WO1999047636A2 - Improved method and apparatus for processing a preparation - Google Patents
Improved method and apparatus for processing a preparation Download PDFInfo
- Publication number
- WO1999047636A2 WO1999047636A2 PCT/NZ1999/000031 NZ9900031W WO9947636A2 WO 1999047636 A2 WO1999047636 A2 WO 1999047636A2 NZ 9900031 W NZ9900031 W NZ 9900031W WO 9947636 A2 WO9947636 A2 WO 9947636A2
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- wort
- stage
- preparation
- screening
- components
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C7/00—Preparation of wort
- C12C7/14—Lautering, i.e. clarifying wort
- C12C7/16—Lautering, i.e. clarifying wort by straining
- C12C7/165—Lautering, i.e. clarifying wort by straining in mash filters
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12C—BEER; PREPARATION OF BEER BY FERMENTATION; PREPARATION OF MALT FOR MAKING BEER; PREPARATION OF HOPS FOR MAKING BEER
- C12C9/00—Methods specially adapted for the making of beerwort
- C12C9/02—Beerwort treatment; Boiling with hops; Hop extraction
-
- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
- C12H—PASTEURISATION, STERILISATION, PRESERVATION, PURIFICATION, CLARIFICATION OR AGEING OF ALCOHOLIC BEVERAGES; METHODS FOR ALTERING THE ALCOHOL CONTENT OF FERMENTED SOLUTIONS OR ALCOHOLIC BEVERAGES
- C12H3/00—Methods for reducing the alcohol content of fermented solutions or alcoholic beverage to obtain low alcohol or non-alcoholic beverages
- C12H3/04—Methods for reducing the alcohol content of fermented solutions or alcoholic beverage to obtain low alcohol or non-alcoholic beverages using semi-permeable membranes
Definitions
- This invention relates to an improved method and apparatus for processing a preparation.
- preparation referred to throughout is commonly known in the art of beer production as wort. However, it should be appreciated by those skilled in the art that other preparations may be processed in conjunction with the present invention. For example, in other embodiments, preparations used in the production of wine, cider or other low alcohol beverages may be processed in accordance with the present invention.
- a lauter tun consists of a chamber with perforated bottom plates and a wort recirculation system, where the wort may be drawn through the perforated plates, through the recirculated system and then deposited back into the lauter tun. Husks from the malt will fall to the bottom of the tun and act as a crude filter, preventing large particles in the wort stream from being transferred to the next brewing vessel. Circulation of the wort in the lauter tun continues until the wort is clear of large particles. Throughout the sparging stage the perforated plates of the lauter tun trap and separate spent grain and other large particles from the wort to form a substantially clear wort stream. When the circulated wort has an acceptable clarity the flow is diverted to the kettle.
- the wort preparation method discussed above involves a number of limitations and problems.
- beta-glucans may be leached from the grain bed, which creates a hazy beer due to filtration difficulties. These compounds may also inhibit the metabolism of yeast during fermentation.
- DMS dimethyl sulphide
- Oxidation of the wort in the kettle and whirlpool degrade chemical structure and organoleptic properties of the worts flavour compounds. If the wort is left in the kettle or whirlpool too long, the resulting beer will exhibit an undesirable oxidised flavour.
- the process of boiling also promotes the loss of natural compounds that assist in the formation of a head on the beer. Normally, additional head promoting compounds must be added to wort processed with a kettle and whirlpool due to loss of these volatile components.
- the wort preparation method discussed above also creates a large amount of high BOD (Biochemical Oxygen Demand) wastewater from the lauter tun.
- BOD Biochemical Oxygen Demand
- the BOD of materials discharged from particular industries is monitored and a business may be fined or penalised if it has discharged too much high BOD waste.
- the wort preparation method discussed above also requires large and costly elements such as the kettle and whirlpool. Manufacturing of the elements required substantially increases the capital cost of setting up a production line, which is eventually passed on to the consumer through higher beer prices.
- the wort preparation method listed above is slow and relatively inefficient.
