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WO1995001929A1 - A method of producing a coreless roll of fibre-based, web-like material - Google Patents

A method of producing a coreless roll of fibre-based, web-like material Download PDF

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Publication number
WO1995001929A1
WO1995001929A1 PCT/SE1994/000666 SE9400666W WO9501929A1 WO 1995001929 A1 WO1995001929 A1 WO 1995001929A1 SE 9400666 W SE9400666 W SE 9400666W WO 9501929 A1 WO9501929 A1 WO 9501929A1
Authority
WO
WIPO (PCT)
Prior art keywords
axle
web
friction
paper
reducing agent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/SE1994/000666
Other languages
French (fr)
Inventor
Anders Andersson
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Essity Hygiene and Health AB
Original Assignee
Molnlycke Vafveri AB
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from SE9302313A external-priority patent/SE9302313D0/en
Application filed by Molnlycke Vafveri AB filed Critical Molnlycke Vafveri AB
Priority to DK94920636T priority Critical patent/DK0710212T3/en
Priority to DE69409527T priority patent/DE69409527T2/en
Priority to AU71353/94A priority patent/AU685474B2/en
Priority to JP7504001A priority patent/JPH08512275A/en
Priority to EP94920636A priority patent/EP0710212B1/en
Priority to FI956292A priority patent/FI956292L/en
Publication of WO1995001929A1 publication Critical patent/WO1995001929A1/en
Priority to NO960026A priority patent/NO302811B1/en
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65HHANDLING THIN OR FILAMENTARY MATERIAL, e.g. SHEETS, WEBS, CABLES
    • B65H19/00Changing the web roll
    • B65H19/22Changing the web roll in winding mechanisms or in connection with winding operations
    • B65H19/2292Removing cores or mandrels from web roll after winding
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B65CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
    • B65HHANDLING THIN OR FILAMENTARY MATERIAL, e.g. SHEETS, WEBS, CABLES
    • B65H2701/00Handled material; Storage means
    • B65H2701/10Handled articles or webs
    • B65H2701/18Form of handled article or web
    • B65H2701/184Wound packages
    • B65H2701/1846Parts concerned

