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WO1997038834A1 - A process for the realization of plates and panels consisting of exhausted olive husks of crushed olive stones and polypropylene, and derived product - Google Patents

A process for the realization of plates and panels consisting of exhausted olive husks of crushed olive stones and polypropylene, and derived product Download PDF

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Publication number
WO1997038834A1
WO1997038834A1 PCT/IT1996/000071 IT9600071W WO9738834A1 WO 1997038834 A1 WO1997038834 A1 WO 1997038834A1 IT 9600071 W IT9600071 W IT 9600071W WO 9738834 A1 WO9738834 A1 WO 9738834A1
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WO
WIPO (PCT)
Prior art keywords
plates
olive
realization
husks
polypropylene
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/IT1996/000071
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French (fr)
Inventor
Domenico Cristofaro
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Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to EP96910174A priority Critical patent/EP0833725A1/en
Priority to PCT/IT1996/000071 priority patent/WO1997038834A1/en
Publication of WO1997038834A1 publication Critical patent/WO1997038834A1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27NMANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
    • B27N1/00Pretreatment of moulding material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27NMANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
    • B27N3/00Manufacture of substantially flat articles, e.g. boards, from particles or fibres
    • B27N3/002Manufacture of substantially flat articles, e.g. boards, from particles or fibres characterised by the type of binder
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27NMANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
    • B27N3/00Manufacture of substantially flat articles, e.g. boards, from particles or fibres
    • B27N3/007Manufacture of substantially flat articles, e.g. boards, from particles or fibres and at least partly composed of recycled material
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27NMANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
    • B27N3/00Manufacture of substantially flat articles, e.g. boards, from particles or fibres
    • B27N3/08Moulding or pressing
    • B27N3/28Moulding or pressing characterised by using extrusion presses

Definitions

  • the present invention concerns a process for the relization of plates, panels and similar consisting of exhausted olive husks of crushed olive stones and polypropylene, and derived products .
  • the aim set forth is reached by the process according to the present invention, that determines a complete immersion into polypropylene of each single part of olive husks, of different granulometry, by means of the realization of a mixture at high temperature, that may be obtained with extrusion screws.
  • the percentage of the exhausted olive husks in the constitution mixture is provided for in order of 50-80% in weight.
  • the process according to the present invention comprises the following phases:
  • the olive husks are poured onto a conveyor belt that feeds a crushing mill with rotating blades, that provides for a variable granulometry according to tne featuies ol the final product;
  • the crushed material that flows out of the mill is extracted from the bottom by means of an Archimedean screw and led to the dryer, consisting of a steam burner that makes lower the moisture degree around a value of 5-6%;
  • the dried olive husks material is led to a storage silos and from there, by means of pneumatic tubings, transported into the feedbox;
  • the crushed olive stones play the role of filling, heat-resistant material (charge), while the polypropylene, that turns into plastic at a temperature about 230°C, has an amalgamating function;
  • the crushed material passes through a central extruder, while the polypropylene is plasticized in a lateral extruder and the plastic material comes out from a plane head;
  • the product obtained by means of the process according to the present invention is fed into a calender, where it is squeezed and brought to the desired thickness obtaining a plane plate that is now led onto a cooling down roll.
  • Shears and a piling up device allow to perform automatic repeating cuts with the same length and to pile the plates up.
  • three small blades are provided between the calender and the pulling device, for performing the cut of the lateral wastes, as well as the central cut, while the lateral bands are directly led into the mouth of each crushing and re-crushing mill and then prepared for the immediate use by means of an appropriate loading feedbox.
  • the plates having a variable thicknes between 0 and 25 mm, obtained at the end of the extrusion and calendering process, may be used, according to the present invention, as elements in many finished products, as, e.g.:
  • the plates With a feeding belt connected to said oven, the plates are placed onto the press bank in a number variable according to the final product to be obtained.
  • the press acts onto the pre-heated plates with a constant and uniform pessure, variable according to the thickness, to the mould of the components and to the final destination of the product.
  • the cooling phase takes place, during which the material returns to its final density.
  • a further, parallel and/or successive working cycle may be coupled to the one already described, having for purpose the use of the exhausted olive husks of greater granulometry (5 to 8 mm), discarded in the extrusion process and which, together with other olive husks of smaller granulometry, may be mineralized so as t be used as inert in mixing processes with many binders, in particular with cement.
  • the obtained conglomerate has a high resistance to compression, provided by the short fibre of the olive husks, and may therefore be used for the production of industrial modular elements, like bricks, and in particular for the production of hand-made vibro-compressed materials like the self-blocking blocks for external flooring which at present are realized with inert materials taken from quarries and/or rivers.
  • the product obtained according to said variant is a valid alternative to the exploitation of the ground, with a further protection of the ambient.
  • the plates or panels obtained with exhausted olive husks may be reinforced by using glass-fibre, polyester or carbon, in a coupling between the plate and the fibres (one-layer or multi-layer), as well as a component of the mixture, in the mixing and extruding phase of the plates.
  • This treatment considerably improves the physical and mechanical features of the final product, in particular those that concern the elasticity module and the pulling resistance, thus opening the possibility of use in many uses difficult for the conventional panels like lofts, constructions with lamellar beams, etc.
  • fibres allows to reduce, maitaining the known resistance, the thicknesses of the panels, with a further improvement of the efficiency for what concerns the weight, the transport, the assemblying, the working.
  • a tridimensional aspect may be given to the plates and pannels obtained according to the present invention, by a simple printing operation. It is known that this shaping - that concerns the thickness of the panel and that may also concerns the aesthetic aspect (ashlar, edging, frames etc.) as well as the statical aspect (ribbings etc.) - may be obtained, in the conventional panels and in wood only by means of complex and delicate working cycles (panelgraphing) , as well as by means of coupling machine-shaped elements according to their thickness and final shape.