- the wort requires long cooking times, and large amounts of heat via steam percolators to be applied and subsequently removed during processing.
- the large quantities of steam required leads to substantial boiler house capital investment and fuel costs.
- Filtered beers are also well known in the art. With these beers the fermented wort is filtered through a micro-filtration unit to remove any enzymes or microbiological components, sterilising the beer. A filtered beer is sterilised by the filtering stage and does not need to be pasteurized before it is bottled, thereby providing a distinctly flavoured and unique beer.
- a filtering device for a preparation is used in the production of a beverage
- the filtering device including at least one filtering stage, and is characterised in that a filtering stage is adapted to pass a first constituent fluid of the preparation, and retain required components of the preparation.
- the preparation to be processed may be wort used to prepare beer.
- Wort is a liquid formed from ground malted grain added to warm water. This basic mixture is normally filtered, treated then fermented to produce beer.
- Alternative embodiments of the present invention may not employ wort as the preparation processed in conjunction with the present invention.
- other preparations may be used to produce cider, wine or any other beverage, and reference to the above should in no way be seen as limiting.
- a first constituent fluid of the wort may be water. This first constituent fluid is to be removed to further concentrate the wort. As the main component of wort is water, the removal of water will quickly concentrate the required components of the wort.
- Alternative embodiments of the present invention may not pass water only from the wort using a filtering stage.
- water as well as other waste components may be passed out of a filtering stage while retaining the required components within the filter stage.
- a desired characteristic which determines when the retained components of the wort are transferred to a treatment stage is the concentration levels of carbohydrate within the wort.
- these carbohydrate concentration levels are determined by measuring the specific gravity of the wort as water is passed from a filtering stage.
- Alternative embodiments may not use carbohydrate concentration levels as the desired characteristic that determines when the wort is transferred to a treatment stage.
- the desired characteristic used may be the wort colour, viscosity or the concentration level of waste or other unwanted compounds within the wort.
- the required components of the wort will mostly consist of a mixture of water, carbohydrate compounds, flavour components, head retention components and colour components.
- a mixture of components is required to keep the wort in a liquid form and also to ensure that the wort contains material that may be readily fermented to produce the distinctive flavourings present in beer.
- a filter stage may include a membrane filter.
- membrane filters can be produced with customised pore sizes to trap and retain particular types of chemicals while allowing others to permeate through the membrane.
- the filter stage may be configured to process wort by the wort being passed through the membrane filter a number of times until the retained components of the wort exhibit a desired characteristic.
- the filter stage may be designed so that it can be used in continuous flow processing operations, where a single pass of the wort stream through the filter stage may result in the retained components of the wort exhibiting a desired characteristic.
- a filter stage includes a reverse osmosis membrane.
- Such reverse osmosis membranes are configured to allow water to pass or permeate through the membrane while retaining all other components to form a retentate.
- This type of membrane is particularly well adapted to this application as it allows the concentration of carbohydrates within the wort to be readily increased.
- a filter stage may not include a reverse osmosis membrane.
- a nano filtration membrane may be used as a filter stage.
- Such nano filtration membranes operate in a similar manner to reverse osmosis membranes but also allow some forms of mono-valient salts (for example sodium ions) through a membrane in addition to water.
- a combination of both reverse osmosis membranes and nano filtration membranes may be used as a filter stage.
- the use of a nano filtration membrane in this application has the potential to give a characteristic and possibly improved new flavour to the resulting beer produced from the wort processed.
- a filter stage may include a spiral wound reverse osmosis membrane. This configuration of reverse osmosis membrane may be easily adapted to this particular type of application.
- Alternative embodiments of the present invention may not employ reverse osmosis membrane filters in a filter stage or a spiral would reverse osmosis membrane.
- alternative embodiments may employ any type and shape of filtering membrane or apparatus that readily passes water through the filter stage while retaining components of the wort within the filter stage.
- any types of apparatus which functions in the same way as a reverse osmosis membrane, (or which alternatively may be a flat sheet membrane) may be used in the filter stage.
