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WO1992017303A1 - Procede et installation permettant d'obtenir des poudres hautement dispersives de substances non organiques - Google Patents

Procede et installation permettant d'obtenir des poudres hautement dispersives de substances non organiques Download PDF

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Publication number
WO1992017303A1
WO1992017303A1 PCT/RO1992/000064 RO9200064W WO9217303A1 WO 1992017303 A1 WO1992017303 A1 WO 1992017303A1 RO 9200064 W RO9200064 W RO 9200064W WO 9217303 A1 WO9217303 A1 WO 9217303A1
Authority
WO
WIPO (PCT)
Prior art keywords
узел
installation
nickel
energy
blank
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
Application number
PCT/RO1992/000064
Other languages
English (en)
Russian (ru)
Inventor
Nikolai Aleksandrovich Yavorovsky
Valery Ivanovich Davydovich
Boris Andreevich Bil
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
AKTSIONERNOE OBSCHESTVO SERVER
Original Assignee
AKTSIONERNOE OBSCHESTVO SERVER
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from SU4947132 external-priority patent/RU2048277C1/ru
Priority claimed from SU5004107 external-priority patent/RU2048278C1/ru
Application filed by AKTSIONERNOE OBSCHESTVO SERVER filed Critical AKTSIONERNOE OBSCHESTVO SERVER
Priority to JP50904792A priority Critical patent/JP2002517172A/ja
Publication of WO1992017303A1 publication Critical patent/WO1992017303A1/fr
Anticipated expiration legal-status Critical
Ceased legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/02—Making metallic powder or suspensions thereof using physical processes
    • B22F9/14—Making metallic powder or suspensions thereof using physical processes using electric discharge

Definitions

  • a major disadvantage of this method is the inability to receive accidents with a particle size of less than 0.2 ⁇ m, which results in a worse performance loss.
  • the main disadvantage of this device is the poorly received high quality accidents, and there is a disadvantage.
  • a fixed task is resolved by the receipt of high-quality disruptions due to the failure of metallic objects due to the failure of metallic explosions.
  • the operation is carried out by the impulse of the current and the specific energy supplied to the batch, as well as 0.9 energy. - 4 - sublimation of metal to energy of its initialization for no more than 15 microseconds, and thus use baking materials with a diameter of 0.2-0.7 mm. 5 Consent to the invention as a result of the preparation of bins, it is not possible to use the shipments only from metals, but also from metal alloys.
  • metals and alloys are used that have an energy reduction of sublimation energy equal to 10 or more than 0.9.
  • metals selected from the series: aluminum, aluminum, 15th century, copper, silver, nickel, iron, aluminum, molybdenum.
  • alloys selected from the order: brass, nickel, iron, nickel.
  • alloy composition (% of mass): 80 nickel - 20 degrees, 50 iron - 50 nickel. 20
  • blasting is carried out in a gaseous environment using gases taken from the group: water, gedi, aron.
  • gas as a gas medium, as well as gas as a gas, acetylene or 25 mixtures with argon or helium.
  • the process is pressurized (0.5- ⁇ 0) - » ⁇ 0 Pa.
  • Such a product has a low sintering temperature, a high dispersion, one-stop and low-density, and a high chemical resistance.
  • the prerequisite for an efficient process is also the impulse to the process. Over a period of exposure of more than 15 msec, a decrease in the cooling rate occurs and improved components are used.
  • non-organic materials resulting from electric explosions of metallic materials, depend on the size of the particles. . ⁇ sn ⁇ vnym ⁇ a ⁇ ame ⁇ m, ⁇ edelyaschim s ⁇ edny ⁇ azme ⁇ chas ⁇ its but yavlyae ⁇ sya specific ene ⁇ giya B (J / g), introduced in ⁇ v ⁇ dni ⁇ , ⁇ ichem and ⁇ ⁇ " ⁇ sv ⁇ yu ⁇ che ⁇ ed introduced in ⁇ v ⁇ dni ⁇ specific ene ⁇ giya zavisi ⁇ ⁇ mn ⁇ zhes ⁇ va ⁇ a ⁇ ame ⁇ v: ⁇ a ⁇ ame ⁇ v ⁇ az ⁇ yadn ⁇ g ⁇ ⁇ n ⁇ u ⁇ a, ma ⁇ e- ⁇ iala and sizing in the blown up metal baking, a gas-quick gas compressor, in a quick blowing up these bunkers.
  • N is the step of the channel
  • ® is the diameter of the channel
  • ⁇ is the boot diameter
  • the isolated electrical outlet of the power supply is connected to the energy storage device through the power supply unit, which consists of a
  • the installation has a cleaning device, a connected device
  • the elec- trode 7 is electrically disconnected from the earth ⁇ e ⁇ anizm ⁇ dachi ⁇ azmeschen on iz ⁇ lyatsi- ⁇ nn ⁇ m ⁇ sn ⁇ vanii v ⁇ lyuchae ⁇ II and a node de ⁇ matsii ⁇ v ⁇ l ⁇ i 12 ⁇ daschie ⁇ li ⁇ i 13 ⁇ a ⁇ ush ⁇ u with ⁇ v ⁇ l ⁇ y 14 and 30 vz ⁇ yvaemy ⁇ ez ⁇ ⁇ v ⁇ l ⁇ i 15. ⁇ ea ⁇ ⁇ a ⁇ ub ⁇ ami 16 and 17 s ⁇ edinen s ⁇ sb ⁇ ni ⁇ m ⁇ sh ⁇ a 18 ⁇ y capacitance imee ⁇ Space for room 19.
  • Highly dispersed aluminum nitride is produced by the explosion of aluminum in the nitrogen atmosphere.
  • -y-sostoyashsh ⁇ / ⁇ -g 2.2.
  • the blast chamber is evacuated and filled with a gas medium - nitrogen at a pressure of 10 10 Pa.
  • the batch was supplied with an energy of 45 J / mm. This is 0.9 "2 s and change-2 .. Energy for the supply was supplied within 3.3 ⁇ s.
  • Nickel powder The average size is 5 particles of 0.22 ⁇ m, the specific size is 18 ug / g, and the Picnic area is 8.6 g / cm. The temperature is 4 ° C.
  • the energy input was 62 Jmm. Energy input time is 5 microseconds.
  • Table I presents the data on the parameters used in this method of metals and alloys.
  • Table 2 provides data on the parameters of the process for the receipt of highly dispersed data.
  • the products obtained by the proposed method are: they have a high chemical activity and are able to achieve a lower tempera- ture; is sealed in the mode of sauryurasprostostavlyayuschego process and extremely low temperatures; easy intermetallic connections; has a reduced output of elec- trons.

