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WO1992017417A1 - Regulation d'un ecoulement gazeux a travers une colonne de ciment - Google Patents

Regulation d'un ecoulement gazeux a travers une colonne de ciment Download PDF

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Publication number
WO1992017417A1
WO1992017417A1 PCT/US1992/000698 US9200698W WO9217417A1 WO 1992017417 A1 WO1992017417 A1 WO 1992017417A1 US 9200698 W US9200698 W US 9200698W WO 9217417 A1 WO9217417 A1 WO 9217417A1
Authority
WO
WIPO (PCT)
Prior art keywords
weight
cement
copolymer
styrene
amount
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/US1992/000698
Other languages
English (en)
Inventor
Kalyan K. Ganguli
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Western Company of North America
Original Assignee
Western Company of North America
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Western Company of North America filed Critical Western Company of North America
Publication of WO1992017417A1 publication Critical patent/WO1992017417A1/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
    • C04B24/16—Sulfur-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
    • C04B24/24—Macromolecular compounds
    • C04B24/26—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C04B24/2641—Polyacrylates; Polymethacrylates
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B24/00—Use of organic materials as active ingredients for mortars, concrete or artificial stone, e.g. plasticisers
    • C04B24/24—Macromolecular compounds
    • C04B24/26—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C04B24/2676—Polystyrenes
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
    • C04B28/02—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing hydraulic cements other than calcium sulfates
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C09K8/46—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing inorganic binders, e.g. Portland cement
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K8/00—Compositions for drilling of boreholes or wells; Compositions for treating boreholes or wells, e.g. for completion or for remedial operations
    • C09K8/42—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells
    • C09K8/46—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing inorganic binders, e.g. Portland cement
    • C09K8/467—Compositions for cementing, e.g. for cementing casings into boreholes; Compositions for plugging, e.g. for killing wells containing inorganic binders, e.g. Portland cement containing additives for specific purposes
    • C09K8/487—Fluid loss control additives; Additives for reducing or preventing circulation loss
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2103/00—Function or property of ingredients for mortars, concrete or artificial stone
    • C04B2103/46—Water-loss or fluid-loss reducers, hygroscopic or hydrophilic agents, water retention agents

