WO1997015681B1 - Procedes d'extraction de polyhydroxyalkanoates a partir de vegetaux - Google Patents
Procedes d'extraction de polyhydroxyalkanoates a partir de vegetauxInfo
- Publication number
- WO1997015681B1 WO1997015681B1 PCT/US1996/016921 US9616921W WO9715681B1 WO 1997015681 B1 WO1997015681 B1 WO 1997015681B1 US 9616921 W US9616921 W US 9616921W WO 9715681 B1 WO9715681 B1 WO 9715681B1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- pha
- oil
- group
- plant
- biomass
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
Abstract
Cette invention concerne des procédés permettant d'extraire des polyhydroxyalkanoates ('PHA') de végétaux tels que des plantes oléagineuses transgéniques. Ces procédés permettent avantageusement de récupérer à la fois les PHA et l'huile de la biomasse végétale. Dans une réalisation, afin d'isoler les PHA, on prétraite une biomasse dérivée d'une plante oléagineuse, par exemple en procédant à la mouture, l'écrasement ou l'aplatissement par rouleau. Puis on extrait l'huile de la biomasse en utilisant un premier solvant dans lequel l'huile est soluble et dans lequel les PHA ne sont pas fortement solubles de façon à extraire l'huile. On peut ensuite extraire la biomasse en utilisant un second solvant dans lequel le PHA est soluble, de façon à séparer PHA et biomasse. Une autre possibilité consiste à traiter la biomasse contenant les PHA avec un agent chimique ou biochimique, tel qu'un enzyme, de manière à transformer chimiquement le PHA en un dérivé de PHA. On extrait ensuite ce dérivé de PHA du mélange au moyen, par exemple, d'un processus de séparation physique du type distillation, extraction ou chromatographie. La mise en oeuvre de ce procédé permet, avantageusement, d'extraire et de purifier, à grande échelle, les huiles végétales, les PHA et dérivés de PHA, de végétaux contenant de l'huile tels que des végétaux oléagineux transgéniques.
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CA 2234965 CA2234965C (fr) | 1995-10-26 | 1996-10-23 | Procedes d'extraction de polyhydroxyalkanoates a partir de vegetaux |
| EP96936839A EP0859858B1 (fr) | 1995-10-26 | 1996-10-23 | Procedes d'extraction de polyhydroxyalkanoates a partir de vegetaux |
| DE69637253T DE69637253T2 (de) | 1995-10-26 | 1996-10-23 | Verfahren zur isolierung von polyhydroxyalkanoaten aus pflanzen |
| JP51672197A JP2001517070A (ja) | 1995-10-26 | 1996-10-23 | 植物からポリヒドロキシアルカノエートを単離する方法 |
| AU74663/96A AU722033B2 (en) | 1995-10-26 | 1996-10-23 | Methods for isolating polyhydroxyalkanoates from plants |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US08/548,840 US6083729A (en) | 1995-10-26 | 1995-10-26 | Methods for isolating polyhydroxyalkanoates from plants |
| US548,840 | 1995-10-26 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| WO1997015681A1 WO1997015681A1 (fr) | 1997-05-01 |
| WO1997015681B1 true WO1997015681B1 (fr) | 1997-06-19 |
| WO1997015681A9 WO1997015681A9 (fr) | 1997-07-17 |
Family
ID=24190604
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/US1996/016921 Ceased WO1997015681A1 (fr) | 1995-10-26 | 1996-10-23 | Procedes d'extraction de polyhydroxyalkanoates a partir de vegetaux |
Country Status (7)
| Country | Link |
|---|---|