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Wood Science & Technology (AREA)
  • Forests & Forestry (AREA)
  • Dry Formation Of Fiberboard And The Like (AREA)

Abstract

The process according to the present invention provides the use of exhausted olive husks, obtained from the crushing of olives, for playing the role of filling, heat-resistant material, in mixture with the polypropylene, that turns into plastic at a temperature about 230 °C, and that has an amalgamating function, so as to determine a complete immersion into the polypropylene of each single particle of olive husks, of different granulometry, by means of the realization of a high temperature mixture, for the realization of listel panels, plates charged with exhausted olive husks powder, multi-layer panels and similar.

Description

"A PROCESS FOR THE REALIZATION OF PLATES AND PANELS CONSISTING OF EXHAUSTED OLIVE HUSKS OF CRUSHED OLIVE STONES AND POLYPROPYLENE, AND DERIVED PRODUCT"
The present invention concerns a process for the relization of plates, panels and similar consisting of exhausted olive husks of crushed olive stones and polypropylene, and derived products .
The problem of the discharge of the materials resultant from the working in the oil-mills is well known: up to now, these materials are delivered on the soil as compost or burned, with great disadvantages for the ecological ambient.
It is the aim of the present invention to positively exploit the olive husks, i.e. the final product of this working, by using it as a constructive means (charge), by mixing it up with plastic materials for the realization of plates and structures of any shape, dimension and colour, for many different uses.
The aim set forth is reached by the process according to the present invention, that determines a complete immersion into polypropylene of each single part of olive husks, of different granulometry, by means of the realization of a mixture at high temperature, that may be obtained with extrusion screws.
For obtaining the many kinds of derived products according to the aim of the present invention, the percentage of the exhausted olive husks in the constitution mixture is provided for in order of 50-80% in weight.
The present invention will be described more in detail hereinbelow, relating to some preferred embodiments.
In one embodiment, the process according to the present invention comprises the following phases:
- the olive husks are poured onto a conveyor belt that feeds a crushing mill with rotating blades, that provides for a variable granulometry according to tne featuies ol the final product;
- the crushed material that flows out of the mill is extracted from the bottom by means of an Archimedean screw and led to the dryer, consisting of a steam burner that makes lower the moisture degree around a value of 5-6%; - by means of a second Archimedean screw, the dried olive husks material is led to a storage silos and from there, by means of pneumatic tubings, transported into the feedbox;
- during that extrusion process, the crushed olive stones play the role of filling, heat-resistant material (charge), while the polypropylene, that turns into plastic at a temperature about 230°C, has an amalgamating function;
- in the plastiσization phase, the crushed material passes through a central extruder, while the polypropylene is plasticized in a lateral extruder and the plastic material comes out from a plane head;
- by means of the shape of the extruders' screws, assembled to injection techniques of the polymer, a plasticized mixture is obtained with a percentage variable between 50% and 80% of crushed exhausted olive husks, with an optimal dispersion, as all particles of olive husks are immersed in said polypropylene.
For the realization,in particular of one-layer and multi-layer plates, the product obtained by means of the process according to the present invention is fed into a calender, where it is squeezed and brought to the desired thickness obtaining a plane plate that is now led onto a cooling down roll.
Shears and a piling up device allow to perform automatic repeating cuts with the same length and to pile the plates up.
Furthermore, three small blades are provided between the calender and the pulling device, for performing the cut of the lateral wastes, as well as the central cut, while the lateral bands are directly led into the mouth of each crushing and re-crushing mill and then prepared for the immediate use by means of an appropriate loading feedbox.
