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WO1999042794A1 - Device for measurement of characteristic reflection coefficient for electromagnetic waves in multiphase flour - Google Patents

Device for measurement of characteristic reflection coefficient for electromagnetic waves in multiphase flour Download PDF

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Publication number
WO1999042794A1
WO1999042794A1 PCT/NO1999/000148 NO9900148W WO9942794A1 WO 1999042794 A1 WO1999042794 A1 WO 1999042794A1 NO 9900148 W NO9900148 W NO 9900148W WO 9942794 A1 WO9942794 A1 WO 9942794A1
Authority
WO
WIPO (PCT)
Prior art keywords
probe
reflection coefficient
electromagnetic waves
measuring
terminal surface
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/NO1999/000148
Other languages
French (fr)
Other versions
WO1999042794A8 (en
Inventor
Øyvind ISAKSEN
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
CHRISTIAN MICHELSEN RESEARCH AS
Original Assignee
CHRISTIAN MICHELSEN RESEARCH AS
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by CHRISTIAN MICHELSEN RESEARCH AS filed Critical CHRISTIAN MICHELSEN RESEARCH AS
Priority to AU30612/99A priority Critical patent/AU3061299A/en
Publication of WO1999042794A1 publication Critical patent/WO1999042794A1/en
Publication of WO1999042794A8 publication Critical patent/WO1999042794A8/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N22/00Investigating or analysing materials by the use of microwaves or radio waves, i.e. electromagnetic waves with a wavelength of one millimetre or more
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01FMEASURING VOLUME, VOLUME FLOW, MASS FLOW OR LIQUID LEVEL; METERING BY VOLUME
    • G01F23/00Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm
    • G01F23/22Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water
    • G01F23/28Indicating or measuring liquid level or level of fluent solid material, e.g. indicating in terms of volume or indicating by means of an alarm by measuring physical variables, other than linear dimensions, pressure or weight, dependent on the level to be measured, e.g. by difference of heat transfer of steam or water by measuring the variations of parameters of electromagnetic or acoustic waves applied directly to the liquid or fluent solid material
    • G01F23/284Electromagnetic waves
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N33/00Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
    • G01N33/26Oils; Viscous liquids; Paints; Inks
    • G01N33/28Oils, i.e. hydrocarbon liquids
    • G01N33/2823Raw oil, drilling fluid or polyphasic mixtures

Definitions

  • the invention includes a device for measuring the characteristic reflection coefficient of high-frequency electromagnetic waves (normally above 100 kHz) in fluids and multiphase flow regimes.
  • 'multiphase flow regimes means volume flows in pipes mainly containing varying fractions of oil, gas and water. This type of flow regime is typical in crude oil production.
  • High-frequency electromagnetic waves are reflected by the interface between the device and the fluid (the combination of fluids and gases).
  • the reflection coefficient is a manifestation of the dielectric properties (permittivity) of the medium to be measured.
  • the relative permittivity of water is 80 and the relative permittivity of oil is 2.
  • the relative permittivity of gas is 1.
  • the device may be used in a measuring arrangement to distinguish between fluids of different permittivity.
  • the invention is designed as an open-ended coaxial probe and can replace the capacitive measuring principles used previously, which require installation of plate electrodes inside the pipe.
  • Measuring of permittivity in tanks and pipes is important for the characterisation of fluids and can for example be used for calculating the percentage of the water content in the fluid phase.
  • the fractions of gas and water will increase with the age of the oil wells. Particularly large gas fractions appear in wells where production is driven by gas pressure and in wells producing condensate. In some oil wells, the fraction of free gas may exceed 95 per cent. Free gas in the medium has previously been a complicating factor when measuring reflection coefficients/permittivity.
  • the probe may be used effectively where gas fractions range from 0 to 95 per cent.
  • the patent US-4503383 has already described a device (coaxial probe) and a procedure to determine interfaces in tanks containing two different fluids.
  • the coaxial probe is designed with level measurements in mind. Therefore, it is relatively long (60-90 cm) so that it can be inserted into tanks.
  • the central conductor is not in the same plane as the outer conductor and the excitation signals are low-frequency signals.
  • the procedure is a type of bulk measuring (measuring on the basis of a cross section) unlike local, detailed measuring.
  • a vertical multiphase flow with high gas fractions produces an annular flow regime with a fluid film along the walls of the pipe.
  • the design and placement of the probe are optimised for measuring the complex reflection coefficient of high-frequency electromagnetic waves in a local area near the pipe wall beside the terminal surface of the probe.
  • the penetration depth of the electric field can be changed by changing the diameter of the outer conductor.
  • the device is designed taking into account the high pressures and the high temperatures common in crude oil production tubings, but may also be used in characterisation of fluids in storage tanks and gas free flow regimes in pipes.
  • Figure 1 shows the invention installed in the wall (10) of a pipe or a tank.
  • the probe has a flat terminal surface which is in the same plane as the inner wall of the pipe/tank. The design contributes to the electric field being reduced to a small area beside the terminal surface of the probe.
  • the device (the probe) has a coupling for a coaxial cable ( 1 ).
  • the inner conductor (2) is insulated from the outer conductor (3) with a heat resistant, insulating plastic material (4) with a very low permittivity.
  • the probe consists of a female threaded sleeve (5) and a screw (6).
  • the screw presses against a conical metal ring (7) squeezing the conically formed insulation material (9) against the inner conductor.
  • An O-ring (8) provides a tight connection between the probe and the outside of the pipe wall/tank wall.

