WO2002012365A3 - Adhesif durcissant a base de polyurethanne adhesive a une partie d'humidite - Google Patents
Adhesif durcissant a base de polyurethanne adhesive a une partie d'humidite Download PDFInfo
- Publication number
- WO2002012365A3 WO2002012365A3 PCT/US2001/024703 US0124703W WO0212365A3 WO 2002012365 A3 WO2002012365 A3 WO 2002012365A3 US 0124703 W US0124703 W US 0124703W WO 0212365 A3 WO0212365 A3 WO 0212365A3
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- adhesive
- dispersion
- triol
- substrates together
- isocyanate
- Prior art date
Links
- 239000000853 adhesive Substances 0.000 title abstract 5
- 230000001070 adhesive effect Effects 0.000 title abstract 5
- 229920002635 polyurethane Polymers 0.000 title 1
- 239000004814 polyurethane Substances 0.000 title 1
- 239000000758 substrate Substances 0.000 abstract 5
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical compound ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 abstract 3
- 239000006185 dispersion Substances 0.000 abstract 3
- 229920001730 Moisture cure polyurethane Polymers 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 239000002245 particle Substances 0.000 abstract 2
- 229920001228 polyisocyanate Polymers 0.000 abstract 2
- 239000005056 polyisocyanate Substances 0.000 abstract 2
- 239000004825 One-part adhesive Substances 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 150000002009 diols Chemical class 0.000 abstract 1
- 239000012948 isocyanate Substances 0.000 abstract 1
- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 abstract 1
- 150000002513 isocyanates Chemical class 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 229920000620 organic polymer Polymers 0.000 abstract 1
- 229920000642 polymer Polymers 0.000 abstract 1
- 229920005862 polyol Polymers 0.000 abstract 1
- 150000003077 polyols Chemical class 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/63—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers
- C08G18/632—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers onto polyethers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
- C08G18/12—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step using two or more compounds having active hydrogen in the first polymerisation step
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/16—Catalysts
- C08G18/18—Catalysts containing secondary or tertiary amines or salts thereof
- C08G18/20—Heterocyclic amines; Salts thereof
- C08G18/2009—Heterocyclic amines; Salts thereof containing one heterocyclic ring
- C08G18/2018—Heterocyclic amines; Salts thereof containing one heterocyclic ring having one nitrogen atom in the ring
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/08—Processes
- C08G18/16—Catalysts
- C08G18/22—Catalysts containing metal compounds
- C08G18/227—Catalysts containing metal compounds of antimony, bismuth or arsenic
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/4009—Two or more macromolecular compounds not provided for in one single group of groups C08G18/42 - C08G18/64
- C08G18/4072—Mixtures of compounds of group C08G18/63 with other macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/40—High-molecular-weight compounds
- C08G18/48—Polyethers
- C08G18/4804—Two or more polyethers of different physical or chemical nature
- C08G18/4812—Mixtures of polyetherdiols with polyetherpolyols having at least three hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J175/00—Adhesives based on polyureas or polyurethanes; Adhesives based on derivatives of such polymers
- C09J175/04—Polyurethanes
- C09J175/08—Polyurethanes from polyethers
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Polyurethanes Or Polyureas (AREA)