It shall be underlined that in the process according to the present invention, virgin polypropylene as well as the recycled one may be used and that therefore two storing silos are provided, one for each kind of polypropylene. For both kinds, and in particular for the recycled one, of which usually the exact origin is unknown, the process according to the present invention provides that it must have an MFI value between 2 and 10, so as to maintain a high productivity. For what concerns the products eventually derived from the process according to the present invention, in some variants thereof they may be the following:
- the above mentioned listel panels;
- plates loaded with exhausted olive husk powder;
- one-layer and multi-layer panels.
The plates, having a variable thicknes between 0 and 25 mm, obtained at the end of the extrusion and calendering process, may be used, according to the present invention, as elements in many finished products, as, e.g.:
- they may form one or more layers of multi-layer panels consisting of different materials like wood, rubber, etc;
- they may be coupled to each other for obtaining the desired thicknesses and physical and thechnological features;
- they may be reinforced with fibres, inserting also synthetic materials as glass-fibre, polyester, carbon-fibre, for improving their technological efficiency;
- they may be coated and ennobled with different materials, like aluminium, copper, essence of wood, paper with serigraphies , moquette, polypropylene, etc.; - they may be hot-shaped and printed according to the desired drawing and geometry.
All above described workings must be performed by pre-heating the single plates in an appropriate oven for bringing them to a temperature depending on a plurality of factors and that may vary between 80°C and 130°C.
With a feeding belt connected to said oven, the plates are placed onto the press bank in a number variable according to the final product to be obtained. The press acts onto the pre-heated plates with a constant and uniform pessure, variable according to the thickness, to the mould of the components and to the final destination of the product. During pressing - which depends on above mentioned variants - the cooling phase takes place, during which the material returns to its final density.
The panels thus obtained are now edged and squared.
IP. a possible variant, a further, parallel and/or successive working cycle may be coupled to the one already described, having for purpose the use of the exhausted olive husks of greater granulometry (5 to 8 mm), discarded in the extrusion process and which, together with other olive husks of smaller granulometry, may be mineralized so as t be used as inert in mixing processes with many binders, in particular with cement.
The obtained conglomerate has a high resistance to compression, provided by the short fibre of the olive husks, and may therefore be used for the production of industrial modular elements, like bricks, and in particular for the production of hand-made vibro-compressed materials like the self-blocking blocks for external flooring which at present are realized with inert materials taken from quarries and/or rivers.
The product obtained according to said variant is a valid alternative to the exploitation of the ground, with a further protection of the ambient.
In a further variant according to the present invention, the plates or panels obtained with exhausted olive husks may be reinforced by using glass-fibre, polyester or carbon, in a coupling between the plate and the fibres (one-layer or multi-layer), as well as a component of the mixture, in the mixing and extruding phase of the plates. This treatment considerably improves the physical and mechanical features of the final product, in particular those that concern the elasticity module and the pulling resistance, thus opening the possibility of use in many uses difficult for the conventional panels like lofts, constructions with lamellar beams, etc.
Furthermore, the use of said fibres allows to reduce, maitaining the known resistance, the thicknesses of the panels, with a further improvement of the efficiency for what concerns the weight, the transport, the assemblying, the working.
A tridimensional aspect may be given to the plates and pannels obtained according to the present invention, by a simple printing operation. It is known that this shaping - that concerns the thickness of the panel and that may also concerns the aesthetic aspect (ashlar, edging, frames etc.) as well as the statical aspect (ribbings etc.) - may be obtained, in the conventional panels and in wood only by means of complex and delicate working cycles (panelgraphing) , as well as by means of coupling machine-shaped elements according to their thickness and final shape.
It is evident that these operation considerably increase the cost of the product, due to the handcraft and apparatuses as well as to the use of raw materials.

