UY27519A1 - "PROCEDURE FOR THE PREPARATION OF OPTICALLY PURE OR ENRICHED RACEMIC TETRALONE" - Google Patents
"PROCEDURE FOR THE PREPARATION OF OPTICALLY PURE OR ENRICHED RACEMIC TETRALONE"Info
- Publication number
- UY27519A1 UY27519A1 UY27519A UY27519A UY27519A1 UY 27519 A1 UY27519 A1 UY 27519A1 UY 27519 A UY27519 A UY 27519A UY 27519 A UY27519 A UY 27519A UY 27519 A1 UY27519 A1 UY 27519A1
- Authority
- UY
- Uruguay
- Prior art keywords
- procedure
- optically pure
- preparation
- racemic tetralone
- liquid phase
- Prior art date
Links
- 238000000034 method Methods 0.000 title abstract 3
- XHLHPRDBBAGVEG-UHFFFAOYSA-N 1-tetralone Chemical compound C1=CC=C2C(=O)CCCC2=C1 XHLHPRDBBAGVEG-UHFFFAOYSA-N 0.000 title 1
- WEVYAHXRMPXWCK-UHFFFAOYSA-N Acetonitrile Chemical compound CC#N WEVYAHXRMPXWCK-UHFFFAOYSA-N 0.000 abstract 3
- 239000007791 liquid phase Substances 0.000 abstract 2
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 abstract 1
- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 abstract 1
- 238000013375 chromatographic separation Methods 0.000 abstract 1
- 239000004927 clay Substances 0.000 abstract 1
- 239000011229 interlayer Substances 0.000 abstract 1
- 230000003287 optical effect Effects 0.000 abstract 1
- 239000002245 particle Substances 0.000 abstract 1
- 239000012071 phase Substances 0.000 abstract 1
- VGKDLMBJGBXTGI-SJCJKPOMSA-N sertraline Chemical compound C1([C@@H]2CC[C@@H](C3=CC=CC=C32)NC)=CC=C(Cl)C(Cl)=C1 VGKDLMBJGBXTGI-SJCJKPOMSA-N 0.000 abstract 1
- 229960002073 sertraline Drugs 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Un procedimiento para la producción de sertralina sustancialmente pura en forma óptica, utiliza una separación cromatográfica sobre una fase quiral sólida y estacionaria de partículas esféricas de arcilla con una intercapa que contiene un complejo metálico-orgánico ópticamente puro, y una fase líquida móvil que preferentemente contiene al menos metil-acetato. La fase líquida móvil está preferentemente libre de acetonitrilo. El procedimiento puede operar a temperaturas superiores a 40s C.A process for the production of substantially pure sertraline in optical form, uses a chromatographic separation on a solid and stationary chiral phase of spherical clay particles with an interlayer containing an optically pure metallic-organic complex, and a mobile liquid phase that preferably contains at least methyl acetate. The mobile liquid phase is preferably free of acetonitrile. The procedure can operate at temperatures above 40s C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| UY27519A UY27519A1 (en) | 2002-10-28 | 2002-10-28 | "PROCEDURE FOR THE PREPARATION OF OPTICALLY PURE OR ENRICHED RACEMIC TETRALONE" |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| UY27519A UY27519A1 (en) | 2002-10-28 | 2002-10-28 | "PROCEDURE FOR THE PREPARATION OF OPTICALLY PURE OR ENRICHED RACEMIC TETRALONE" |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| UY27519A1 true UY27519A1 (en) | 2003-05-30 |
Family
ID=38812709
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| UY27519A UY27519A1 (en) | 2002-10-28 | 2002-10-28 | "PROCEDURE FOR THE PREPARATION OF OPTICALLY PURE OR ENRICHED RACEMIC TETRALONE" |
Country Status (1)
| Country | Link |
|---|---|
| UY (1) | UY27519A1 (en) |
-
2002
- 2002-10-28 UY UY27519A patent/UY27519A1/en not_active Application Discontinuation
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 109 | Application deemed to be withdrawn |
Effective date: 20150126 |