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| MXPA03001191A MXPA03001191A (es) | 2000-08-07 | 2001-08-07 | Adhesivo de poliuretano de una sola parte, curable con humedad. |
| AU2001283149A AU2001283149A1 (en) | 2000-08-07 | 2001-08-07 | One-part moisture curable polyurethane adhesive |
| JP2002518333A JP5059274B2 (ja) | 2000-08-07 | 2001-08-07 | 一液型湿分硬化性ポリウレタン接着剤 |
| KR1020037001830A KR100859428B1 (ko) | 2000-08-07 | 2001-08-07 | 원-파트 습기 경화성 폴리우레탄 접착제 |
| BR0113451-5A BR0113451A (pt) | 2000-08-07 | 2001-08-07 | Adesivo de poliuretano monocomponente curável em umidade método para ligar dois substratos usando tal adesivo |
| CA002416908A CA2416908A1 (fr) | 2000-08-07 | 2001-08-07 | Adhesif durcissant a base de polyurethanne adhesive a une partie d'humidite |
| EP01961926A EP1311574B1 (fr) | 2000-08-07 | 2001-08-07 | Adhesif durcissant a base de polyurethanne adhesive a une partie d'humidite |
| DE60124264T DE60124264T2 (de) | 2000-08-07 | 2001-08-07 | Feuchtigkeitshärtbarer einkomponenten-polyurethanklebstoff |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US22313500P | 2000-08-07 | 2000-08-07 | |
| US60/223,135 | 2000-08-07 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| WO2002012365A2 WO2002012365A2 (fr) | 2002-02-14 |
| WO2002012365A3 true WO2002012365A3 (fr) | 2002-04-25 |
Family
ID=22835181
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/US2001/024703 WO2002012365A2 (fr) | 2000-08-07 | 2001-08-07 | Adhesif durcissant a base de polyurethanne adhesive a une partie d'humidite |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US6709539B2 (fr) |
| EP (1) | EP1311574B1 (fr) |
| JP (1) | JP5059274B2 (fr) |
| KR (1) | KR100859428B1 (fr) |
| CN (1) | CN1233681C (fr) |
| AT (1) | ATE344286T1 (fr) |
| AU (1) | AU2001283149A1 (fr) |
| BR (1) | BR0113451A (fr) |
| CA (1) | CA2416908A1 (fr) |
| DE (1) | DE60124264T2 (fr) |
| ES (1) | ES2271062T3 (fr) |
| MX (1) | MXPA03001191A (fr) |
| WO (1) | WO2002012365A2 (fr) |
Families Citing this family (53)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| MXPA06002031A (es) * | 2003-08-22 | 2006-05-31 | Dow Global Technologies Inc | Composicion util como adhesivo para instalar ventanas en vehiculos. |
| US7361292B2 (en) * | 2004-11-08 | 2008-04-22 | Dow Global Technologies Inc. | High modulus, nonconductive adhesive useful for installing vehicle windows |
| DE102006033796A1 (de) | 2006-07-19 | 2008-01-31 | Tesa Ag | Haftklebestoffe aus einem harzmodifizierten Polyurethan |
| DE102006033368A1 (de) * | 2006-07-19 | 2008-01-24 | Wilhelm Karmann Gmbh | Verfahren zur Herstellung einer Verklebung und Fahrzeugdach mit textilem Verdeckstoff |
| CA2673328A1 (fr) | 2006-12-21 | 2008-06-26 | Dow Global Technologies Inc. | Composition utile en tant qu'adhesif pour l'installation de vitres de vehicules |
| US7842146B2 (en) | 2007-01-26 | 2010-11-30 | Dow Global Technologies Inc. | Ultrasonic energy for adhesive bonding |
| WO2008097852A1 (fr) * | 2007-02-02 | 2008-08-14 | Dow Global Technologies Inc. | Adhésif utile pour l'installation de fenêtres de véhicule |
| WO2009015149A1 (fr) * | 2007-07-23 | 2009-01-29 | Dow Global Technologies Inc. | Composition vulcanisable de polyuréthane à deux parties ayant un module g sensiblement constant sur la plage de températures d'utilisation |
| US20090030146A1 (en) * | 2007-07-24 | 2009-01-29 | Yuliya Berezkin | Polyurethane dispersions for sealants |
| JP5294251B2 (ja) * | 2008-05-12 | 2013-09-18 | 株式会社イノアックコーポレーション | ポリウレタンフォームの接着方法 |
| DE102008023252A1 (de) * | 2008-05-13 | 2009-11-19 | Tesa Se | Hotmelt-Verfahren zur Herstellung eines chemisch vernetzten Polyurethanfilms |
| BRPI0912919B1 (pt) * | 2008-08-22 | 2019-04-24 | Dow Global Technologies Llc | Composição bicomponente e método para ligar dois ou mais substratos entre si |