Definitions

  • the present invention relates to a method of producing a coreless roll of fibre-based, web-like material, in particular soft crepe paper or some other nonwoven material, for instance cleaning paper, kitchen paper, or toilet paper.
  • toilet paper rolls, kitchen paper rolls and cleaning paper rolls intended for large consumers are produced by winding a paper web onto a thin tubular core, normally a paperboard cylinder.
  • This paperboard cylinder or core naturally incurs an additional cost in the manufacture of the paper roll, and since it remains when all the paper has been used it must be thrown away.
  • Coreless paper rolls where the paper is taken from the centre of the rolls are known from SE-B-399,694, for instance.
  • the inner ⁇ most paper turns are secured to one another by means of water, optionally with a binder additive. This results in a stiffening core, formed by the innermost turns although these turns are not glued together directly, but can be unrolled with the remainder of the paper web and used in the same manner as the remainder of the paper.
  • the paper web is rolled onto an expandable wind- ing-on axle which is contracted so as to enable it to be removed easily from the paper roll carried by the axle at the end of a winding-on process.
  • SE-B-455,367 teaches a coreless toilet paper roll with which the paper can be taken from the periphery of the roll.
  • the winding-on axle used to produce the roll has a relatively small diameter, approximately 10-15 mm, and is of polygonal cross-sectional shape.
  • the centre hole that is formed when the paper web is rolled onto the axle and the axle removed, will present alternating, radially outwardly extending compressions and inwardly arched parts.
  • the winding-on axle is rigid, i.e. not expandable, although it can be removed easily from the paper roll, because of the small axle diameter.
  • the object of the present invention is to provide a simplified method for the manufacture of a coreless roll of material, for instance a paper roll, provided with a relatively large centre hole, and consequently the winding-on axle used must have a correspondingly large diameter. This accentuates the problem of removing the winding-on axle from the paper roll. This problem has been solved by means of the present invention.
  • the in-, ventive method is characterized by placing the leading end of the web around a non-expandable winding-on axle which has a fixed diameter of at least 35 mm and which is caused to rotate so as to wind the web onto the axle; applying a friction-reducing agent to the axle or to the first turn or turns of the web, with the intention of reducing friction between the web and the axle; and withdrawing the axle from the resultant roll, subsequent to termination of the web winding-on process.
  • Figure 1 is an end view of a centre-feed paper roll
  • Figures 2 and 3 illustrate schematically the initial stage of winding-on a paper web in accordance with two different methods
  • Figure 4 illustrates an alternative embodiment of a winding-on axle.
  • the paper roll 1 is produced by moving the free end 2a of a paper web 2 into engagement with a winding-on axle 3 in a winding-on machine.
  • the web is rolled up on a so- called carrying roller machine in which the winding-on axle 3 is mounted between a pair of rotatable carrying rollers 4.
  • Figure 3 illustrates a so-called centre drive system in which the actual winding-on axle is rotated. In both systems, as the axle 3 rotates paper is wound onto the axle and the axle is removed from the resultant paper roll upon completion of the winding-on process.
  • Paper rolls with which paper is taken from the centre of the roll require a relatively large centre opening, about 35-100 mm, which is governed by the other dimensions of the roll. Moreover, most paper rolls in- tended for taking the paper from the periphery of the roll are provided with centre holes with a diameter larger than 35 mm. Winding-on axles of corresponding dimensions are difficult to withdraw from the paper roll wound onto the axle. The friction between roll and axle is particularly great in the case of a fully cylindrical axle, since the abutment surface between paper and axle is then large. Slightly less friction is obtained with axles of a non-circular cross-section.
  • a fric- tion-reducing agent is applied to the axle immediately before or in conjunction with initiation of the winding- on process, with the intention of reducing the friction between the paper web and the axle.
  • This agent may consist of water, optionally with an addition of a softener, for instance quaternary amine, or other lubricant, such as silicone or the like.
  • the friction- reducing agent may alternatively consist of an oil, oil emulsion, triglyceride, teflon or the like.
  • the friction-reducing agent is applied to the axle 3 with the aid of a spray nozzle 4. It will be understood, however, that the agent can be applied in some other way, for instance it can be brushed onto the axle. Alternatively, the friction- reducing agent can be applied to the innermost turn or turns of the paper web 2 instead of to the axle 3, as illustrated in Figure 2.
  • Friction is reduced still further when the axle 3 is heated in conjunction with applying the friction-reduc ⁇ ing agent.
  • the axle can be heated either electrically or with the aid of steam or some other heating medium, for instance oil.
  • the axle 3 used will preferably be of the kind illustrated in Figure 4, i.e. a hollow axle or spindle provided with a plurality of radial holes 5. Steam, or water that has been heated electrically within the axle, is applied to the interior of the axle through a pipe 6 and then allowed to flow out through the holes 5. Water applied to the paper in vapour form in this way penetrates the paper web more effectively than water in liquid form.
  • Heating of the axle results in an ironing effect, i.e. the fibres in the innermost turn or turns of the paper web are compacted and the paper surface abutting the spindle will be smoother, thereby reducing the friction between axle and paper surface. Heating of the axle also accelerates the drying process.
  • the axle 3 may either be cylindrical, as illustrated in the drawing, or may have some other form which includes teeth, splines or the like, which may optionally be given a helical shape.
  • the axle may also have a slightly conical shape, to facilitate its withdrawal from the paper roll.
  • the axle may consist of a low friction material or may be coated with such a material.” Examples of suitable materials are nylon, acetal, teflon or low- friction treated metal alloys.