Landscapes

  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

L'invention se rapporte à un procédé permettant d'obtenir des poudres hautement dispersives de substances non organiques par explosion d'ébauches de métal au moyen d'une impulsion de courant électrique dans un milieu gazeux sous haute pression, à une densité spécifique de l'énergie appliquée à l'ébauche comprise entre 90 % de l'énergie de sublimation du métal de l'ébauche et l'énergie de sa ionisation, pendant une durée maximum de 15 msec. Une installation permettant d'obtenir des poudres hautement dispersives par ledit procédé comprend un accumulateur d'énergie électrique (2), un réacteur pour l'explosion de l'ébauche de métal (6), qui est pourvu de deux électrodes (7, 8), et d'un mécanisme d'avance de l'ébauche (9). L'une des électrodes du réacteur (8) est mise à la terre et montée à une distance de l'ébauche égale à 5-10 diamètres et à une distance du mécanisme d'avance égale à 20-40 diamètres. Pour augmenter la précision de maintien des paramètres désirés, le mécanisme d'avance de l'ébauche est équipé d'une unité de formage servant à donner à l'ébauche une forme en spirale (12). L'électrode (7) du réacteur est connectée à l'accumulateur d'énergie électrique par un commutateur (3), lequel est constitué par un diviseur de tension (4) et par un organe d'arrêt de décharge à deux électrodes (5).
PCT/RO1992/000064 1991-04-04 1992-03-31 Procede et installation permettant d'obtenir des poudres hautement dispersives de substances non organiques Ceased WO1992017303A1 (fr)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP50904792A JP2002517172A (ja) 1991-04-04 1992-03-31 高度に分散された粉末を製造する方法及び該方法を実施するための装置