- Reference to the above only throughout this specification should be in no way seen as limiting.
- Reference throughout this specification shall now be made to a filtering stage as including a reverse osmosis membrane.
- other types of filter stage may be used in conjunction with the present invention and reference to the above should in no way be seen as limiting.
- water that has permeated through the reverse osmosis membrane may be recirculated back into a lauter tun used at the start of the preparation process. In this way the permeated water may be recirculated back to the original source of the wort. Recycling wastewater in this way reduces water consumption and wastewater production.
- a treatment stage may consist of a number of elements, which heat treat, cool and oxygenate the wort and lastly transfer it to a fermenter. These treatment stages complete the final processing of the wort, making it ready to be fermented into beer.
- Alternative embodiments of the present invention may not employ a treatment stage as listed above.
- any or all of the treatments stage elements listed above may be employed as required.
- a method of processing a wort stream used in the production of a beer using at least one reverse osmosis membrane as a filter stage and at least one treatment stage,
- the above invention allows wort for the production of beer to be quickly and cheaply processed.
- Capital costs for setting up a production line are reduced as the need for a kettle to set the carbohydrate concentrate level within the wort is eliminated.
- a screening device for a preparation used in the production of a beverage including a screening stage adapted to pass required components of the preparation while retaining waste beta-glucans or polyphenols or enzymes or micrological compounds or protein containing compounds within the screening stage.
- the required components passed through a screening stage may consist of water mixed with carbohydrate compounds.
- a filtering stage is required to remove waste compounds such as proteins, polyphenols, beta- glucans, enzymes or microbiological components that degrade the taste of a beer and make the beer appear cloudy.
- a screening stage as being configured to retain beta-glucans, enzymes, microbiological components, polyphenols and protein containing compounds within the screening stage.
- a screening stage may be configured to retain any number and type of waste products within the screening stage, and reference to the above types of chemicals should in no way be seen as limiting.
- a screening stage may include a filter membrane. Filter membranes can be produced to trap and retain particular types of compound with customised pore sizes, while allowing other types of chemicals to permeate through the membrane.
- a screening stage includes an ultra filtration membrane with pore sizes ranging from 0.001 to 0.1 micrometers. This may be contrasted with standard micro filtration membranes currently used in the production of beer, which have pore sizes ranging from 0.1 to 1.5 micrometers. Ultra filtration membranes may be used in the present invention to catch selected particles such as beta-glucans, enzymes and microbiological components, polyphenols or protein containing compounds while still allowing the remainder of the wort to permeate through the membrane.
- the invention discussed above which employs a screening stage also allows extended sparging of wort in the lauter tun.
- the screening stage will remove any beta-glucans formed within the lauter tun, the wort can be extensively diluted without fear of degrading the quality of the beer to be produced. This results in more efficient use of malt, allowing most of the carbohydrate present to be extracted.
- required components may be transferred straight on into further stages of processing the preparation. This immediate transfer decreases processing times for the preparation and eliminates requirements for storage tanks in the processing apparatus. However alternative embodiments may still employ storage tanks to store the screened preparation until it may be further processed by other preparation stages.
- the applicants believe that the use of such a screening stage also has the potential to removing yeast-inhibiting compounds that slow the fermentation of wort into beer.
- the use of such a screening stage in the present invention may substantially reduce the time period required for wort to ferment into beer.
- a processing device for a preparation used in the production of a beverage said processing device including a filtering device and a screening device substantially as described above.
- the combined elements discussed above may work together to eliminate the requirement for both a kettle and whirlpool stage as used in existing preparation methods. Protein and other waste products are initially removed via an ultra filtration membrane after the lauter tun. Secondly, water may be removed from the wort with the filtering stage reverse osmosis membrane which retains the required components of the wort as a retentate and recycles the permeate water back into the lauter tun.
- the volumes of water used in such a system are also limited. Clean sterile water can be obtained as a permeate from the reverse osmosis membrane then plumbed back into the lauter tun creating a closed system into which very little extra water needs to be added during processing of wort. The same treatment may also be applied to the retentates from the ultra filtration membrane that can be plumbed back into the 1 auter tun.