Definitions

  • This invention relates to cement compositions for the oil industry and a method for their use in cementing wells. In another aspect, this invention relates to the control of the gas migration or gas channeling phenomenon that occurs during the setting of a cement slurry.
  • Gas channeling is a phenomenon that occurs during the setting of a cement slurry. Once the cement slurry begins to set, the hydrostatic pressure in the cement column begins to decrease. This reduction in hydrostatic pressure allows the channeling of gas through the partially set slurry. This gas, which is under pressure from the formation, flows through the partially set cement slurry creating microchannels. These microchannels can lead to safety problems when they extend to the surface.
  • This invention provides cement slurry compositions capable of controlling the migration or channeling of gas that occurs during the setting of a cement slurry.
  • a cementing composition is provided that is capable of inhibiting pressure gas channeling.
  • This composition comprises aqueous fluid, hydraulic cement, and a gas channeling inhibiting additive comprised of the copolymer 2-acrylamido- 2-methylpropane-3-sulphonic acid, vinylacylamide, in the presence or absence of acr lamide.
  • gas channeling inhibiting polymers of the present invention comprised of the copolymer product of 2- acrylamido-2-methyl propane-3-sulphonic acid in an amount of from 5 to 95 percent by total weight of copolymer, vinylacylamide in an amount of from 5 to 95 percent by total weight of copolymer, and acrylamide in an amount of from 0 to 80 percent by total weight of copolymer.
  • This copolymer is effective at well bottom hole temperatures ranging from 100 to 500°F, and is not adversely affected by brine.
  • a method of inhibiting gas channeling that occurs during the cementing of a casing in a borehole penetrating a high temperature subterranean formation comprising: introducing a cementing composition into the annulus between said conduit and said formation, said cementing composition containing a gas channeling inhibiting additive comprised of
  • SUBSTITUTESHEET a copolymer of (1) 5 to 95 weight percent of 2- acrylamido-2-methylpropane-3-sulphonic acid; (2) 5 to 95 weight percent of a vinylacylamide; and (3) 0 to 80 weight percent of acrylamide; and allowing said cementing composition to set within said space.
  • a cement slurry composition that contains, in addition to the 2-acrylamido-2-methylpropane-3-sulphonic acid/vinylacylamide/acrylamide additive, a gas channeling inhibiting amount of a styrene/butadiene latex copolymer.
  • the styrene/butadiene latex copolymer is substituted with at least one selected from the group consisting of carboxyl
  • composition of the gas channeling inhibitor of the present invention is comprised of an aqueous fluid, hydraulic cement and a polymer comprising the reaction product of the polymerization of 2-acrylamido-2-methyl propane-3- sulphonic acid (AMPS) , vinylacylamide, and if appropriate, acrylamide.
  • AMPS 2-acrylamido-2-methyl propane-3- sulphonic acid
  • AMPS is present in the polymerization reaction product in acid or salt form in an amount of from about 5 to about 95 percent by total weight of copolymer. More preferably, AMPS is present in an amount from about 10 to about 90 percent by total weight of copolymer. Most preferably, AMPS is present in an amount of from about 60 to about 70 percent by total weight of copolymer.
  • Vinylacylamide is present in an amount of from about 5 to 95 percent by total weight of copolymer. More preferably, vinylacylamide is present in an amount of from about 7 to 80 percent by total weight of copolymer. Most preferably, vinylacylamide is present in an amount of from about 10 to 30 percent by weight.
  • Acrylamide is present in an amount of from about 0 to 80 percent by total weight of copolymer; more preferably, in an amount of from about 5 to 60 percent by total weight of copolymer. Most preferably, acrylamide is present in an amount of from about 10 to 30 percent by total weight of copolymer.
  • Illustrative of the acrylamides useful in the present invention is a terpolymer product available commercially from Hoechst Celanese under the trade name Hostamer® V2825.
  • the polymers generally are admixed with the cementing composition in an amount of from about 0.1 to about 5.0 percent by weight of the dry "
  • the gas channeling inhibitor is admixed with the cement in an amount of from about 0.5 to about 2.0 percent, and most preferably, from about 1.0 to about 1.5 percent weight of dry cement.
  • the gas channeling inhibitor of this invention is effective in high temperature wells.
  • This additive is well suited for use in wells having a bottom hole temperature of from about 100°F to about 500°F.
  • the gas channeling inhibitor of this invention is effective even in the presence of salt water.
  • Gas channeling inhibiting characteristics may be maintained in salt cement compositions, such as saturated NaCl and seawater, without changing the rheological properties of the cement. Indeed, these characteristics may be maintained at a cement salt concentration of up to approximately 38 percent or in seawater.
  • Cement compositions containing such fluid loss additives display improved pumpability. This feature, in turn, enhances drilling fluid removal and decreases lost circulation when cementing a conduit.
  • the cement portion of the composition of this invention may be any of the API classes of cement as defined in the American Petroleum Institute Bulletin entitled “API Specification for Material & Testing for Well Cements” dated January 1982 ("API Spec. 10"), and incorporated herein by reference. These include cements defined as classes “G” and “H” in API Spec. 10.
  • SUBSTITUTESHEET viscosifiers may include, for example, (1) heavy weight additives, such as hematite, illmenite, silica flour and sand; (2) cement retarders such as lignins and lignosulfonates; and (3) additives for controlling lost circulation such as walnut hulls and cellophane flakes.
  • Styrene/butadiene latex copoly ers may be added to the cement slurry composition.
  • any styrene/butadiene latex copolymer effective in inhibiting gas channeling may be added to the composition.
  • the styrene/butadiene latex copolymer is substituted with at least one selected from the group consisting of carboxyl
  • sulfonic (-C00R) , sulfonic (-S0 3 R) and hydroxyl, wherein R is H or a C j - ⁇ alkyl group.
  • R is H or a C j - ⁇ alkyl group.
  • a carboxylated styrene/butadiene latex copolymer comprising approximate equal amounts by weight of carboxylated styrene and butadiene is added in an amount up to about 20% by weight of cement.
  • the preferred carboxyl is -COOH
  • the preferred sulfonic is -S0 3 H.
  • the styrene/butadiene latex copolymer When the styrene/butadiene latex copolymer is added to the composition, concomitant use of an anionic high temperature dispersant with or without a latex stabilizer is required.
  • the dispersant may be useful in dispersing the cement system.
  • the preferred dispersant in this invention is a sulfonated styrene/maleic anhydride copolymer.
  • the latex stabilizer-anionic surfactant used may be any that generally prevents the coagulation
  • the latex stabilizer used is Carbapon®, a product available commercially from Hoechst Celanese consisting of organophosphonate and acrylate.
  • Other potential latex stabilizers include (1) linear alkylbenzene sulfonate, (2) COCO fatty betaine, (3) polycarboxylic acid, (4) sodium dodecylbenzene sulfonate, and (5) ether- carboxylate.
  • gas channeling inhibitor As a gas channeling inhibitor will result in significant reductions in gas migration or gas channeling rate.
  • excellent gas channeling control (30-40 cc gas flow/ in.) may be achieved by the addition of about 0.1 to about 1.7 percent by weight of the cement, of such gas channeling inhibitor to a normal dense cement.
  • Table 1 depicts the gas channeling inhibition produced by the polymers of the present invention.
  • the copolymer consisting of AMPS, vinylacylamide, and acrylamide reduced gas flow to negligible levels.
  • the gas migration control capabilities of the designed slurry was tested in a gas flow simulator.
  • the gas flow simulator is a high temperature high pressure apparatus which monitors and records gas flow