Landscapes

  • Sanitary Thin Papers (AREA)
  • Paper (AREA)
  • Preliminary Treatment Of Fibers (AREA)
  • Yarns And Mechanical Finishing Of Yarns Or Ropes (AREA)
  • Rolls And Other Rotary Bodies (AREA)
  • Winding Of Webs (AREA)
  • Treatment Of Fiber Materials (AREA)

Abstract

A method of producing a coreless roll from a web of fibre-based material, particularly soft crêpe paper or some other nonwoven material, for instance cleaning paper, kitchen paper or toilet paper. The web (2) is wound onto a non-expandable winding-on axle (3) having a diameter of between 35-100mm. In order to facilitate withdrawal of the axle from the roll after winding the web onto the roll, a friction-reducing agent (4) is applied to the axle or to the first turn or turns of the web. This agent may be water, to which a surfactant or some other lubricant is optionally added, or oil, triglyceride, silicone, Teflon<TM> or the like. The axle (2) may be heated, either electrically or with the aid of steam, in conjunction with applying the agent, therewith further reducing the friction between web and axle.

Description

A METHOD OF PRODUCING A CORELESS ROLL OF FIBRE-BASED. WEB-LIKE MATERIAL
Technical Field
The present invention relates to a method of producing a coreless roll of fibre-based, web-like material, in particular soft crepe paper or some other nonwoven material, for instance cleaning paper, kitchen paper, or toilet paper.
Background of the Invention
Normally, toilet paper rolls, kitchen paper rolls and cleaning paper rolls intended for large consumers are produced by winding a paper web onto a thin tubular core, normally a paperboard cylinder. This paperboard cylinder or core naturally incurs an additional cost in the manufacture of the paper roll, and since it remains when all the paper has been used it must be thrown away.
Coreless paper rolls where the paper is taken from the centre of the rolls are known from SE-B-399,694, for instance. In order to avoid collapsing of the centre hole, it is proposed in this publication that the inner¬ most paper turns are secured to one another by means of water, optionally with a binder additive. This results in a stiffening core, formed by the innermost turns although these turns are not glued together directly, but can be unrolled with the remainder of the paper web and used in the same manner as the remainder of the paper. The paper web is rolled onto an expandable wind- ing-on axle which is contracted so as to enable it to be removed easily from the paper roll carried by the axle at the end of a winding-on process. Such an expandable axle, however, requires maintenance and can cause dis- turbances in operation. SE-B-455,367 teaches a coreless toilet paper roll with which the paper can be taken from the periphery of the roll. The winding-on axle used to produce the roll has a relatively small diameter, approximately 10-15 mm, and is of polygonal cross-sectional shape. The centre hole that is formed when the paper web is rolled onto the axle and the axle removed, will present alternating, radially outwardly extending compressions and inwardly arched parts. The winding-on axle is rigid, i.e. not expandable, although it can be removed easily from the paper roll, because of the small axle diameter.
The Objects and Most Important Characteristic Features of the Invention The object of the present invention is to provide a simplified method for the manufacture of a coreless roll of material, for instance a paper roll, provided with a relatively large centre hole, and consequently the winding-on axle used must have a correspondingly large diameter. This accentuates the problem of removing the winding-on axle from the paper roll. This problem has been solved by means of the present invention. The in-, ventive method is characterized by placing the leading end of the web around a non-expandable winding-on axle which has a fixed diameter of at least 35 mm and which is caused to rotate so as to wind the web onto the axle; applying a friction-reducing agent to the axle or to the first turn or turns of the web, with the intention of reducing friction between the web and the axle; and withdrawing the axle from the resultant roll, subsequent to termination of the web winding-on process.
Brief Description of the Drawings
The present invention will now be described in more detail with reference to exemplifying embodiments there¬ of and also with reference to the accompanying drawings, in which Figure 1 is an end view of a centre-feed paper roll; Figures 2 and 3 illustrate schematically the initial stage of winding-on a paper web in accordance with two different methods; and Figure 4 illustrates an alternative embodiment of a winding-on axle.