| KR101605928B1 (ko) * | 2008-12-23 | 2016-03-23 | 다우 글로벌 테크놀로지스 엘엘씨 | 신속한 운행가능 시간을 제공하는 차량 창문 설치에 유용한 접착제 |
| US20110147240A1 (en) * | 2009-12-18 | 2011-06-23 | Kim Ernest J | Device and Method for Storing and Dispensing |
| CN102869695B (zh) | 2010-04-30 | 2015-07-01 | 陶氏环球技术有限责任公司 | 改进的交通工具玻璃粘合剂和粘合所述玻璃的方法 |
| CN104672413B (zh) | 2010-12-20 | 2019-05-03 | 陶氏环球技术有限责任公司 | 在固化状态下具有改进的耐久性的含异氰酸酯官能组分的可固化组合物 |
| KR101597888B1 (ko) | 2011-05-03 | 2016-02-25 | 다우 글로벌 테크놀로지스 엘엘씨 | 유리에의 결합에 유용한 이중 경화 접착제 |
| WO2012151085A1 (fr) | 2011-05-03 | 2012-11-08 | Dow Global Technologies Llc | Composition à durcissement accéléré contenant un prépolymère à fonctionnalité isocyanate |
| DE102011077200A1 (de) * | 2011-06-08 | 2012-12-13 | Bayer Materialscience Aktiengesellschaft | Klebstoffe |
| US9493604B2 (en) | 2012-02-21 | 2016-11-15 | Dow Global Technologies Llc | Compositions containing aromatic isocyanate functional components and aliphatic aromatics isocyanate functional components having improved cure speed |
| WO2014014499A1 (fr) | 2012-07-16 | 2014-01-23 | Dow Global Technologies Llc | Compositions polymérisables contenant des composants à fonction isocyanate et des polymères linéaires amorphes, adhésifs ainsi obtenus |
| EP2904039B1 (fr) | 2012-10-08 | 2020-10-07 | Dow Global Technologies LLC | Collage accéléré d'un adhésif à fonction isocyanate sur des plastiques renforcés par des fibres |
| WO2014074140A1 (fr) | 2012-11-08 | 2014-05-15 | Dow Global Technologies Llc | Adhésif ultrarapide à double durcisseur utile pour le collage sur verre |
| AU2013364399B2 (en) | 2012-12-21 | 2017-05-25 | Dow Global Technologies Llc | Adhesive useful for installing vehicle windows |
| EP2935384B1 (fr) | 2012-12-21 | 2020-09-02 | Dow Global Technologies LLC | Adhésif à durcissement rapide utile pour un collage au verre |
| US10533119B2 (en) | 2013-05-02 | 2020-01-14 | Dow Global Technologies Llc | Rapid drive away time adhesive for installing vehicle windows |
| CN105764949B (zh) | 2013-12-09 | 2019-05-31 | 陶氏环球技术有限责任公司 | 具有极少或无塑化剂的改进的聚氨基甲酸酯预聚物和其在车辆玻璃粘合剂中的用途 |
| EP3087114B1 (fr) | 2013-12-23 | 2020-04-15 | Dow Global Technologies LLC | Adhésif contenant un prépolymère polyol polyuréthanne de type copolymère à teneur élevée en solides |
| US9821512B2 (en) | 2014-04-10 | 2017-11-21 | Dow Global Technologies Llc | Method and apparatus for dispensing reactive two-part systems |
| CN106257984B (zh) | 2014-05-08 | 2019-08-30 | 陶氏环球技术有限责任公司 | 可用于粘结玻璃的可湿致固化聚氨酯粘合剂组合物的加速固化 |
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| MX2017006889A (es) | 2014-12-01 | 2017-09-01 | Dow Global Technologies Llc | Películas de contracción, y métodos para su fabricación. |
| BR112017023097A2 (pt) | 2015-05-05 | 2018-07-10 | Dow Global Technologies Llc | plastificantes reativos de poliuretano e adesivos feitos a partir dos mesmos |
| CN107690464A (zh) | 2015-06-25 | 2018-02-13 | 陶氏环球技术有限责任公司 | 改良的单组分可湿固化粘合剂 |
| WO2017142714A1 (fr) | 2016-02-17 | 2017-08-24 | Dow Global Technologies Llc | Compositions contenant des prépolymères fonctionnels isocyanate et des nanoargiles modifiées par des ammoniums quaternaires |
| EP3464402B1 (fr) | 2016-05-23 | 2020-11-11 | Dow Global Technologies LLC | Procédé pour améliorer le fini de surface d'objets fabriqués de manière additive |
| JP2017222746A (ja) * | 2016-06-14 | 2017-12-21 | ヘンケルジャパン株式会社 | ウレタン粘着剤 |
| WO2018005349A1 (fr) | 2016-06-28 | 2018-01-04 | Dow Global Technologies Llc | Articles thermodurcissables à fabrication additive incorporant un matériau à changement de phase, et leur procédé de fabrication |
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| EP3638708A1 (fr) | 2017-06-15 | 2020-04-22 | Ddp Specialty Electronic Materials Us, Inc. | Compositions contenant des adhésifs contenant un prépolymère hydrophobe à fonction isocyanate modifiée |