Claims

1. A process for the relization of plates, panels and similar consisting of exhausted olive husks of crushed olive stones and polypropylene, and derived products, and that determines a complete immersion into polypropylene of each single part of olive husks, of different granulometry, by means of the realization of a mixture at high temperature, that may be obtained with extrusion screws, and characterized in the following phases:
- the olive husks are poured onto a conveyor belt that feeds a crushing mill with rotating blades, that provides for a variable granulometry according to the features of the final product;
- the crushed material that flows out of the mill is extracted from the bottom by means of an Archimedean screw and led to the dryer, consisting of a steam burner that makes lower the moisture degree around a value of 5-6%;
- by means of a second Archimedean screw, the dried olive husks material is led to a storage silos and from there, by means of pneumatic tubings, transported into the feedbox;
- during that extrusion process, the crushed olive stones play the role of filling, heat-resistant material (charge), while the polypropylene, that 1]
turns into plastic at a temperature about 230°C, has an amalgamating function;
- in the plasticization phase, the crushed material passes through a central extruder, while the polypropylene is plasticized in a lateral extruder and the plastic material comes out from a plane head;
- by means of the shape of the extruders ' screws, assembled to injection techniques of the polymer, a plasticized mixture is obtained with a percentage variable between 50% and 80% of crushed exhausted olive husks, with an optimal dispersion, as all particles of olive husks are immersed in said polypropylene.
2. A product derived from the process according to claim 1, characterized in obtaining listel panels.
3. A product derived from the process according to claim 1, chracterized in obtaining plates loaded with exhaust olive husks powder.
4. A product derived from the process according to claim 1, characterized in ontaining multi-layer panels.
5. A process according to claim 1 for the realization of listel plates , characterized in that the product is fed into a calender, where it is squeezed and brought to the des ired thickness obtaining a plane plate that is now led onto a cooling down rolls Shears and a piling up device allow to perform automatic repeating cuts with the same length and to pile the plates up; and three small blades are provided between the calender and the pulling device , for performing the cut of the lateral wastes , as well as the central cut , while the lateral bands are directly led into the mouth of each crushing and re-crushing mill and then prepared for the immediate use by means of an appropriate loading feedbox.
6. A product derived from the process according to clami 1 , characterized in the realization of plates with variable thickness , obtained at the end of an extrusion and calendering process , and used as components of f inished products , in particular for realizing one or more layers of multi-layer panels composed with dif ferent materials like wood, rubber and similar.
7 . A product derived from the process according to claim 1 , characterized in the realization of plates with different thickness, obtained at the end of the extrusion and calendering process, like glass-fibre-reinfreed plates, alternated with synthetic material (glass-fibre, polyester, carbon-fibre, etc. ) .
8. A product derived from the process according to claim 1, characterized in the realization of plates with variable thicknesses, obtained at the end of the extrusion and calendering process, coated with different and/or hot-shaped and printed materils.
9. A process according to claim 1 ,characterized in the use of exhausted olive husks with great granulometry ( 5 to 8 mm), decarded from the extrusion cycle, mineralized together with olive husks with smaller granulometru, to as to be used as inert material in mixing processes with different binders, in particular with cement.
10. A product derived from the process according to claim 1, characterized in the realization of plates or panels out of exhausted olive husks, reinforced by using glass-fibre, polyester or carbon, in a coupling between the plate and the fibres (one-layer or multi-layer), as well as a component of the mixture, in the mixing and extruding phase of the plates.
PCT/IT1996/000071 1996-04-12 1996-04-12 A process for the realization of plates and panels consisting of exhausted olive husks of crushed olive stones and polypropylene, and derived product Ceased WO1997038834A1 (en)