Description of Exemplifying Embodiments
The paper roll 1 is produced by moving the free end 2a of a paper web 2 into engagement with a winding-on axle 3 in a winding-on machine. In the case of the embodiment illustrated in Figure 2, the web is rolled up on a so- called carrying roller machine in which the winding-on axle 3 is mounted between a pair of rotatable carrying rollers 4. Figure 3 illustrates a so-called centre drive system in which the actual winding-on axle is rotated. In both systems, as the axle 3 rotates paper is wound onto the axle and the axle is removed from the resultant paper roll upon completion of the winding-on process.
Paper rolls with which paper is taken from the centre of the roll require a relatively large centre opening, about 35-100 mm, which is governed by the other dimensions of the roll. Moreover, most paper rolls in- tended for taking the paper from the periphery of the roll are provided with centre holes with a diameter larger than 35 mm. Winding-on axles of corresponding dimensions are difficult to withdraw from the paper roll wound onto the axle. The friction between roll and axle is particularly great in the case of a fully cylindrical axle, since the abutment surface between paper and axle is then large. Slightly less friction is obtained with axles of a non-circular cross-section. It is therefore proposed in accordance with the invention that a fric- tion-reducing agent is applied to the axle immediately before or in conjunction with initiation of the winding- on process, with the intention of reducing the friction between the paper web and the axle. This agent may consist of water, optionally with an addition of a softener, for instance quaternary amine, or other lubricant, such as silicone or the like. The friction- reducing agent may alternatively consist of an oil, oil emulsion, triglyceride, teflon or the like.
In the Figure 1 illustration, the friction-reducing agent is applied to the axle 3 with the aid of a spray nozzle 4. It will be understood, however, that the agent can be applied in some other way, for instance it can be brushed onto the axle. Alternatively, the friction- reducing agent can be applied to the innermost turn or turns of the paper web 2 instead of to the axle 3, as illustrated in Figure 2.
It has been surprisingly found that friction can be reduced substantially with water on its own. This can be explained by the fact that when creped paper is moist- ened with water, the paper stretches and remains in a stretched state after having dried. This stretching of the paper reduces the friction between paper and axle. Friction is reduced still further when a softener or some other lubricant is added to the water, as before mentioned. A corresponding reduction in friction is obtained when oil, triglyceride or the like is applied either to the axle or to the innermost turn or turns of the paper web.
Friction is reduced still further when the axle 3 is heated in conjunction with applying the friction-reduc¬ ing agent. The axle can be heated either electrically or with the aid of steam or some other heating medium, for instance oil. In this latter case, the axle 3 used will preferably be of the kind illustrated in Figure 4, i.e. a hollow axle or spindle provided with a plurality of radial holes 5. Steam, or water that has been heated electrically within the axle, is applied to the interior of the axle through a pipe 6 and then allowed to flow out through the holes 5. Water applied to the paper in vapour form in this way penetrates the paper web more effectively than water in liquid form.
Heating of the axle, either electrically or with the aid of steam, in combination with moisture supply, results in an ironing effect, i.e. the fibres in the innermost turn or turns of the paper web are compacted and the paper surface abutting the spindle will be smoother, thereby reducing the friction between axle and paper surface. Heating of the axle also accelerates the drying process.
The axle 3 may either be cylindrical, as illustrated in the drawing, or may have some other form which includes teeth, splines or the like, which may optionally be given a helical shape. The axle may also have a slightly conical shape, to facilitate its withdrawal from the paper roll. The axle may consist of a low friction material or may be coated with such a material." Examples of suitable materials are nylon, acetal, teflon or low- friction treated metal alloys.
It will be understood that the invention is not re¬ stricted to the described and illustrated exemplifying embodiments thereof and that modifications and changes are conceivable within the scope of the following Claims.

