きに設けられている接続管 4 7 と、 前記スク リユーコンべャ 4 0のハブ According to such a third embodiment, the cleaning liquid in the residual layer cleaning liquid receiving portion 46 is located at a position adjacent to the surface 42 b of the fly 42 opposite to the processing object transport surface 42 a. A connecting pipe 47 provided at a predetermined interval along a spiral direction of the fly 42, and a hub of the screw conveyor 40.

4 1に設けられている洗浄液連通孔 4 8 とを通り、 前記フライ ト 4 2の 反対側の面 4 2 bに、 フライ ト 4 2のらせん方向に沿って所定間隔おき に設けられている洗浄液排出パイプ 8 0に導入される。 The cleaning liquid provided at predetermined intervals along the spiral direction of the fly 42 on the surface 42b opposite to the fly 42 passing through the cleaning liquid communication hole 48 provided in 41. It is introduced into the discharge pipe 80.

各洗浄液排出パイプ 8 0は、 フライ ト 4 2の内周縁より外周縁にかけ て放射方向に延びており、 フライ ト 4 2外周縁に沿った各洗浄液排出パ イブ 8 0の先端口より、 前記残層処理物に向けて洗浄液を直接噴出させ ることができる。 このような構成によれば、 フライ ト 4 2自体に孔を設 ける加工は不要となり、 洗浄液排出パイプ 8 0をフライ ト 4 2に後付け することができ、 比較的容易に製作することができる。 なお、 各洗浄液 排出パイプ 8 0を放射状にできるだけ狭い間隔で取り付けることにより . 洗浄液を残層結晶に対して全周方向に広がるように噴出させることがで さる。 Each washing liquid discharge pipe 80 extends from the inner peripheral edge of the fly 42 to the outer peripheral edge. The cleaning liquid can be directly ejected toward the residual layer processing object from the distal end port of each cleaning liquid discharge pipe 80 along the outer periphery of the fly 42. According to such a configuration, it is not necessary to form a hole in the fly 42 itself, and the cleaning liquid discharge pipe 80 can be retrofitted to the fly 42, so that it can be manufactured relatively easily. By attaching the cleaning liquid discharge pipes 80 radially at as small an interval as possible, the cleaning liquid can be ejected so as to spread over the remaining layer crystals in all circumferential directions.

以上、 本発明の実施の形態を図面によって説明してきたが、 これらの 具体的な構成によれば、 結晶に対する洗浄液の透過性および残層結晶の 移動性を高めることが可能となる。 ただし、 本発明はこれらの実施の形 態に限定されるものではなく、 本発明の要旨を逸脱しない範囲における 変更や追加があっても本発明に含まれることは言うまでもない。 産業上の利用可能性  As described above, the embodiments of the present invention have been described with reference to the drawings. According to these specific configurations, it is possible to enhance the permeability of the cleaning liquid to the crystals and the mobility of the remaining layer crystals. However, the present invention is not limited to these embodiments, and it goes without saying that changes and additions without departing from the spirit of the present invention are included in the present invention. Industrial applicability

本発明に係る遠心分離機によれば、 スク リユーコンべャのフライ ト外 周縁より、 スク リーン部の内周面に付着している残層処理物に直接洗浄 液を噴射させることができるため、 この残層の移動性を改善し、 洗浄液 全体の透過性が増すため、 局所的に残層処理物のみを洗浄し、 処理物の 含液率を高くすることにより、 残層の固化防止が可能となる。  ADVANTAGE OF THE INVENTION According to the centrifugal separator which concerns on this invention, since a washing | cleaning liquid can be sprayed directly from the outer periphery of the fry of a screen conveyor to the remaining layer processing thing adhering to the inner peripheral surface of a screen part, Since the mobility of the remaining layer is improved and the permeability of the entire cleaning solution is increased, it is possible to prevent the solidification of the remaining layer by locally cleaning only the remaining layer processed material and increasing the liquid content of the processed material. It becomes.

