WO1982001568A1 - Utilisation de l'ethanol dans le pulpage alcalin - Google Patents
Utilisation de l'ethanol dans le pulpage alcalin Download PDFInfo
- Publication number
- WO1982001568A1 WO1982001568A1 PCT/US1980/001451 US8001451W WO8201568A1 WO 1982001568 A1 WO1982001568 A1 WO 1982001568A1 US 8001451 W US8001451 W US 8001451W WO 8201568 A1 WO8201568 A1 WO 8201568A1
- Authority
- WO
- WIPO (PCT)
- Prior art keywords
- ethanol
- pulping
- wood
- pulp
- naoh
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C3/00—Pulping cellulose-containing materials
- D21C3/20—Pulping cellulose-containing materials with organic solvents or in solvent environment
Definitions
- This invention relates to wood pulping using chemical pulping media and more particularly relates to such media which result in superior wood pulps with a lower refining energy requirement.
- a method for manufacturing wood pulp which comprises pulping wood with a mixture of ethanol and sodium hydroxide.
- the invention also includes wood pulp manufactured in accordance with the method. DETAILED DESCRIPTION OF THE INVENTION
- the pulping time in accordance with the preferred embodiment, is from about 1/2 to about 4 hours and the pulping temperature is from about 100 to about 200°C.
- any wood can be pulped in accordance with the method of the invention to obtain a superior wood pulp than was obtained by commercially usuable prior arti chemical wood pulping methods.
- Spruce chips are cooked in an electrically heated digester with mixtures of water and ethanol (1 :1 by volume), at a 5:1 liquor to wood ratio, 170°C for 2-1/2 hr.
- cooks under the same conditions were carried out with the addition of 20% NaOH (calculated on wood), and with alkali alone.
- Table 1 shows that ethanol plus NaOH (column 1) is more effective than either ingredient alone
- the ethanol-NaOH process is especially significant in the area of high-yield pulping, because it allows a greater preservation of carbohydrates than NaOH alone. So, e.g., an ethanol-NaOH pulp of 81.6% yield (obtained with 5% NaOH, 170°C, 45 min.) has a Kappa number of 157, while a soda pulp (obtained with 20% NaOH) of 66% yield has a very similar (147) Kappa number. This is because in soda pulping only limited delignif ication can occur, thus low Kappa number pulps are obtained.
Landscapes
- Paper (AREA)
Abstract
Procede de fabrication de pulpe de bois comprenant la reduction en pulpe du bois au moyen d'un melange d'ethanol et d'hydroxyde de sodium et pulpe de bois obtenue conformement a ce procede.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/US1980/001451 WO1982001568A1 (fr) | 1980-10-29 | 1980-10-29 | Utilisation de l'ethanol dans le pulpage alcalin |
| EP19810901196 EP0063565A1 (fr) | 1980-10-29 | 1980-10-29 | Utilisation de l'ethanol dans le pulpage alcalin |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PCT/US1980/001451 WO1982001568A1 (fr) | 1980-10-29 | 1980-10-29 | Utilisation de l'ethanol dans le pulpage alcalin |
| WOUS80/01451801029 | 1980-10-29 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| WO1982001568A1 true WO1982001568A1 (fr) | 1982-05-13 |
Family
ID=22154626
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PCT/US1980/001451 Ceased WO1982001568A1 (fr) | 1980-10-29 | 1980-10-29 | Utilisation de l'ethanol dans le pulpage alcalin |
Country Status (2)
| Country | Link |
|---|---|
| EP (1) | EP0063565A1 (fr) |
| WO (1) | WO1982001568A1 (fr) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4496426A (en) * | 1982-04-06 | 1985-01-29 | Md-Verwaltungesellschaft Nicolaus Gmbh & Co. Kg | Process for the continuous extraction of vegetable-fiber material in two stages |
| WO2012027767A1 (fr) | 2010-09-02 | 2012-03-08 | Annikki Gmbh | Procédé d'obtention de lignine |
| WO2013164234A1 (fr) | 2012-05-03 | 2013-11-07 | Annikki Gmbh | Procédé de production de cellulose à faible teneur en lignine à partir d'un matériau lignocellulosique |
| WO2015075080A1 (fr) | 2013-11-20 | 2015-05-28 | Annikki Gmbh | Procédé de fractionnement de matières lignocellulosiques |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2166540A (en) * | 1937-12-17 | 1939-07-18 | Univ Minnesota | Alcoholic treatment of ligneous cellulosic material |
| JPH05149905A (ja) * | 1991-12-02 | 1993-06-15 | Canon Inc | 測定装置 |
-
1980
- 1980-10-29 EP EP19810901196 patent/EP0063565A1/fr not_active Withdrawn
- 1980-10-29 WO PCT/US1980/001451 patent/WO1982001568A1/fr not_active Ceased
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2166540A (en) * | 1937-12-17 | 1939-07-18 | Univ Minnesota | Alcoholic treatment of ligneous cellulosic material |
| JPH05149905A (ja) * | 1991-12-02 | 1993-06-15 | Canon Inc | 測定装置 |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4496426A (en) * | 1982-04-06 | 1985-01-29 | Md-Verwaltungesellschaft Nicolaus Gmbh & Co. Kg | Process for the continuous extraction of vegetable-fiber material in two stages |
| WO2012027767A1 (fr) | 2010-09-02 | 2012-03-08 | Annikki Gmbh | Procédé d'obtention de lignine |
| US9487549B2 (en) | 2010-09-02 | 2016-11-08 | Annikki Gmbh | Preparation of lignin |
| WO2013164234A1 (fr) | 2012-05-03 | 2013-11-07 | Annikki Gmbh | Procédé de production de cellulose à faible teneur en lignine à partir d'un matériau lignocellulosique |
| WO2015075080A1 (fr) | 2013-11-20 | 2015-05-28 | Annikki Gmbh | Procédé de fractionnement de matières lignocellulosiques |
Also Published As
| Publication number | Publication date |
|---|---|
| EP0063565A1 (fr) | 1982-11-03 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| AK | Designated states |
Designated state(s): DE GB JP US |
|
| AL | Designated countries for regional patents |
Designated state(s): AT CH DE FR GB LU NL SE |
|
| REG | Reference to national code |
Ref country code: DE Ref legal event code: 8642 |