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
SU4947132 RU2048277C1 (ru) 1991-04-04 1991-04-04 Способ получения высокодисперсных порошков неорганических веществ
RU4947132/02 1991-04-04
RU5004107/02 1991-07-18
SU5004107 RU2048278C1 (ru) 1991-07-18 1991-07-18 Установка для получения высокодисперсных порошков неорганических материалов электрическим взрывом и реактор для взрыва металлической заготовки

Publications (1)

Publication Number Publication Date
WO1992017303A1 true WO1992017303A1 (fr) 1992-10-15

Family

ID=26666257

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/RO1992/000064 Ceased WO1992017303A1 (fr) 1991-04-04 1992-03-31 Procede et installation permettant d'obtenir des poudres hautement dispersives de substances non organiques

Country Status (2)

Country Link
JP (1) JP2002517172A (fr)
WO (1) WO1992017303A1 (fr)

Cited By (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993023189A1 (fr) * 1992-05-19 1993-11-25 Mezhdunarodnaya Assotsiatsiya 'zemlya I Kosmonavtika Procede d'obtention de materiaux a l'etat disperse au moyen d'une structure d'agglomerat de particules
EP0718061A1 (fr) * 1994-12-23 1996-06-26 Institute of Petroleum Chemistry, Russian Academy of Sciences Poudre métallique active
RU2139777C1 (ru) * 1998-08-10 1999-10-20 Институт сильноточной электроники СО РАН Установка для получения высокодисперсных порошков
RU2201798C2 (ru) * 2001-02-19 2003-04-10 Российский Федеральный Ядерный Центр - Всероссийский Научно-Исследовательский Институт Экспериментальной Физики Способ получения ультрадисперсных материалов
KR100394390B1 (ko) * 2001-05-29 2003-08-14 한국원자력연구소 전기폭발법에 의한 금속 나노분말 제조방법 및 장치
EP1230017A4 (fr) * 1999-09-03 2003-09-10 American Inter Metallics Inc Dispositifs et procedes servant a fabriquer des poudres
KR100407160B1 (ko) * 2001-05-12 2003-11-28 한국원자력연구소 나노분말 제조 장치
KR100446956B1 (ko) * 2002-04-23 2004-09-01 한국전기연구원 나노분말 제조용 전기폭발 장비의 피딩장치
US6972115B1 (en) 1999-09-03 2005-12-06 American Inter-Metallics, Inc. Apparatus and methods for the production of powders
DE102006031888A1 (de) * 2006-07-07 2008-01-10 Ilt Industrie-Luftfiltertechnik Gmbh Ionisationselement und elektrostatischer Filter
RU2465982C1 (ru) * 2011-07-15 2012-11-10 Учреждение Российской академии наук Институт электрофизики Уральского отделения РАН (ИЭФ УрО РАН) Способ получения нанопорошков оксида цинка, допированных медью, методом электрического взрыва проволоки
CN103990534A (zh) * 2014-05-20 2014-08-20 大连理工大学 一种等离子体辅助高能球磨制备AlN纳米粉末的方法
CN104275488A (zh) * 2013-11-21 2015-01-14 大林企业株式会社 利用电爆炸方法的纳米粉末制备方法
RU2699886C1 (ru) * 2018-12-13 2019-09-11 Федеральное государственное бюджетное учреждение науки Институт физики прочности и матероиаловедения Сибирского отделения Российской академии наук (ИФПМ СО РАН) Способ получения металлического порошка и устройство для его осуществления
CN110862072A (zh) * 2019-11-07 2020-03-06 深圳第三代半导体研究院 一种纳米金属氧化物材料的制备方法
RU211926U1 (ru) * 2021-12-28 2022-06-28 Федеральное государственное автономное образовательное учреждение высшего образования "Национальный исследовательский Томский государственный университет" Устройство для получения наночастиц оксидов металлов путем электрического взрыва проволоки

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5693249B2 (ja) * 2011-01-13 2015-04-01 国立大学法人長岡技術科学大学 合金微粒子の製造方法
CN104995134B (zh) * 2013-01-22 2018-06-05 Mcd技术有限公司 生产碳纳米结构的方法及装置
KR102029474B1 (ko) * 2013-06-28 2019-10-07 삼성전기주식회사 전기폭발에 의한 금속 나노분말의 제조방법 및 제조장치