| US (2) | US6083729A (fr) |
| EP (1) | EP0859858B1 (fr) |
| JP (4) | JP2001517070A (fr) |
| AT (1) | ATE373722T1 (fr) |
| AU (1) | AU722033B2 (fr) |
| DE (1) | DE69637253T2 (fr) |
| WO (1) | WO1997015681A1 (fr) |
Families Citing this family (64)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6083729A (en) * | 1995-10-26 | 2000-07-04 | Metabolix, Inc. | Methods for isolating polyhydroxyalkanoates from plants |
| EP0975788A1 (fr) * | 1997-04-15 | 2000-02-02 | Monsanto Company | Procedes d'extraction et de recuperation de pha a l'aide de solvants non halogenes |
| DE69837914T2 (de) * | 1997-04-15 | 2008-02-21 | Metabolix, Inc., Cambridge | Hochtemperatur-PHA Extraktion mit schlecht-lösenden Lösungsmittel für PHA |
| DK1045642T3 (da) | 1998-01-07 | 2003-03-03 | Metabolix Inc | Dyrefodersammensætninger |
| US6586658B1 (en) | 1998-03-06 | 2003-07-01 | Metabolix, Inc. | Modification of fatty acid metabolism in plants |
| EP1070135B1 (fr) | 1998-04-08 | 2010-02-24 | Metabolix, Inc. | Procedes pour la separation et la purification des biopolymeres |
| DE69932818T2 (de) | 1998-06-09 | 2007-01-18 | Metabolix, Inc., Cambridge | Verfahren und vorrichtung zur herstellung von amorphen polymersuspensionen |
| ATE283056T1 (de) | 1998-07-22 | 2004-12-15 | Metabolix Inc | Nahrungs- und therapeutische verwendung von hydroxyalkanoat oligomere |
| EP1975236B1 (fr) | 1998-08-04 | 2015-05-06 | Metabolix, Inc. | Production de polyhydroxyalkanoate à partir de polyols |
| EP2305324B1 (fr) | 1999-03-25 | 2014-09-17 | Metabolix, Inc. | Dispositifs médicaux et applications de polymères polyhydroxyalkanoates |
| US6340580B1 (en) * | 1999-05-12 | 2002-01-22 | Metabolix, Inc. | Methods for purifying polyhydroxy alkanoates |
| US6451564B1 (en) | 1999-07-02 | 2002-09-17 | Massachusetts Institute Of Technology | Methods for producing L-isoleucine |
| WO2001019361A2 (fr) * | 1999-09-14 | 2001-03-22 | Tepha, Inc. | Utilisations therapeutiques de polymeres et d'oligomeres a base de gamma-hydroxybutyrate (ghb) |
| DE10013514C2 (de) * | 2000-03-14 | 2002-06-27 | Ufz Leipzighalle Gmbh | Verfahren zur Gewinnung von Polyhydroxyalkanoaten (PHA) oder deren Copolymeren |
| US20020077269A1 (en) * | 2000-10-27 | 2002-06-20 | Whitehouse Robert S. | Alkanoic acid ester monomer compositions and methods of making same |
| JP3768799B2 (ja) * | 2000-10-30 | 2006-04-19 | キヤノン株式会社 | 置換脂肪酸エステル化物を原料とするポリヒドロキシアルカノエートの製造方法 |
| WO2004006691A2 (fr) * | 2002-07-12 | 2004-01-22 | The Texas A & M University System | Procede enzymatique permettant de produire des aliments et des aliments pour animaux, et ingredients correspondants |
| WO2004013204A2 (fr) * | 2002-08-06 | 2004-02-12 | Metabolix Inc. | Procedes d'extraction de polymeres |
| JP5079321B2 (ja) * | 2003-02-21 | 2012-11-21 | メタボリックス インコーポレイティッド | Pha接着組成物 |
| US7781539B2 (en) * | 2003-02-21 | 2010-08-24 | Metabolix Inc. | PHA blends |
| ES2819189T3 (es) | 2003-05-08 | 2021-04-15 | Tepha Inc | Tejidos y fibras médicos de polihidroxialcanoato |
| US7579176B2 (en) | 2003-10-15 | 2009-08-25 | Newlight Technologies, Llc | Method for the production of polyhydroxyalkanoic acid |
| US8735113B2 (en) | 2003-10-15 | 2014-05-27 | Newlight Technologies, Llc | Methods and systems for production of polyhydroxyalkanoate |