Priority Applications (2)

Application Number Priority Date Filing Date Title
EP96910174A EP0833725A1 (en) 1996-04-12 1996-04-12 A process for the realization of plates and panels consisting of exhausted olive husks of crushed olive stones and polypropylene, and derived product
PCT/IT1996/000071 WO1997038834A1 (en) 1996-04-12 1996-04-12 A process for the realization of plates and panels consisting of exhausted olive husks of crushed olive stones and polypropylene, and derived product

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/IT1996/000071 WO1997038834A1 (en) 1996-04-12 1996-04-12 A process for the realization of plates and panels consisting of exhausted olive husks of crushed olive stones and polypropylene, and derived product

Publications (1)

Publication Number Publication Date
WO1997038834A1 true WO1997038834A1 (en) 1997-10-23

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WO (1) WO1997038834A1 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001096256A3 (en) * 2000-06-13 2002-05-23 Meinhard Meier Component in the form of a plate, a strand or a moulded body made out of natural fibres or shavings linked by a binding agent, having the form of a semi-finished or finished product, method for the production thereof, and method for coating or repairing the surface of such moulded bodies
WO2016071932A1 (en) 2014-11-06 2016-05-12 Selex Es S.P.A. Eco-friendly thermoplastic conformal coating for antenna array systems
WO2019234460A1 (en) * 2018-06-05 2019-12-12 Makrygeorgou Alexandra Environmentally friendly olive leaf panels

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114090327B (en) * 2022-01-20 2022-05-17 浙江吉利控股集团有限公司 Single-particle error processing method, system and device

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2427888A1 (en) * 1978-06-08 1980-01-04 Stavrakellis Panayotis NEW WOODY PRODUCT, PROCESS FOR ITS MANUFACTURE AND APPLICATION
EP0292628A2 (en) * 1987-05-25 1988-11-30 Panayiotis Stavrakellis Synthetic wood composition from fruit kernels or shells and/or marble chips
EP0292584A1 (en) * 1987-05-23 1988-11-30 Mario Miani Method of making panels, apparatus for carrying out the method and panels obtained thereby
EP0683024A2 (en) * 1994-05-20 1995-11-22 LIGNOTOCK GmbH Process for making shaped articles

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2427888A1 (en) * 1978-06-08 1980-01-04 Stavrakellis Panayotis NEW WOODY PRODUCT, PROCESS FOR ITS MANUFACTURE AND APPLICATION
EP0292584A1 (en) * 1987-05-23 1988-11-30 Mario Miani Method of making panels, apparatus for carrying out the method and panels obtained thereby
EP0292628A2 (en) * 1987-05-25 1988-11-30 Panayiotis Stavrakellis Synthetic wood composition from fruit kernels or shells and/or marble chips
EP0683024A2 (en) * 1994-05-20 1995-11-22 LIGNOTOCK GmbH Process for making shaped articles

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2001096256A3 (en) * 2000-06-13 2002-05-23 Meinhard Meier Component in the form of a plate, a strand or a moulded body made out of natural fibres or shavings linked by a binding agent, having the form of a semi-finished or finished product, method for the production thereof, and method for coating or repairing the surface of such moulded bodies
WO2016071932A1 (en) 2014-11-06 2016-05-12 Selex Es S.P.A. Eco-friendly thermoplastic conformal coating for antenna array systems
US10158166B2 (en) 2014-11-06 2018-12-18 Leonardo S.P.A. Eco-friendly thermoplastic conformal coating for antenna array systems
WO2019234460A1 (en) * 2018-06-05 2019-12-12 Makrygeorgou Alexandra Environmentally friendly olive leaf panels
US11845197B2 (en) 2018-06-05 2023-12-19 Alexandra MAKRYGEORGOU Environmentally friendly olive leaf panels

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Publication number Publication date
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