Claims

Claims
1. A method of producing a coreless roll from a web of fibre-based material, in particular soft crepe paper or other nonwoven material, for instance cleaning paper, kitchen paper or toilet paper, c h a r a c t e r ¬ i z e d by laying the leading end (2a) of the material web around a non-expandable winding-on axle (3) having a fixed diameter of between 35-100 mm and rotating the axle so as to wind the web (2) onto said axle; applying (4) a friction-reducing agent to the axle or to the first turn or turns of the material web, with the intention of reducing the friction between the web and the axle; and withdrawing the axle from the resultant roll after completion of the web winding-on process.
2. A method according to Claim 1, c h a r a c t ¬ e r i z e d in that the friction-reducing agent is water, optionally with an additive of surfactant or some other lubricant.
3. A method according to Claim 2, c h a r a c t ¬ e r i z e d in that the surfactant is a softener, for instance a quaternary amine.
4. A method according to Claim 1, c h a r a c t ¬ e r i z e d in that the friction-reducing agent is an oil, oil emulsion, triglyceride, silicone, teflon or the like.
5. A method according to one or more of the preceding Claims, c h a r a c t e r i z e d by heating the axle (3) in conjunction with applying the friction-reducing agent to the axle or to the material web.
6. A method according to Claim 5, c h a r a c t ¬ e r i z e d by heating the axle (3) electrically.
7. A method according to Claim 5, c h a r a c t ¬ e r i z e d by heating the axle (3) with the aid of a heating medium, e.g. steam or oil, applied (6) to the centre of the axle.
8. A method according to Claim 7, c h a r a c t ¬ e r i z e d in that the axle (3) is hollow and includes a plurality of radial holes (5) ; and in that the applied steam is permitted to flow out through said holes while moistening and heating the web (2) , wherein the moisture thus applied constitutes the friction-reducing agent.
9. A method according to one or more of the preceding Claims, c h a r a c t e r i z e d in that the axle (3) is comprised of a low friction material or is at least surface-coated with a low friction material, for in¬ stance nylon, acetal, teflon or low-friction treated metal alloys.
10. A method according to one or more of the preceding Claims, c h a r a c t e r i z e d in that the axle (3) has a slightly conical configuration.
PCT/SE1994/000666 1993-07-05 1994-07-05 A method of producing a coreless roll of fibre-based, web-like material Ceased WO1995001929A1 (en)

Priority Applications (7)

Application Number Priority Date Filing Date Title
DK94920636T DK0710212T3 (en) 1993-07-05 1994-07-05 Process for producing a coreless roll of a fiber-based web-like material
DE69409527T DE69409527T2 (en) 1993-07-05 1994-07-05 METHOD FOR PRODUCING A CORELESS ROLL MADE OF FIBROUS, RAIL-LIKE MATERIAL
AU71353/94A AU685474B2 (en) 1993-07-05 1994-07-05 A method of producing a coreless roll of fibre-based, web-like material
JP7504001A JPH08512275A (en) 1993-07-05 1994-07-05 Method for manufacturing coreless roll of fiber-based web-like material
EP94920636A EP0710212B1 (en) 1993-07-05 1994-07-05 A method of producing a coreless roll of fibre-based, web-like material
FI956292A FI956292L (en) 1993-07-05 1994-07-05 Method for producing a coreless roll from a fiber-based web-like material
NO960026A NO302811B1 (en) 1993-07-05 1996-01-04 Process for producing a coreless roll of fiber-based, web-like material

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
SE9302313A SE9302313D0 (en) 1993-07-05 1993-07-05 MADE TO MAKE A SHELF ROLL OF FIBER BASED MATERIAL
SE9302313-3 1993-07-05
SE9303175A SE502630C2 (en) 1993-07-05 1993-09-29 Ways to make a coreless roll of fiber-based web-shaped material
SE9303175-5 1993-09-29

Publications (1)

Publication Number Publication Date
WO1995001929A1 true WO1995001929A1 (en) 1995-01-19

Family

ID=26661792

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/SE1994/000666 Ceased WO1995001929A1 (en) 1993-07-05 1994-07-05 A method of producing a coreless roll of fibre-based, web-like material

Country Status (12)

Country Link
EP (1) EP0710212B1 (en)
JP (1) JPH08512275A (en)
AT (1) ATE164815T1 (en)
AU (1) AU685474B2 (en)
CA (1) CA2165445A1 (en)
DE (1) DE69409527T2 (en)
DK (1) DK0710212T3 (en)
ES (1) ES2117793T3 (en)
FI (1) FI956292L (en)
NO (1) NO302811B1 (en)
SE (1) SE502630C2 (en)
WO (1) WO1995001929A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1999012461A1 (en) * 1997-09-08 1999-03-18 Kimberly-Clark Worldwide, Inc. A system for dispensing coreless rolls of product