| US7745197B1 (en) | 2003-10-15 | 2010-06-29 | Newlight Technologies, Llc | Process for the utilization of ruminant animal methane emissions |
| JP4455413B2 (ja) * | 2004-06-11 | 2010-04-21 | キヤノン株式会社 | ビニル基、エステル基、カルボキシル基並びにスルホン酸基を有するポリヒドロキシアルカン酸並びにその製造方法 |
| EP1758948B1 (fr) * | 2004-06-11 | 2009-05-13 | Canon Kabushiki Kaisha | Acide polyhydroxyalcanoïque comportant un groupe vinyle, ester, carboxyle ou acide sulfonique et procédé de production de cet acide |
| JP4741883B2 (ja) * | 2004-06-11 | 2011-08-10 | キヤノン株式会社 | エステル基、カルボキシル基並びにスルホン酸基を有するポリヒドロキシアルカノエート並びにその製造方法 |
| WO2005121207A2 (fr) * | 2004-06-11 | 2005-12-22 | Canon Kabushiki Kaisha | Polyhydroxyalcanoate comportant un groupe vinyle, un groupe ester, un groupe carboxyle et un groupe sulfonique, et procédé de production de ce composé |
| PL1778305T3 (pl) | 2004-08-03 | 2011-04-29 | Tepha Inc | Szwy z polihydroksyalkanianów nieulegające zwijaniu się |
| CA2581458A1 (fr) * | 2006-03-22 | 2007-09-22 | National Research Council Of Canada | Methode de production de poly-.beta.-hydroxybutyrate |
| US8377151B2 (en) * | 2006-07-19 | 2013-02-19 | Zackery Allen McMurry | Process for producing a renewable biofuel from waste water treatment plants |
| US20080102176A1 (en) * | 2006-10-26 | 2008-05-01 | Wu Ying Fong | Method for Extracting Plant Fats |
| CN100434134C (zh) * | 2006-11-07 | 2008-11-19 | 苏州市兴科现代中药工艺装备开发有限公司 | 一种连续提取分离植物中有效成分的方法 |
| WO2008120343A1 (fr) * | 2007-03-29 | 2008-10-09 | Minoru Nakahama | Procédé d'utilisation d'une installation de biomasse et biomasse |
| TW200846475A (en) * | 2007-05-29 | 2008-12-01 | Univ Yuan Ze | High purity polyhydroxylalkanoates (PHAs) copolymer and manufacturing method thereof |
| CA2761803A1 (fr) * | 2009-05-14 | 2010-11-18 | University Of North Dakota | Procede pour la creation de produits a teneur elevee en carbone a partir de biomasse huileuse |
| US20120165500A1 (en) | 2009-08-27 | 2012-06-28 | Newlight Technologies, Llc | Process for the production of polyhydroxyalkanoates |
| US9402415B2 (en) | 2010-04-21 | 2016-08-02 | R. J. Reynolds Tobacco Company | Tobacco seed-derived components and materials |
| ES2383383B1 (es) * | 2010-11-24 | 2013-02-21 | Jesús Zorrilla González | Extracción de polihidroxialcanoatos (pha), a partir de biomasa oleaginosa y utilización del disolvente obtenido para la extracción de polihidroxialcanoatos (pha), a partir de biomasa. |
| US9458476B2 (en) | 2011-04-18 | 2016-10-04 | R.J. Reynolds Tobacco Company | Method for producing glycerin from tobacco |
| US20130125907A1 (en) | 2011-11-17 | 2013-05-23 | Michael Francis Dube | Method for Producing Triethyl Citrate from Tobacco |
| US12060597B2 (en) | 2011-12-02 | 2024-08-13 | Newlight Technologies, Inc. | Polyhydroxyalkanoate production methods and systems for same |
| US9085784B1 (en) | 2012-03-29 | 2015-07-21 | Newlight Technologies, Llc | Polyhydroxyalkanoate production methods and materials and microorganisms used in same |
| US20200347417A1 (en) | 2012-03-29 | 2020-11-05 | Newlight Technologies, Inc | Polyhydroxyalkanoate production methods and materials and microorganisms used in same |