また、 スクリーン部の目漏れについても処理物全体に洗浄液をかけた 場合、 処理物層を通過する洗浄液の液量に比例した量の処理物と、 スク リーン部の目開きに比例した量の処理物の-目漏れを生じるが、 前述の如 く洗浄液をフライ ト外周縁より直接的に残層処理物に噴射することによ り、 残層処理物の固着がなくなり、 搬送中の処理物に対する洗浄液の透 過率が向上するため、 本来の処理物中の不純物の置換用としての洗浄液 量を抑制することが可能になり 、 スク リーン部における処理物の総合目 漏れ量を減少させることが可能となる。 In addition, when the cleaning liquid is applied to the entire processed material, the amount of the processed material is proportional to the amount of the cleaning liquid passing through the processed material layer, and the amount of the processed liquid is proportional to the opening of the screen. The cleaning liquid is sprayed directly from the outer peripheral edge of the freight to the remaining layer processing material as described above, thereby preventing the remaining layer processing material from sticking to the processing object being transported. Since the permeability of the cleaning solution is improved, the cleaning solution is intended to replace impurities in the original processed product. This makes it possible to reduce the amount, and it is possible to reduce the total leakage amount of the processed material in the screen part.

Claims

請求の範囲 The scope of the claims 1. ボウル ( 2 0 ) 内にスク リューコンペャ (4 0) を備え、 これらを 相対的に回転可能に支持してなり、 前記ボウル ( 2 0 ) 内に供給した原 液から処理物を分離すると共に、 該ポウル ( 2 0) の一端側の内周面に 沿って設けたスク リーン部 ( 3 0.) で、 前記処理物の洗浄およぴ脱液を 行う遠心分離機 ( 1 0 , 1 0 A, 1 0 B) において、 前記スク リ ューコ ンべャ (4 0 ) のハブ (4 1 ) に、 その内部に供給した洗浄液を受け入 れる洗浄液受け部 (4 3 ) と、 該洗浄液受け部 (4 3 ) 内の洗浄液を前 記スク リーン部 ( 3 0) に向かって噴出する洗浄ノズル (4 5 ) とを有 する遠心分離機 (.1 0, 1 0 A, 1 0 B) であって、 1. A screw conveyor (40) is provided in the bowl (20), and these are relatively rotatably supported to separate the processed material from the stock solution supplied into the bowl (20). A centrifuge (10, 10) for washing and dewatering the processed material at a screen section (30.) provided along the inner peripheral surface on one end side of the powl (20). A, 10 B), a cleaning liquid receiving part (43) for receiving the cleaning liquid supplied to the hub (41) of the screw conveyor (40), and the cleaning liquid receiving part A centrifuge (.10, 10A, 10B) having a cleaning nozzle (45) for jetting the cleaning liquid in (43) toward the screen section (30). hand, 前記洗浄液受け部 (4 3 ) 内に、 前記スクリューコンペャ (4 0 ) の フライ ト (4 2) 外周縁と前記スクリーン部 ( 3 0 ) 内周面との間の隙 間に生じる残層処理物を洗浄する洗浄液を受け入れる残層用洗浄液受け 部 (4 6 ) を、 前記洗浄液受け部 (4 3 ) 内とは独立に区画して設け、 前記フライ ト (4 2) のらせん方向に沿って、 前記残層用洗浄液受け 部 (4 6 ) 内の洗浄液を、 前記洗浄液受け部 (4 3 ) とは仕切られた状 態で前記フライ ト (4 2 ) 外周縁より前記残層処理物に向けて直接噴出 させる残層用洗浄経路を形成したことを特徴とする遠心分離機 ( 1 0, 1 0 A, 1 0 B ) 。  Remaining layer treatment generated in the cleaning liquid receiving portion (43) in a gap between the outer peripheral edge of the flight (42) of the screw conveyer (40) and the inner peripheral surface of the screen portion (30). A residual layer cleaning liquid receiving section (46) for receiving a cleaning liquid for cleaning an object is provided separately from the inside of the cleaning liquid receiving section (43), and is provided along the spiral direction of the fly (42). The cleaning liquid in the residual layer cleaning liquid receiving section (46) is directed from the outer periphery of the fly (42) toward the residual layer processing material in a state of being separated from the cleaning liquid receiving section (43). A centrifugal separator (10, 10A, 10B) characterized by forming a cleaning path for the residual layer to be directly ejected by using a centrifuge. 