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UST968002I4 - Polyurethane foam stabilized against scorch with a mixture of hydroquinone and a phosphite containing secondary antioxidant - Google Patents

Polyurethane foam stabilized against scorch with a mixture of hydroquinone and a phosphite containing secondary antioxidant Download PDF

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Publication number
UST968002I4
UST968002I4 US05/771,706 US77170677A UST968002I4 US T968002 I4 UST968002 I4 US T968002I4 US 77170677 A US77170677 A US 77170677A US T968002 I4 UST968002 I4 US T968002I4
Authority
US
United States
Prior art keywords
mixture
hydroquinone
phosphite
stabilized against
secondary antioxidant
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
US05/771,706
Inventor
William F. Baxter, Jr.
Ted L. Douglas
Gether Irick
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Priority to US05/771,706 priority Critical patent/UST968002I4/en
Application granted granted Critical
Publication of UST968002I4 publication Critical patent/UST968002I4/en
Pending legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/0014Use of organic additives
    • C08J9/0038Use of organic additives containing phosphorus
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/0014Use of organic additives
    • C08J9/0023Use of organic additives containing oxygen
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/04Oxygen-containing compounds
    • C08K5/13Phenols; Phenolates
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/49Phosphorus-containing compounds
    • C08K5/51Phosphorus bound to oxygen
    • C08K5/52Phosphorus bound to oxygen only
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08KUse of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K5/00Use of organic ingredients
    • C08K5/49Phosphorus-containing compounds
    • C08K5/51Phosphorus bound to oxygen
    • C08K5/52Phosphorus bound to oxygen only
    • C08K5/524Esters of phosphorous acids, e.g. of H3PO3
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2375/00Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
    • C08J2375/04Polyurethanes

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Emergency Medicine (AREA)
  • Polyurethanes Or Polyureas (AREA)

Abstract

polyurethane foams are stabilized against scorching when a mixture of hydroquinone and a phosphite containing secondary antioxidant is present in a foam-forming mixture of an organic polyisocyanate with a polyether polyol in the presence of a reaction catalyst and a foaming agent. The proportion of hydroquinone to the phosphite is in the range of 10:1 to about 1:1. Especially advantageous results can be obtained by adding p,p'-dialkylphenylamines containing between 3 and 18 carbon atoms in the alkyl moiety to the above two stabilizers. When the amine is present the stabilizer mixture usually comprises between about 15 and 90% by weight of the amine and the rest of the stabilizer comprises the hydroquinone and the phosphite in the range relative to each other as given above. The proportion of the stabilizer mixture is usually between about 10 and about 50,000 parts per million parts of the polyether polyol. The stabilizer mixture is preferably mixed with the polyol before using the polyol in making urethane foams.
US05/771,706 1977-02-24 1977-02-24 Polyurethane foam stabilized against scorch with a mixture of hydroquinone and a phosphite containing secondary antioxidant Pending UST968002I4 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US05/771,706 UST968002I4 (en) 1977-02-24 1977-02-24 Polyurethane foam stabilized against scorch with a mixture of hydroquinone and a phosphite containing secondary antioxidant

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US05/771,706 UST968002I4 (en) 1977-02-24 1977-02-24 Polyurethane foam stabilized against scorch with a mixture of hydroquinone and a phosphite containing secondary antioxidant

Publications (1)

Publication Number Publication Date
UST968002I4 true UST968002I4 (en) 1978-03-07

Family

ID=25092706

Family Applications (1)

Application Number Title Priority Date Filing Date
US05/771,706 Pending UST968002I4 (en) 1977-02-24 1977-02-24 Polyurethane foam stabilized against scorch with a mixture of hydroquinone and a phosphite containing secondary antioxidant

Country Status (1)

Country Link
US (1) UST968002I4 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4178420A (en) 1978-07-21 1979-12-11 Stauffer Chemical Company Amine antioxidants as antiscorch agents in flame retarded polyurethane foams
EP0564259A3 (en) * 1992-03-30 1994-01-19 Arco Chem Tech
US20110230579A1 (en) * 2010-03-18 2011-09-22 R.T. Vanderbilt Company, Inc. Polyurethane Foam Scorch Inhibitor

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4178420A (en) 1978-07-21 1979-12-11 Stauffer Chemical Company Amine antioxidants as antiscorch agents in flame retarded polyurethane foams
EP0564259A3 (en) * 1992-03-30 1994-01-19 Arco Chem Tech
US20110230579A1 (en) * 2010-03-18 2011-09-22 R.T. Vanderbilt Company, Inc. Polyurethane Foam Scorch Inhibitor
US8716359B2 (en) 2010-03-18 2014-05-06 Vanderbilt Chemicals, Llc Polyurethane foam scorch inhibitor

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