| ES2448823B1 (es) | 2012-08-14 | 2014-10-13 | Neol Biosolutions, S.A. | Producción de bioplásticos |
| CN104755538B (zh) | 2012-08-17 | 2018-08-31 | Cj 第一制糖株式会社 | 用于聚合物共混物的生物基橡胶改性剂 |
| US9289011B2 (en) | 2013-03-07 | 2016-03-22 | R.J. Reynolds Tobacco Company | Method for producing lutein from tobacco |
| WO2014194220A1 (fr) | 2013-05-30 | 2014-12-04 | Metabolix, Inc. | Mélanges de recyclat |
| US20140356295A1 (en) | 2013-06-03 | 2014-12-04 | R.J. Reynolds Tobacco Company | Cosmetic compositions comprising tobacco seed-derived component |
| US9163202B2 (en) | 2013-08-02 | 2015-10-20 | Eastman Chemical Company | Aqueous cleaning compositions including an alkyl 3-hydroxybutyrate |
| US9255059B2 (en) | 2013-08-02 | 2016-02-09 | Eastman Chemical Company | Method for producing an alkyl 3-hydroxybutyrate |
| US9388114B2 (en) | 2013-08-02 | 2016-07-12 | Eastman Chemical Company | Compositions including an alkyl 3-hydroxybutyrate |
| US9249378B2 (en) | 2013-08-02 | 2016-02-02 | Eastman Chemical Company | Aqueous cleaning compositions having enhanced properties |
| US9265284B2 (en) | 2014-01-17 | 2016-02-23 | R.J. Reynolds Tobacco Company | Process for producing flavorants and related materials |
| WO2015149029A1 (fr) | 2014-03-27 | 2015-10-01 | Metabolix, Inc. | Systèmes polymères fortement chargés |
| CA2958747C (fr) | 2014-08-15 | 2022-08-16 | Tepha, Inc. | Sutures auto-retentive de poly-4-hydroxybutyrate et de copolymeres de celui-ci |
| EP4591894A3 (fr) | 2014-12-11 | 2025-08-27 | Tepha, Inc. | Procédés d'orientation de fil multifilament et monofilaments de poly-4-hydroxybutyrate et copolymères correspondants |
| US10626521B2 (en) | 2014-12-11 | 2020-04-21 | Tepha, Inc. | Methods of manufacturing mesh sutures from poly-4-hydroxybutyrate and copolymers thereof |
| US10881133B2 (en) | 2015-04-16 | 2021-01-05 | R.J. Reynolds Tobacco Company | Tobacco-derived cellulosic sugar |
| US10499684B2 (en) | 2016-01-28 | 2019-12-10 | R.J. Reynolds Tobacco Company | Tobacco-derived flavorants |
| US11154087B2 (en) | 2016-02-02 | 2021-10-26 | R.J. Reynolds Tobacco Company | Method for preparing flavorful compounds isolated from black liquor and products incorporating the flavorful compounds |
| US11091446B2 (en) | 2017-03-24 | 2021-08-17 | R.J. Reynolds Tobacco Company | Methods of selectively forming substituted pyrazines |
| CZ308735B6 (cs) * | 2017-06-02 | 2021-04-14 | Vysoké Učení Technické V Brně | Způsob rozpouštění biodegradabilních polyesterů |
| KR20230070465A (ko) | 2020-09-21 | 2023-05-23 | 그랜트 인더스트리스, 아이엔씨. | 화장품에 사용하기 위한 바이오 기반, 생분해성 복합 분말 |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB8311677D0 (en) * | 1983-04-28 | 1983-06-02 | Ici Plc | Extraction process |
| US5245023A (en) * | 1987-06-29 | 1993-09-14 | Massachusetts Institute Of Technology | Method for producing novel polyester biopolymers |
| US5229279A (en) * | 1987-06-29 | 1993-07-20 | Massachusetts Institute Of Technology | Method for producing novel polyester biopolymers |
| US5250430A (en) * | 1987-06-29 | 1993-10-05 | Massachusetts Institute Of Technology | Polyhydroxyalkanoate polymerase |
| EP0482077B1 (fr) * | 1989-07-10 | 1998-10-21 | Massachusetts Institute Of Technology | Procédé de production de biopolymères à base de polyesters |