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103708260B (en) * 2013-12-31 2016-02-10 黄聪伟 A method for automatically wrapping a raw material tape on a tape head
EA032995B1 (en) * 2017-08-28 2019-08-30 Александр Сергеевич ИВАНОВ Method for removal of a polymer film roll wound without a core from a mandrel

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE817192C (en) * 1950-05-23 1951-10-15 Hakle Papierwerke Method for producing the shell-like opening on toilet paper rolls
SE399694B (en) * 1976-05-19 1978-02-27 Moelnlycke Ab ROLL OF RAILWAY MATERIAL
SE419742B (en) * 1978-09-21 1981-08-24 Fiskeby Ab Cylinder core for web-shaped material and method for manufacturing the same
SE452974B (en) * 1981-06-18 1988-01-04 Jouko Juhani Salmela SET UP TO ROLL UP A MATERIAL COURSE ON A CORE COVER
SE455367B (en) * 1982-05-19 1988-07-11 Masashi Kobayashi NUCLEAR PILOT TOILET PAPER ROLL AND PROCEDURE FOR ITS MANUFACTURING
US4763785A (en) * 1987-10-09 1988-08-16 Basf Aktiengesellschaft Center-pull fiber package and method for producing the package
EP0553493A1 (en) * 1992-01-10 1993-08-04 Bayer Ag Coated bobbins, process for their fabrication and their use in the treatment of glass fibers

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE817192C (en) * 1950-05-23 1951-10-15 Hakle Papierwerke Method for producing the shell-like opening on toilet paper rolls
SE399694B (en) * 1976-05-19 1978-02-27 Moelnlycke Ab ROLL OF RAILWAY MATERIAL
SE419742B (en) * 1978-09-21 1981-08-24 Fiskeby Ab Cylinder core for web-shaped material and method for manufacturing the same
SE452974B (en) * 1981-06-18 1988-01-04 Jouko Juhani Salmela SET UP TO ROLL UP A MATERIAL COURSE ON A CORE COVER
SE455367B (en) * 1982-05-19 1988-07-11 Masashi Kobayashi NUCLEAR PILOT TOILET PAPER ROLL AND PROCEDURE FOR ITS MANUFACTURING
US4763785A (en) * 1987-10-09 1988-08-16 Basf Aktiengesellschaft Center-pull fiber package and method for producing the package
EP0553493A1 (en) * 1992-01-10 1993-08-04 Bayer Ag Coated bobbins, process for their fabrication and their use in the treatment of glass fibers

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
PATENT ABSTRACTS OF JAPAN, Vol. 10, No. 181, M-492; & JP,A,61 027 857 (MITSUI TOATSU CHEM INC), 7 February 1986. *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1999012461A1 (en) * 1997-09-08 1999-03-18 Kimberly-Clark Worldwide, Inc. A system for dispensing coreless rolls of product

Also Published As

Publication number Publication date
NO960026D0 (en) 1996-01-04
EP0710212B1 (en) 1998-04-08
SE9303175D0 (en) 1993-09-29
EP0710212A1 (en) 1996-05-08
FI956292A7 (en) 1995-12-28
JPH08512275A (en) 1996-12-24
FI956292A0 (en) 1995-12-28
AU7135394A (en) 1995-02-06
SE9303175L (en) 1995-01-06
FI956292L (en) 1995-12-28
DK0710212T3 (en) 1998-12-07
ES2117793T3 (en) 1998-08-16
DE69409527D1 (en) 1998-05-14
ATE164815T1 (en) 1998-04-15
NO960026L (en) 1996-01-04
CA2165445A1 (en) 1995-01-19
SE502630C2 (en) 1995-11-27
AU685474B2 (en) 1998-01-22
DE69409527T2 (en) 1998-10-15
NO302811B1 (en) 1998-04-27

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