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  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Electromagnetism (AREA)
  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Pathology (AREA)
  • Immunology (AREA)
  • Biochemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Food Science & Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Medicinal Chemistry (AREA)
  • Thermal Sciences (AREA)
  • Fluid Mechanics (AREA)
  • Measurement Of Resistance Or Impedance (AREA)
  • Investigating Or Analyzing Materials By The Use Of Electric Means (AREA)
  • Measuring Volume Flow (AREA)

Abstract

The invention includes a device for measuring the reflection coefficient of high-frequency electromagnetic waves in fluids and multiphase flow regimes. The device is designed as an open-ended probe for measuring the reflection coefficient in a local area near the terminal surface of the probe. The probe is designed taking particular account of the high pressures and the high temperatures common in oil production tubings.

Description

DEVICE FOR MEASUREMENT OF CHARACTERISΗC REFLECΗON COEFFICIENT FOR ELECTROMAGNETIC WAVES IN MULTIPHASE FLOUR
The invention includes a device for measuring the characteristic reflection coefficient of high-frequency electromagnetic waves (normally above 100 kHz) in fluids and multiphase flow regimes. In this application, 'multiphase flow regimes' means volume flows in pipes mainly containing varying fractions of oil, gas and water. This type of flow regime is typical in crude oil production. High-frequency electromagnetic waves are reflected by the interface between the device and the fluid (the combination of fluids and gases). The reflection coefficient is a manifestation of the dielectric properties (permittivity) of the medium to be measured. The relative permittivity of water is 80 and the relative permittivity of oil is 2. For comparison, the relative permittivity of gas is 1. The device may be used in a measuring arrangement to distinguish between fluids of different permittivity. The invention is designed as an open-ended coaxial probe and can replace the capacitive measuring principles used previously, which require installation of plate electrodes inside the pipe.
Measuring of permittivity in tanks and pipes is important for the characterisation of fluids and can for example be used for calculating the percentage of the water content in the fluid phase. In the production of crude oil, the fractions of gas and water will increase with the age of the oil wells. Particularly large gas fractions appear in wells where production is driven by gas pressure and in wells producing condensate. In some oil wells, the fraction of free gas may exceed 95 per cent. Free gas in the medium has previously been a complicating factor when measuring reflection coefficients/permittivity. The probe may be used effectively where gas fractions range from 0 to 95 per cent. The patent US-4503383 has already described a device (coaxial probe) and a procedure to determine interfaces in tanks containing two different fluids. The coaxial probe is designed with level measurements in mind. Therefore, it is relatively long (60-90 cm) so that it can be inserted into tanks. The central conductor is not in the same plane as the outer conductor and the excitation signals are low-frequency signals. The procedure is a type of bulk measuring (measuring on the basis of a cross section) unlike local, detailed measuring.
A vertical multiphase flow with high gas fractions produces an annular flow regime with a fluid film along the walls of the pipe. According to the invention, the design and placement of the probe are optimised for measuring the complex reflection coefficient of high-frequency electromagnetic waves in a local area near the pipe wall beside the terminal surface of the probe. The penetration depth of the electric field can be changed by changing the diameter of the outer conductor.
The device is designed taking into account the high pressures and the high temperatures common in crude oil production tubings, but may also be used in characterisation of fluids in storage tanks and gas free flow regimes in pipes. Figure 1 shows the invention installed in the wall (10) of a pipe or a tank. The probe has a flat terminal surface which is in the same plane as the inner wall of the pipe/tank. The design contributes to the electric field being reduced to a small area beside the terminal surface of the probe. The device (the probe) has a coupling for a coaxial cable ( 1 ). The inner conductor (2) is insulated from the outer conductor (3) with a heat resistant, insulating plastic material (4) with a very low permittivity. Further, the probe consists of a female threaded sleeve (5) and a screw (6). The screw presses against a conical metal ring (7) squeezing the conically formed insulation material (9) against the inner conductor. An O-ring (8) provides a tight connection between the probe and the outside of the pipe wall/tank wall.