- Additional additives such as sugar or liquid hops may be added to the wort stream after the reverse osmosis membrane. Such additives may be provided at this stage to modify the resulting beer's flavour and colour as required.
- the present invention uses the filters discussed above in a completely new application for beer production.
- wort is pitched with yeast and transferred to a fermenter where it is left to ferment into beer.
- malted barley and hot water are added together and agitated in the mash tun 12 to form the basic components of wort.
- the wort is transferred to a lauter tun 13 and processed in substantially the same manner as that discussed with respect to figure 1.
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- General Engineering & Computer Science (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Food Science & Technology (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Distillation Of Fermentation Liquor, Processing Of Alcohols, Vinegar And Beer (AREA)
Abstract
Description
Claims
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AU31763/99A AU3176399A (en) | 1998-03-16 | 1999-03-16 | Improved method and apparatus for processing a preparation |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| NZ329960 | 1998-03-16 | ||
| NZ32996098 | 1998-03-16 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| WO1999047636A2 true WO1999047636A2 (en) | 1999-09-23 |
| WO1999047636A3 WO1999047636A3 (en) | 1999-11-25 |
Family
ID=19926638
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/NZ1999/000031 Ceased WO1999047636A2 (en) | 1998-03-16 | 1999-03-16 | Improved method and apparatus for processing a preparation |
Country Status (2)
| Country | Link |
|---|---|
| AU (1) | AU3176399A (en) |
| WO (1) | WO1999047636A2 (en) |
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2002028995A1 (en) * | 2000-10-05 | 2002-04-11 | Miller Brewing Company | Method of oxygenating yeast slurry using hydrophobic polymeric membranes |
| US7186428B1 (en) | 1999-11-23 | 2007-03-06 | Miller Brewing Company | Method of oxygenating yeast slurry using hydrophobic polymer membranes |
| WO2012011807A1 (en) * | 2010-07-22 | 2012-01-26 | Heineken Supply Chain B.V. | A method of stabilising yeast fermented beverages |
| US20140212542A1 (en) * | 2013-01-31 | 2014-07-31 | Manhoman Singh MINHAS | Method For Producing Gluten-Free Vodka From Gluten Sources |
| EP3026104A1 (en) * | 2014-11-25 | 2016-06-01 | Anheuser-Busch InBev S.A. | Beer or cider concentrate |
| WO2016083482A1 (en) * | 2014-11-25 | 2016-06-02 | Anheuser-Busch Inbev S.A. | Beer or cider concentrate |
| US9476021B2 (en) | 2010-07-22 | 2016-10-25 | Heineken Supply Chain B.V. | Method for the regeneration of PVPP from a membrane filter retentate after clarification and stabilization of a yeast fermented beverage |
| US9476020B2 (en) | 2010-07-22 | 2016-10-25 | Heineken Supply Chain B.V. | Method and apparatus for the recovery of PVPP after contact with a yeast fermented beverage by sedimentation separation |
| EP3101114A1 (en) * | 2015-06-04 | 2016-12-07 | Anheuser-Busch InBev S.A. | Beer concentrate |
| WO2016207079A1 (en) * | 2015-06-22 | 2016-12-29 | Anheuser-Busch Inbev S.A. | Beer or cider base |
| EP3165595A1 (en) * | 2015-11-09 | 2017-05-10 | Anheuser-Busch InBev S.A. | Beer or cider base |