2. ボウル (2 0 ) 内にスクリューコンペャ (4 0) を備え、 これらを 相対的に回転可能に支持してなり、 前記ボウル (2 0 ) 内に供給した原 液から処理物を分離すると共に、 該ボウル (2 0) の一端側の内周面に 沿って設けたスク リーン部 ( 3 0 ) で、 前記処理物の洗浄および脱液を 行う遠心分離機 ( 1 0, 1 0 A) において、 前記スク リ ューコンペャ ( 2. A screw conveyor (40) is provided in the bowl (20), and these are relatively rotatably supported to separate the processed material from the stock solution supplied into the bowl (20). At the same time, a centrifuge (10, 10A) for washing and dewatering the processed material at a screen portion (30) provided along the inner peripheral surface on one end side of the bowl (20). In the above, the screw conveyor ( 4 0 ) のハブ (4 1 ) に、 その内部に供給した洗浄液を受け入れる洗浄 液受け部 (4 3 ) と、 該洗浄液受け部 (4 3 ) 内の洗浄液を前記スク リ ーン部 ( 3 0 ) に向かって噴出する洗浄ノズル (4 5 ) とを有する遠心 分離機 ( 1 0 , 1 0 A) であって、 , Washing that receives the washing liquid supplied to the hub (41) of 40) A centrifuge (1) having a liquid receiving portion (43) and a cleaning nozzle (45) for jetting the cleaning liquid in the cleaning liquid receiving portion (43) toward the screen portion (30). 0, 1 0 A) where, 前記洗浄液受け部 (4 3 ) 内に、 前記スクリユーコンべャ (4 0 ) の フライ ト (4 2) 外周縁と前記スクリーン部 ( 3 0) 内周面との間の隙 間に生じる残層処理物を洗浄する洗浄液を受け入れる残層用洗浄液受け 部 (4 6 ) を、 前記洗浄液受け部 (4 3 ) 内とは独立に区画して設け、 前記フライ ト (4 2) の内周縁が連なる位置にて、 フライ ト (4 2 ) のらせん方向に沿って所定間隔おきに、 前記残層用洗浄液受け部 (4 6 ) の底側に接続管 (4 7 ) を設けると共に、 前記スクリューコンペャ ( 4 0 ) のハブ (4 1 ) ないしフライ ト (4 2) 内部に、 ハブ ( 4 1 ) 内 周側よりフライ ト (4 2 ) 外周縁にかけて放射方向に延びて前記接続管 (4 7) が連通する洗浄液排出孔 (4 9 ) を設け、  In the cleaning liquid receiving portion (43), a residual layer formed between the outer periphery of the flight (42) of the screw conveyor (40) and the inner peripheral surface of the screen portion (30). A residual layer cleaning liquid receiving section (46) for receiving a cleaning liquid for cleaning the processing object is provided separately from the inside of the cleaning liquid receiving section (43), and the inner periphery of the fly (42) is continuous. At the position, a connecting pipe (47) is provided at the bottom side of the residual layer cleaning liquid receiving portion (46) at predetermined intervals along the spiral direction of the fly (42), and the screw conveyer is provided. The connecting pipe (47) extends radially from the inner periphery of the hub (41) to the outer periphery of the fly (42) inside the hub (41) or the fly (42) of the (40). Is provided with a washing liquid discharge port (4 9) 前記残層用洗浄液受け部 (4 6 ) 内の洗浄液を、 前記フライ ト (4 2 ) 外周縁に開口する前記各洗浄液排出孔 (4 9 ) の先端口より、 前記残 層処理物に向けて直接噴出させることを特徴とする遠心分離機 ( 1 0 , 1 0 A;) 。  The cleaning liquid in the residual-layer cleaning liquid receiving portion (46) is directed toward the residual-layer-processed material from the distal end of each of the cleaning liquid discharge holes (49) opened on the outer periphery of the fly (42). A centrifuge (10, 10A;) characterized by direct ejection. 3. ボウル ( 2 0 ) 内にスクリューコンペャ (4 0) を備え、 これらを 相対的に回転可能に支持してなり、 前記ボウル (2 0 ) 内に供給した原 液から処理物を分離すると共に、 該ボウル (2 0 ) の一端側の内周面に 沿って設けたスク リーン部 ( 3 0) で、 前記処理物の洗浄および脱液を 行う遠心分離機 ( 1 0 B) において、 前記スクリユー コンべャ (4 0) のハブ (4 1 ) に、 その内部に供給した洗浄液を受け入れる洗浄液受け 部 (4 3 ) と、 該洗浄液受け部 (4 3 ) 内の洗浄液を前記スク リーン部 ( 3 0 ) に向かって嘖出する洗浄ノズル (4 5 ) とを有する遠心分離機 ( 1 0 B ) であって、 前記洗浄液受け部 (4 3 ) 内に、 前記スク リ ューコンペャ (4 0 ) の フライ ト (4 2 ) 外周縁と前記スク リーン部 (3 0 ) 内周面との間の隙 間に生じる残層処理物を洗浄する洗浄液を受け入れる残層用洗浄液受け 部 (4 6 ) を、 前記洗浄液受け部 (4 3 ) 内とは独立に区画して設け、 前記フライ ト (4 2) の処理物搬送面 (4 2 a ) と反対側の面 (4 2 b ) に隣接する位置にて、 前記フライ ド (4 2) のらせん方向に沿って 所定間隔おきに、 前記残層用洗浄液受け部 (4 6 ) の底側に接続管 (4 7 ) を設けると共に、 前記スク リ ューコンペャ (4 0 ) のハブ (4 1 ) に前記接続管 (4 7) が連通する洗浄液連通孔 (4 8 ) を設け、 3. Equipped with a screw conveyer (40) in the bowl (20), which is relatively rotatably supported, and separates the processed material from the stock solution supplied into the bowl (20). And a centrifugal separator (10B) for washing and dewatering the processed material at a screen part (30) provided along the inner peripheral surface on one end side of the bowl (20). A cleaning liquid receiving portion (43) for receiving the cleaning liquid supplied therein and a cleaning liquid in the cleaning liquid receiving portion (43) are supplied to the hub (41) of the screw conveyor (40) by the cleaning portion (43). A centrifuge (10B) having a washing nozzle (45) emerging toward 30). In the cleaning liquid receiving portion (43), a residual layer formed between the outer periphery of the fly (42) of the screw conveyor (40) and the inner peripheral surface of the screen portion (30). A residual layer cleaning liquid receiving section (46) for receiving a cleaning liquid for cleaning the processing object is provided separately from the inside of the cleaning liquid receiving section (43), and a processing object transport surface of the fly (42) is provided. At a position adjacent to the surface (42b) opposite to the surface (42a), at predetermined intervals along the spiral direction of the fly (42), the cleaning liquid receiving portion for the residual layer (46) ), A connection pipe (47) is provided on the bottom side, and a cleaning liquid communication hole (48) for connecting the connection pipe (47) to the hub (41) of the screw conveyor (40) is provided. 前記フライ ト (4 2) の反対側の面 (4 2 b ) に、 フライ ト (4 2 ) のらせん方向に沿って所定間隔おきに、 フライ ト (4 2) の内周縁より 外周縁にかけて放射方向に延びて前記洗浄液連通孔 (4 8 ) が連通する 洗浄液排出パイプ (8 0 ) を取り付け、  Radiation is made from the inner peripheral edge to the outer peripheral edge of the fly (42) at predetermined intervals along the spiral direction of the fly (42) on the opposite surface (42b) of the fly (42). A cleaning liquid discharge pipe (80) that extends in the direction and communicates with the cleaning liquid communication hole (48). 前記残層用洗浄液受け部 (4 6 ) 内の洗浄液を、 前記洗浄液排出パイ プ (8 0 ) の先端口より、 前記残層処理物に向けて直接噴出させること を特徴とする遠心分離機 ( 1 0 B) 。  A centrifugal separator characterized in that the cleaning liquid in the residual-layer cleaning liquid receiving section (46) is jetted directly from the distal end port of the cleaning liquid discharge pipe (80) toward the residual-layer processed material. 1 0 B). 4. 前記フライ ト (4 2 ) 外周縁の先端面に、 フライ ト (4 2) のらせ ん方向に連続して延び、 前記各洗浄液排出孔 (4 9 ) の先端口が連通す る溝 (4 9 a ) を形成したことを特徴とする請求の範囲第 2項記載の遠 心分離機 ( 1 0 A) 。  4. A groove extending continuously in the helix direction of the flyt (42) to the tip end surface of the outer periphery of the flyt (42), and communicating with the tip end of each of the cleaning liquid discharge holes (49). 3. The centrifugal separator (10A) according to claim 2, wherein (49a) is formed. 5. 前記スクリユーコンべャ (4 0 ) のハブ (4 1 ) 内部に、 その軸方 向に延びる原液供給用のフィー ドチューブ (6 0 ) を挿入し、  5. Insert the feed tube (60) for supplying the undiluted solution extending in the axial direction into the hub (41) of the screw conveyor (40). 前記フィー ドチューブ ( 6 0) 内に、 前記洗浄液受け部 (4 3 ) に洗 浄液を供給する洗浄液供給経路 ( 7 1 ) を形成すると共に、 前記洗浄液 受け部 (4 3 ) に対して半径方向に重なるフィードチューブ (6 0 ) の 途中に前記洗浄液供給経路 ( 7 1 ) の開放口を設け、 前記フィードチューブ (6 0 ) 内に、 前記残層用洗浄液受け部 (4 6 ) に洗浄液を供給する残層用洗浄液供給経路 ( 7 2 ) を形成すると共に 前記残層用洗浄液受け部 (4 6 ) に対して半径方向に重なるフィードチ ユーブ ( 6 0 ) の途中に前記残層用洗浄液供給経路 ( 7 2) の開放口を 設けたことを特徴とする請求の範囲第 1項, 第 2項, 第 3項または第 4 項記載の遠心分離機 ( 1 0 , 1 0 A, 1 0 B) 。 A cleaning liquid supply path (71) for supplying a cleaning liquid to the cleaning liquid receiving section (43) is formed in the feed tube (60), and a radial direction with respect to the cleaning liquid receiving section (43) is formed. An opening for the cleaning liquid supply path (71) is provided in the middle of the feed tube (60) overlapping the In the feed tube (60), a residual layer cleaning liquid supply path (72) for supplying a cleaning liquid to the residual layer cleaning liquid receiving part (46) is formed, and the residual layer cleaning liquid receiving part (46) is formed. 3. An opening for the residual layer cleaning liquid supply path (72) is provided in the middle of a feed tube (60) radially overlapping with (1), (2) and (3). Centrifuge (10, 10A, 10B) according to paragraph 3 or 4.
PCT/JP2002/013612 2002-12-26 2002-12-26 Centrifugal separator Ceased WO2004060566A1 (en)