| WO2019014582A1 (fr) | 2017-07-13 | 2019-01-17 | Dow Global Technologies Llc | Sels de silylammonium utilisés comme catalyseurs polyuréthane latents |
| WO2019014171A1 (fr) | 2017-07-13 | 2019-01-17 | Dow Global Technologies Llc | Adhésifs polyuréthane latents à deux composants durcissables dans des conditions ambiantes |
| WO2019014593A1 (fr) | 2017-07-13 | 2019-01-17 | Dow Global Technologies Llc | Co-catalyseurs organozinciques pour une latence améliorée dans le durcissement du polyuréthane |
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| CN116113650A (zh) | 2020-08-31 | 2023-05-12 | Ddp特种电子材料美国有限责任公司 | 用于聚氨酯粘合剂的底漆 |
| EP4259709A1 (fr) | 2020-12-08 | 2023-10-18 | Zephyros Inc. | Composition comprenant un prépolymère modifié par silyle et du noir de carbone hautement structuré |
| CN112724911B (zh) * | 2020-12-28 | 2023-03-07 | 安徽匠星联创新材料科技有限公司 | 一种聚脲聚氨酯混合单组份高光背草胶 |
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| EP4410854A1 (fr) | 2023-02-03 | 2024-08-07 | Arkema France | Adhésifs à structure hybride uréthane-acrylate à haute résistance |
| WO2025104495A1 (fr) | 2023-11-14 | 2025-05-22 | Arkema France | Adhésif de polyuréthane 2k à faible module pour lier des composites |
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|---|---|---|---|---|
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| US5603798A (en) * | 1995-01-13 | 1997-02-18 | The Dow Chemical Company | Two-part moisture curable polyurethane adhesive |
| US5922809A (en) * | 1996-01-11 | 1999-07-13 | The Dow Chemical Company | One-part moisture curable polyurethane adhesive |
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2001
- 2001-08-07 BR BR0113451-5A patent/BR0113451A/pt active Search and Examination
- 2001-08-07 WO PCT/US2001/024703 patent/WO2002012365A2/fr active IP Right Grant
- 2001-08-07 KR KR1020037001830A patent/KR100859428B1/ko not_active Expired - Fee Related
- 2001-08-07 AU AU2001283149A patent/AU2001283149A1/en not_active Abandoned
- 2001-08-07 US US09/928,980 patent/US6709539B2/en not_active Expired - Lifetime
- 2001-08-07 CN CNB018138497A patent/CN1233681C/zh not_active Expired - Fee Related
- 2001-08-07 JP JP2002518333A patent/JP5059274B2/ja not_active Expired - Fee Related
- 2001-08-07 AT AT01961926T patent/ATE344286T1/de not_active IP Right Cessation
- 2001-08-07 DE DE60124264T patent/DE60124264T2/de not_active Expired - Lifetime
- 2001-08-07 ES ES01961926T patent/ES2271062T3/es not_active Expired - Lifetime
- 2001-08-07 EP EP01961926A patent/EP1311574B1/fr not_active Expired - Lifetime
- 2001-08-07 MX MXPA03001191A patent/MXPA03001191A/es active IP Right Grant
- 2001-08-07 CA CA002416908A patent/CA2416908A1/fr not_active Abandoned
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| EP0275908A2 (fr) * | 1987-01-23 | 1988-07-27 | Bayer Ag | Adhésif et son application pour la fabrication de collage |
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Also Published As
| Publication number | Publication date |
|---|---|
| KR20040030396A (ko) | 2004-04-09 |
| US20020061962A1 (en) | 2002-05-23 |
| EP1311574B1 (fr) | 2006-11-02 |
| ATE344286T1 (de) | 2006-11-15 |
| CN1233681C (zh) | 2005-12-28 |
| DE60124264T2 (de) | 2007-05-31 |
| AU2001283149A1 (en) | 2002-02-18 |
| US6709539B2 (en) | 2004-03-23 |
| JP5059274B2 (ja) | 2012-10-24 |
| JP2004506075A (ja) | 2004-02-26 |
| WO2002012365A2 (fr) | 2002-02-14 |
| CN1446236A (zh) | 2003-10-01 |
| CA2416908A1 (fr) | 2002-02-14 |
| EP1311574A2 (fr) | 2003-05-21 |
| DE60124264D1 (de) | 2006-12-14 |
| KR100859428B1 (ko) | 2008-09-23 |
| MXPA03001191A (es) | 2004-07-30 |
| ES2271062T3 (es) | 2007-04-16 |
| BR0113451A (pt) | 2003-10-14 |
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