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3634040A (en) * 1970-05-27 1972-01-11 Us Air Force Metal explosion apparatus
FR2222159A1 (fr) * 1973-03-22 1974-10-18 Industrial Materials Tech
SU829199A1 (ru) * 1979-05-22 1981-05-15 Институт высоких температур АН СССР Устройство дл получени порошковэлЕКТРОиМпульСНыМ РАСпылЕНиЕМ РАСплАВОВ

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3634040A (en) * 1970-05-27 1972-01-11 Us Air Force Metal explosion apparatus
FR2222159A1 (fr) * 1973-03-22 1974-10-18 Industrial Materials Tech
SU829199A1 (ru) * 1979-05-22 1981-05-15 Институт высоких температур АН СССР Устройство дл получени порошковэлЕКТРОиМпульСНыМ РАСпылЕНиЕМ РАСплАВОВ

Cited By (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1993023189A1 (fr) * 1992-05-19 1993-11-25 Mezhdunarodnaya Assotsiatsiya 'zemlya I Kosmonavtika Procede d'obtention de materiaux a l'etat disperse au moyen d'une structure d'agglomerat de particules
EP0718061A1 (fr) * 1994-12-23 1996-06-26 Institute of Petroleum Chemistry, Russian Academy of Sciences Poudre métallique active
RU2139777C1 (ru) * 1998-08-10 1999-10-20 Институт сильноточной электроники СО РАН Установка для получения высокодисперсных порошков
US6972115B1 (en) 1999-09-03 2005-12-06 American Inter-Metallics, Inc. Apparatus and methods for the production of powders
EP1230017A4 (fr) * 1999-09-03 2003-09-10 American Inter Metallics Inc Dispositifs et procedes servant a fabriquer des poudres
RU2201798C2 (ru) * 2001-02-19 2003-04-10 Российский Федеральный Ядерный Центр - Всероссийский Научно-Исследовательский Институт Экспериментальной Физики Способ получения ультрадисперсных материалов
KR100407160B1 (ko) * 2001-05-12 2003-11-28 한국원자력연구소 나노분말 제조 장치
KR100394390B1 (ko) * 2001-05-29 2003-08-14 한국원자력연구소 전기폭발법에 의한 금속 나노분말 제조방법 및 장치
KR100446956B1 (ko) * 2002-04-23 2004-09-01 한국전기연구원 나노분말 제조용 전기폭발 장비의 피딩장치
DE102006031888A1 (de) * 2006-07-07 2008-01-10 Ilt Industrie-Luftfiltertechnik Gmbh Ionisationselement und elektrostatischer Filter
DE102006031888A8 (de) * 2006-07-07 2008-05-21 Ilt Industrie-Luftfiltertechnik Gmbh Ionisationselement und elektrostatischer Filter
DE102006031888B4 (de) * 2006-07-07 2009-01-29 Ilt Industrie-Luftfiltertechnik Gmbh Ionisationselement und elektrostatischer Filter
RU2465982C1 (ru) * 2011-07-15 2012-11-10 Учреждение Российской академии наук Институт электрофизики Уральского отделения РАН (ИЭФ УрО РАН) Способ получения нанопорошков оксида цинка, допированных медью, методом электрического взрыва проволоки
CN104275488A (zh) * 2013-11-21 2015-01-14 大林企业株式会社 利用电爆炸方法的纳米粉末制备方法
CN103990534A (zh) * 2014-05-20 2014-08-20 大连理工大学 一种等离子体辅助高能球磨制备AlN纳米粉末的方法
RU2699886C1 (ru) * 2018-12-13 2019-09-11 Федеральное государственное бюджетное учреждение науки Институт физики прочности и матероиаловедения Сибирского отделения Российской академии наук (ИФПМ СО РАН) Способ получения металлического порошка и устройство для его осуществления
CN110862072A (zh) * 2019-11-07 2020-03-06 深圳第三代半导体研究院 一种纳米金属氧化物材料的制备方法
RU211926U1 (ru) * 2021-12-28 2022-06-28 Федеральное государственное автономное образовательное учреждение высшего образования "Национальный исследовательский Томский государственный университет" Устройство для получения наночастиц оксидов металлов путем электрического взрыва проволоки

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