Priority Applications (9)

Application Number Priority Date Filing Date Title
PCT/JP2002/013612 WO2004060566A1 (en) 2002-12-26 2002-12-26 Centrifugal separator
AU2002360052A AU2002360052A1 (en) 2002-12-26 2002-12-26 Centrifugal separator
US10/540,472 US7140494B2 (en) 2002-12-26 2003-12-26 Centrifugal machine
PCT/JP2003/016873 WO2004058410A1 (en) 2002-12-26 2003-12-26 Centrifugal machine
EP09008729A EP2108458B1 (en) 2002-12-26 2003-12-26 Centrifugal separator
CNB2003801074619A CN100337755C (en) 2002-12-26 2003-12-26 centrifuge
CN200710089696XA CN101041145B (en) 2002-12-26 2003-12-26 Centrifugal separator
EP03768302A EP1579918B8 (en) 2002-12-26 2003-12-26 Centrifugal machine
AU2003292669A AU2003292669A1 (en) 2002-12-26 2003-12-26 Centrifugal machine

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/JP2002/013612 WO2004060566A1 (en) 2002-12-26 2002-12-26 Centrifugal separator

Publications (1)

Publication Number Publication Date
WO2004060566A1 true WO2004060566A1 (en) 2004-07-22

Family

ID=32697299

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/JP2002/013612 Ceased WO2004060566A1 (en) 2002-12-26 2002-12-26 Centrifugal separator

Country Status (2)

Country Link
AU (1) AU2002360052A1 (en)
WO (1) WO2004060566A1 (en)