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Structural Engineering (AREA)
  • Inorganic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Abstract

Cette invention se rapporte à des compositions de cimentation utilisées dans l'industrie pétrolière pour cimenter des trous de forage. Plus particulièrement, cette invention se rapporte à la régulation du phénomène de migration des gaz ou de renardage par les gaz qui a lieu au cours du durcissement d'un coulis de ciment. On décrit une composition de cimentation susceptible d'inhiber le renardage par les gaz, laquelle composition se compose d'un fluide gazeux, de ciment hydraulique et d'un additif inhibant le renardage et comprenant un copolymère d'acide 2-acrylamido-2-méthylpropane-3-sulfonique, de N-vinylacylamide et d'acrylamide.
PCT/US1992/000698 1991-03-26 1992-02-05 Regulation d'un ecoulement gazeux a travers une colonne de ciment Ceased WO1992017417A1 (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US07/675,309 US5099922A (en) 1991-03-26 1991-03-26 Control of gas flow through cement column
US675,309 1991-03-26

Publications (1)

Publication Number Publication Date
WO1992017417A1 true WO1992017417A1 (fr) 1992-10-15

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Application Number Title Priority Date Filing Date
PCT/US1992/000698 Ceased WO1992017417A1 (fr) 1991-03-26 1992-02-05 Regulation d'un ecoulement gazeux a travers une colonne de ciment

Country Status (2)

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US (1) US5099922A (fr)
WO (1) WO1992017417A1 (fr)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1994027025A1 (fr) * 1993-05-06 1994-11-24 Bj Services Company Composition de cimentation et procede d'utilisation de polymeres phosphones afin d'ameliorer les proprietes de coulis de ciment
EP0653547A1 (fr) * 1993-11-12 1995-05-17 Halliburton Company Additif pour laitiers de cément petroliers
DE19806482A1 (de) * 1998-02-17 1999-08-19 Sueddeutsche Kalkstickstoff Wasserlösliche oder wasserquellbare sulfogruppenhaltige Copolymere, Verfahren zu deren Herstellung und ihre Verwendung
EP1024154A3 (fr) * 1999-01-26 2003-01-02 Omnova Solutions Inc. Latex de polymères stables aux ions multivalents, leur préparation et leur utilisation
FR2850647A1 (fr) * 2003-01-30 2004-08-06 Rhodia Chimie Sa Composition comprenant un liant hydraulique et un latex possedant un groupement foncitonnel sulfonate, sulfonique ou sulfobetaine