| GB9108756D0 (en) * | 1991-04-24 | 1991-06-12 | Ici Plc | Production of polyalkanoate in plants |
| GB9115245D0 (en) * | 1991-07-16 | 1991-08-28 | Ici Plc | Production of polyalkanoate |
| EP0595896B1 (fr) * | 1991-07-19 | 2005-05-18 | Michigan State University | Plantes transgeniques produisant des polyhydroxyalcanoates |
| US5610041A (en) * | 1991-07-19 | 1997-03-11 | Board Of Trustees Operating Michigan State University | Processes for producing polyhydroxybutyrate and related polyhydroxyalkanoates in the plastids of higher plants |
| US5422257A (en) * | 1991-11-29 | 1995-06-06 | Firmenich Sa | Method for obtaining poly-β-hydroxyoctanoic acid via solvent extraction |
| BR9307130A (pt) * | 1992-09-28 | 1999-03-30 | Zeneca Ltd | Composição de polímero polímero cristalizável processo para preparar e fabricar a composição para fabricar uma estrutura de polímero e para remover de uma fase fluida um composto de solubilidade limitada em água mas difundível na mesma artigo conformado e uso da composição |
| GB9223332D0 (en) * | 1992-11-06 | 1992-12-23 | Ici Plc | Production of polyhydroxyalkanoate in plants |
| WO1994012014A1 (fr) * | 1992-11-20 | 1994-06-09 | Agracetus, Inc. | Pieds de coton transgeniques produisant des bioplastiques heterologues |
| GB9306490D0 (en) * | 1993-03-29 | 1993-05-19 | Zeneca Ltd | Plant gene specifying acetyl,coenzyme a carboxylase and transformed plants containing same |
| GB9309453D0 (en) * | 1993-05-07 | 1993-06-23 | Zeneca Ltd | Polyester purification |
| GB2291648B (en) * | 1994-07-25 | 1998-11-25 | Ici Plc | Aqueous coating composition giving coatings having improved early hardness and tack-resistance |
| GB9416690D0 (en) * | 1994-08-18 | 1994-10-12 | Zeneca Ltd | Process for the recovery of polyhydroxyalkanoic acid |
| US5942597A (en) * | 1995-08-21 | 1999-08-24 | The Procter & Gamble Company | Solvent extraction of polyhydroxyalkanoates from biomass |
| US6083729A (en) * | 1995-10-26 | 2000-07-04 | Metabolix, Inc. | Methods for isolating polyhydroxyalkanoates from plants |
| US5821299A (en) * | 1996-02-16 | 1998-10-13 | The Proctor & Gamble Company | Solvent extraction of polyhydroxy-alkanoates from biomass facilitated by the use of marginal nonsolvent |
-
1995
- 1995-10-26 US US08/548,840 patent/US6083729A/en not_active Expired - Lifetime
-
1996
- 1996-10-23 DE DE69637253T patent/DE69637253T2/de not_active Expired - Lifetime
- 1996-10-23 JP JP51672197A patent/JP2001517070A/ja not_active Withdrawn
- 1996-10-23 EP EP96936839A patent/EP0859858B1/fr not_active Expired - Lifetime
- 1996-10-23 WO PCT/US1996/016921 patent/WO1997015681A1/fr not_active Ceased
- 1996-10-23 AU AU74663/96A patent/AU722033B2/en not_active Expired
- 1996-10-23 AT AT96936839T patent/ATE373722T1/de not_active IP Right Cessation
-
2000
- 2000-06-12 US US09/591,739 patent/US6709848B1/en not_active Expired - Lifetime
-
2007
- 2007-06-06 JP JP2007151037A patent/JP2007277574A/ja not_active Withdrawn
-
2008
- 2008-07-10 JP JP2008180815A patent/JP4422776B2/ja not_active Expired - Fee Related
-
2009
- 2009-02-27 JP JP2009045960A patent/JP2009112315A/ja not_active Ceased
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