| CN109689850A (en) * | 2016-06-01 | 2019-04-26 | 安海斯-布希英博股份有限公司 | The method for preparing the beverage based on malt |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3911697A1 (en) * | 1989-04-10 | 1990-10-25 | Gessner & Co Gmbh | USE OF A MICROPOROUS MEMBRANE CONSTRUCTED FROM A POLYMERIC SUBSTRATE AND A SURFACE COATING OF THE SUBSTRATE WITH A POLYACRYLIC ACID OR METHACRYLIC ACID DERIVATIVE FOR THE FILTRATION OF BEER |
| US5453285A (en) * | 1991-01-11 | 1995-09-26 | Heineken Technical Services B.V. | Process for membrane filtration of mash to produce wort |
| EP0762929B1 (en) * | 1994-05-30 | 2001-02-21 | Sartorius Ag | Hydrophilic porous membranes made of cross-linked cellulose hydrate, method of producing them and their use |
| DE4442393C1 (en) * | 1994-11-29 | 1995-09-21 | Umweltkompatible Prozestechnik | Separation of organic matter from wort vapour condensation |
| DE19757138C1 (en) * | 1997-12-20 | 1998-10-22 | Michael Eumann | Beer wort condensate processing apparatus |
-
1999
- 1999-03-16 WO PCT/NZ1999/000031 patent/WO1999047636A2/en not_active Ceased
- 1999-03-16 AU AU31763/99A patent/AU3176399A/en not_active Abandoned
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US7186428B1 (en) | 1999-11-23 | 2007-03-06 | Miller Brewing Company | Method of oxygenating yeast slurry using hydrophobic polymer membranes |
| WO2002028995A1 (en) * | 2000-10-05 | 2002-04-11 | Miller Brewing Company | Method of oxygenating yeast slurry using hydrophobic polymeric membranes |
| US9481859B2 (en) | 2010-07-22 | 2016-11-01 | Heineken Supply Chain B.V. | Method of stabilizing yeast fermented beverages |
| WO2012011807A1 (en) * | 2010-07-22 | 2012-01-26 | Heineken Supply Chain B.V. | A method of stabilising yeast fermented beverages |
| EA025808B1 (en) * | 2010-07-22 | 2017-01-30 | Хейнекен Сэпплай Чэйн Б.В. | Method of stabilising yeast fermented beverages |
| US9476021B2 (en) | 2010-07-22 | 2016-10-25 | Heineken Supply Chain B.V. | Method for the regeneration of PVPP from a membrane filter retentate after clarification and stabilization of a yeast fermented beverage |
| US9476020B2 (en) | 2010-07-22 | 2016-10-25 | Heineken Supply Chain B.V. | Method and apparatus for the recovery of PVPP after contact with a yeast fermented beverage by sedimentation separation |
| US20140212542A1 (en) * | 2013-01-31 | 2014-07-31 | Manhoman Singh MINHAS | Method For Producing Gluten-Free Vodka From Gluten Sources |
| EP3026104A1 (en) * | 2014-11-25 | 2016-06-01 | Anheuser-Busch InBev S.A. | Beer or cider concentrate |
| WO2016083482A1 (en) * | 2014-11-25 | 2016-06-02 | Anheuser-Busch Inbev S.A. | Beer or cider concentrate |
| EP3101114A1 (en) * | 2015-06-04 | 2016-12-07 | Anheuser-Busch InBev S.A. | Beer concentrate |
| WO2016207079A1 (en) * | 2015-06-22 | 2016-12-29 | Anheuser-Busch Inbev S.A. | Beer or cider base |
| KR20180019667A (en) * | 2015-06-22 | 2018-02-26 | 안헤우저-부시 인베브 에스.에이. | Beer or cider base |
| US11299696B2 (en) | 2015-06-22 | 2022-04-12 | Anheuser-Busch Inbev. S.A. | Beer or cider base |
| KR102658330B1 (en) * | 2015-06-22 | 2024-04-18 | 안헤우저-부시 인베브 에스.에이. | Method for producing aromatic beverages |
| EP3165595A1 (en) * | 2015-11-09 | 2017-05-10 | Anheuser-Busch InBev S.A. | Beer or cider base |
| CN109689850A (en) * | 2016-06-01 | 2019-04-26 | 安海斯-布希英博股份有限公司 | The method for preparing the beverage based on malt |
Also Published As
| Publication number | Publication date |
|---|---|
| WO1999047636A3 (en) | 1999-11-25 |
| AU3176399A (en) | 1999-10-11 |
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