Claims

Patent claims
1. Device designed as an open-ended coaxial probe for measuring the characteristic reflection coefficient of electromagnetic waves in fluids and multiphase flow regimes characterised by the fact that the probe has a flat terminal surface which is installed in line with the inner wall of a tank or a pipe, so that the reflection coefficient can be measured near the wall, next to terminal surface of the probe.
2. Device as in claim 1 , which can be installed into the wall of a pipe or a tank, characterised by the fact that a version of the probe has heat resistant plastic material as the dielectric material in the terminal surface, and a metal clamp, with screw adjustment, which ensures a sealed connection between the inner and outer conductor at high pressures and temperatures.
PCT/NO1999/000148 1998-02-18 1999-02-15 Device for measurement of characteristic reflection coefficient for electromagnetic waves in multiphase flour Ceased WO1999042794A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AU30612/99A AU3061299A (en) 1998-02-18 1999-02-15 Device for measurement of characteristic reflection coefficient for electromagnetic waves in multiphase flour

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NO19990694 1998-02-18
NO990694A NO990694L (en) 1999-02-15 1999-02-15 Device for measuring characteristic reflection coefficient for electromagnetic waves in multi-phase tube current

Publications (2)

Publication Number Publication Date
WO1999042794A1 true WO1999042794A1 (en) 1999-08-26
WO1999042794A8 WO1999042794A8 (en) 1999-09-30

Family

ID=19902958

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/NO1999/000148 Ceased WO1999042794A1 (en) 1998-02-18 1999-02-15 Device for measurement of characteristic reflection coefficient for electromagnetic waves in multiphase flour

Country Status (3)

Country Link
AU (1) AU3061299A (en)
NO (1) NO990694L (en)
WO (1) WO1999042794A1 (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10019129A1 (en) * 2000-04-18 2001-10-25 Endress Hauser Gmbh Co Microwave tank level sensor, has tapered coupling unit avoids cavity resonances
US6831470B2 (en) 2001-05-30 2004-12-14 Schlumberger Technology Corporation Methods and apparatus for estimating on-line water conductivity of multiphase mixtures
WO2008029025A1 (en) * 2006-09-08 2008-03-13 Geoservices Equipements Method and device for measuring a multiple-phase fluid flowing through a pipe
WO2009129997A1 (en) * 2008-04-21 2009-10-29 Krohne Messtechnik Gmbh & Co. Kg Process connector for a measuring probe
CN102822642A (en) * 2011-04-06 2012-12-12 株式会社尼利可 Molten metal level measuring device
DE102012105281A1 (en) * 2012-06-18 2013-12-19 Endress + Hauser Gmbh + Co. Kg Level gauge and device for determining the relative permittivity

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4503383A (en) * 1982-01-07 1985-03-05 Agar Corporation, N.V. Device for detecting an interface between two fluids
US4885529A (en) * 1988-03-10 1989-12-05 Lee David O Identification of fluids and an interface between fluids by measuring complex impedance
US5675259A (en) * 1995-09-14 1997-10-07 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Method and apparatus for measuring fluid flow

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4503383A (en) * 1982-01-07 1985-03-05 Agar Corporation, N.V. Device for detecting an interface between two fluids
US4885529A (en) * 1988-03-10 1989-12-05 Lee David O Identification of fluids and an interface between fluids by measuring complex impedance
US5675259A (en) * 1995-09-14 1997-10-07 The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration Method and apparatus for measuring fluid flow

Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10019129A1 (en) * 2000-04-18 2001-10-25 Endress Hauser Gmbh Co Microwave tank level sensor, has tapered coupling unit avoids cavity resonances
US6831470B2 (en) 2001-05-30 2004-12-14 Schlumberger Technology Corporation Methods and apparatus for estimating on-line water conductivity of multiphase mixtures
WO2008029025A1 (en) * 2006-09-08 2008-03-13 Geoservices Equipements Method and device for measuring a multiple-phase fluid flowing through a pipe
FR2905761A1 (en) * 2006-09-08 2008-03-14 Geoservices METHOD AND DEVICE FOR MEASURING A POLYPHASIC FLUID CIRCULATING IN A CONDUIT.
US8220341B2 (en) 2006-09-08 2012-07-17 Geoservices Equipements Method and device for analyzing a multiple-phase fluid by measuring admittance using coaxial probes
WO2009129997A1 (en) * 2008-04-21 2009-10-29 Krohne Messtechnik Gmbh & Co. Kg Process connector for a measuring probe
CN102822642A (en) * 2011-04-06 2012-12-12 株式会社尼利可 Molten metal level measuring device
CN102822642B (en) * 2011-04-06 2015-09-09 株式会社尼利可 Molten metal level measurement Immersion nozzle and molten metal level measurement device
DE102012105281A1 (en) * 2012-06-18 2013-12-19 Endress + Hauser Gmbh + Co. Kg Level gauge and device for determining the relative permittivity
US10001398B2 (en) 2012-06-18 2018-06-19 Endress + Hauser Gmbh + Co. Kg Fill-level measuring device and apparatus for determining the dielectric constant

Also Published As

Publication number Publication date
NO990694D0 (en) 1999-02-15
WO1999042794A8 (en) 1999-09-30
AU3061299A (en) 1999-09-06
NO990694L (en) 1999-08-19

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