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4431913B1 (en) * 1965-10-04 1969-12-19
JPS4964065A (en) * 1972-10-23 1974-06-21
JPS5592157A (en) * 1978-12-29 1980-07-12 Kureha Chem Ind Co Ltd Method and device for refining crystalline substance
JPH0889848A (en) * 1994-09-21 1996-04-09 Ishigaki Mech Ind Co Sludge centrifugal separator
US5509882A (en) * 1994-09-12 1996-04-23 Tetra Laval Holdings & Finance S.A. Decanter centrifuge having an offset conveyor flight to aid rinsing
JPH1028899A (en) * 1996-07-16 1998-02-03 Tsukishima Kikai Co Ltd Screen bowl decanter centrifugal separator

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4431913B1 (en) * 1965-10-04 1969-12-19
JPS4964065A (en) * 1972-10-23 1974-06-21
JPS5592157A (en) * 1978-12-29 1980-07-12 Kureha Chem Ind Co Ltd Method and device for refining crystalline substance
US5509882A (en) * 1994-09-12 1996-04-23 Tetra Laval Holdings & Finance S.A. Decanter centrifuge having an offset conveyor flight to aid rinsing
JPH0889848A (en) * 1994-09-21 1996-04-09 Ishigaki Mech Ind Co Sludge centrifugal separator
JPH1028899A (en) * 1996-07-16 1998-02-03 Tsukishima Kikai Co Ltd Screen bowl decanter centrifugal separator

Also Published As

Publication number Publication date
AU2002360052A1 (en) 2004-07-29
AU2002360052A8 (en) 2004-07-29

Similar Documents

Publication Publication Date Title
JP4335679B2 (en) Apparatus for purifying and separating crystals from a suspension of crystals in an impure crystal melt.
EP0897752B1 (en) Centrifuge with cake churning
JP2001179492A (en) Screw press type concentrating machine, and its concentrating method
JP3191304U (en) centrifuge
WO2016027420A1 (en) Decanter centrifuge and method for operating decanter centrifuge
JP4958788B2 (en) Lime mud treatment method and apparatus
JP2002177712A (en) Rotary drum screen for solid-liquid separation and sludge thickener using the same
WO2004058410A1 (en) Centrifugal machine
JPS6244982B2 (en)
JP3609959B2 (en) Screen bowl type decanter type centrifuge
JP3336291B2 (en) Decanter centrifuge
WO2004060566A1 (en) Centrifugal separator
JP4518531B2 (en) Rinse decanter
JP3974513B2 (en) centrifuge
JP3886894B2 (en) centrifuge
WO2004060567A1 (en) Centrifugal separator
JPH02126908A (en) Continuous solid-liquid separator
JP3770793B2 (en) Rotating single chamber filter and filtration method
JP5161159B2 (en) Cone centrifuge
WO2014049791A1 (en) Pressurized multi-chamber rotary filtration device and method for operating same
JP2017217642A (en) centrifuge
JPH01228515A (en) Purification apparatus
JP3696595B2 (en) Centrifuge method and centrifuge
JP2005193105A (en) Drum screen and solid-liquid separator
JP6108320B2 (en) Filtration device

Legal Events

Date Code Title Description
AK Designated states

Kind code of ref document: A1

Designated state(s): AE AG AL AM AT AU AZ BA BB BG BR BY BZ CA CH CN CO CR CU CZ DE DK DM DZ EC EE ES FI GB GD GE GH GM HR HU ID IL IN IS KE KG KP KR KZ LC LK LR LS LT LU LV MA MD MG MK MN MW MX MZ NO NZ OM PH PL PT RO RU SC SD SE SG SI SK SL TJ TM TN TR TT TZ UA UG US UZ VC VN YU ZA ZM ZW

AL Designated countries for regional patents

Kind code of ref document: A1

Designated state(s): GH GM KE LS MW MZ SD SL SZ TZ UG ZM ZW AM AZ BY KG KZ MD RU TJ TM AT BE BG CH CY CZ DE DK EE ES FI FR GB GR IE IT LU MC NL PT SE SK TR BF BJ CF CG CI CM GA GN GQ GW ML MR NE SN TD TG

121 Ep: the epo has been informed by wipo that ep was designated in this application
122 Ep: pct application non-entry in european phase