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US5679731A (en) * 1994-08-31 1997-10-21 Intevep, S.A. Cement slurry
US5588488A (en) * 1995-08-22 1996-12-31 Halliburton Company Cementing multi-lateral wells
US5679150A (en) * 1996-08-16 1997-10-21 Kerkar; Awdhoot Vasant Drying shrinkage cement admixture
US6302955B1 (en) 1998-11-04 2001-10-16 W. R. Grace & Co.-Conn. Composition for improving freeze/thaw durability of masonry containing fatty acid-based efflorescence control agents
US6258161B1 (en) 1998-11-04 2001-07-10 W. R. Grace & Co.-Conn. Masonry blocks and masonry concrete admixture for improved freeze-thaw durability
US6525116B2 (en) 1999-01-26 2003-02-25 National Gypsum Properties Llc Gypsum composition with ionic styrene butadiene latex additive
US6875729B2 (en) * 2002-06-04 2005-04-05 Halliburton Energy Services, Inc. Sealing composition
EP1674434A1 (fr) * 2004-12-21 2006-06-28 Services Petroliers Schlumberger Agents de regulation de perte de fluide et compositions de cimentation pour des puits de pétrole ou gas contenant ces agents
US7530396B1 (en) * 2008-01-24 2009-05-12 Halliburton Energy Services, Inc. Self repairing cement compositions and methods of using same
CN102212352A (zh) * 2010-04-12 2011-10-12 长江大学 一种防气窜非渗透胶乳固井水泥浆
CA2914643C (fr) * 2013-09-04 2017-10-24 Halliburton Energy Services, Inc. Melange de ciment comprenant des polymeres
US9321953B1 (en) 2013-11-22 2016-04-26 Fritz Industries, Inc. Well cementing
NO338018B1 (no) 2013-12-04 2016-07-18 Wellcem As Fremgangsmåte for tetting av hydrokarbonbrønner.
EP3115432A1 (fr) * 2015-07-07 2017-01-11 Services Pétroliers Schlumberger Compositions et procédés pour la cimentation de puits
EP3208250A1 (fr) * 2016-02-18 2017-08-23 Services Pétroliers Schlumberger Compositions et procédés pour réduire une perte de fluide dans des bouillies de cimentation de puits
US10351754B1 (en) * 2018-01-12 2019-07-16 Saudi Arabian Oil Company Cement compositions comprising aqueous latex containing dispersed solid and liquid elastomer phases

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EP0023712A1 (fr) * 1979-08-06 1981-02-11 CASSELLA Aktiengesellschaft Copolymère soluble dans l'eau, procédé pour sa production et son utilisation
EP0044508A2 (fr) * 1980-07-19 1982-01-27 CASSELLA Aktiengesellschaft Copolymères de poids moléculaire élevé solubles dans l'eau, leur préparation et leur utilisation
EP0116671A1 (fr) * 1983-01-24 1984-08-29 Hoechst Aktiengesellschaft Boues de ciment pour forage profond contenant des copolymères pour réduire la perte d'eau
EP0137872A1 (fr) * 1983-10-14 1985-04-24 Halliburton Company Composition de fluide de forage et de complétion
US4632186A (en) * 1985-12-27 1986-12-30 Hughes Tool Company Well cementing method using an AM/AMPS fluid loss additive blend
GB2247234A (en) * 1990-08-21 1992-02-26 Halliburton Co Fluid loss reduced cement compositions

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EP0116671A1 (fr) * 1983-01-24 1984-08-29 Hoechst Aktiengesellschaft Boues de ciment pour forage profond contenant des copolymères pour réduire la perte d'eau
EP0137872A1 (fr) * 1983-10-14 1985-04-24 Halliburton Company Composition de fluide de forage et de complétion
US4632186A (en) * 1985-12-27 1986-12-30 Hughes Tool Company Well cementing method using an AM/AMPS fluid loss additive blend
GB2247234A (en) * 1990-08-21 1992-02-26 Halliburton Co Fluid loss reduced cement compositions

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1994027025A1 (fr) * 1993-05-06 1994-11-24 Bj Services Company Composition de cimentation et procede d'utilisation de polymeres phosphones afin d'ameliorer les proprietes de coulis de ciment
EP0653547A1 (fr) * 1993-11-12 1995-05-17 Halliburton Company Additif pour laitiers de cément petroliers
DE19806482A1 (de) * 1998-02-17 1999-08-19 Sueddeutsche Kalkstickstoff Wasserlösliche oder wasserquellbare sulfogruppenhaltige Copolymere, Verfahren zu deren Herstellung und ihre Verwendung
US6187887B1 (en) 1998-02-17 2001-02-13 Skw Bauchemie Gmbh Water-soluble or water-swellable copolymers containing sulfonic groups and methods of preparation
EP1024154A3 (fr) * 1999-01-26 2003-01-02 Omnova Solutions Inc. Latex de polymères stables aux ions multivalents, leur préparation et leur utilisation
US6755907B1 (en) 1999-01-26 2004-06-29 Omnova Solutions Inc. Gypsum composition with styrene butadiene latex additive
FR2850647A1 (fr) * 2003-01-30 2004-08-06 Rhodia Chimie Sa Composition comprenant un liant hydraulique et un latex possedant un groupement foncitonnel sulfonate, sulfonique ou sulfobetaine
WO2004067470A1 (fr) * 2003-01-30 2004-08-12 Rhodia Chimie Composition comprenant un liant hydraulique et un latex possedant un groupement fonctionnel sulfonate, sulfonique ou sulfobetaine

Also Published As

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