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UST896051I4 - Zjl fxx mss mss^h disperstbzg,osi for making microporous materials - Google Patents

Zjl fxx mss mss^h disperstbzg,osi for making microporous materials Download PDF

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Publication number
UST896051I4
UST896051I4 US896051DH UST896051I4 US T896051 I4 UST896051 I4 US T896051I4 US 896051D H US896051D H US 896051DH US T896051 I4 UST896051 I4 US T896051I4
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solvent
mss
solution
disperstbzg
zjl
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    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/02Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • C08J3/07Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media from polymer solutions

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  • the microblending being achieved in about 0.5-5 seconds in a high shear mixing zone having a shear rate of 1,000l50,000 reciprocal seconds and of a stream of a solution of a polymeric component, and particularly a linear polyurethane or a blend of a linear polyurethane and poly (vinyl chloride), at about -60 C.

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  • Chemical & Material Sciences (AREA)
  • Dispersion Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)

Abstract

A PROCESS FOR FORMING A COLLOIDAL POLYMERIC DISPERSION USED IN MAKING MICROPOROUS SHEET MATERIAL HAVING A SECANT TENSILE MODULUS AT 5% ELONGATION OF ABOUT 600 P.S.I. BY MICROBLENDING A SOLUTION OF A POLYMERIC COMPONENT AND A SOLUTION OF A SOLVENT AND A NON-SOLVENT FOR THE POLYMERIC COMPONENT. THE MICROBLENDING BEING ACHIEVED IN ABOUT 0.5-5 SECONDS IN A HIGH SHEAR MIXING ZONE HAVING A SHEAR RATE OF 1,000-15,000 RECIPROCAL SECONDS AND OF A STREAM OF A SOLUTION OF A POLYMERIC COMPONENT, AND PARTICULARLY A LINEAR POLYURETHANE OR A BLEND OF A LINEAR POLYURETHANE AND POLY (VINYL CHLORIDE), AT ABOUT 15-60* C. AND OF A STREAM OF AN ORGANIC SOLVENT AND NON-SOLVENT, PARTICLARLY WATER, AT ABOUT 20-50*C. THE QUANTITY OF ORGANIC SOLVENT BEING ABOUT 95-25% AND THE QUAN-

TITY OF NON-SOLVENT BEING ABOUT 5-75%. THE TEMPERATURE OF THE BLEND BEING THEREAFTER REDUCED ABOUT 2-50*C. TO FORM A COLLOIDAL POLYMERIC DISPERSION HAVING A NON-SOLVENT CONTENT OF ABOUT 3-5% BY WEIGHT.

Description

DEFENSIVE PUBLICATION Published at the request of the applicant or owner in accordance with the Notice of Dec. 16, 1969, 869 0.G. 687. The abstracts t Defensive Publication applications are identified by distinctly numbered series and are arranged chronologically. The heading of each abstract indicates the number of pages of specification, including claims and sheets of drawings contained in the application as originally filed. The files of these applications are available to the public for inspection and reproduction may be purchased for 30 cents a sheet.
Defensive Publication applications have not been examined as to the merits of alleged invention. The Patent Ofllce makes no assertion as to the novelty of the disclosed subject matter.
PUBLISHED MARCH 28, 1972 A process for forming a colloidal polymeric dispersion used in making microporous sheet material having a secant tensile modulus at elongation of about 600 p.s.i. by microblending a solution of a polymeric component and a solution of a solvent and a non-solvent for the polymeric component. The microblending being achieved in about 0.5-5 seconds in a high shear mixing zone having a shear rate of 1,000l50,000 reciprocal seconds and of a stream of a solution of a polymeric component, and particularly a linear polyurethane or a blend of a linear polyurethane and poly (vinyl chloride), at about -60 C. and of a stream of an organic solvent and non-solvent, particularly water, at about -50" C. The quantity of organic solvent being about -25% and the quantity of non-solvent being about 5-75 The temperature of the blend being thereafter reduced about 2-50 C. to form a colloidal polymeric dispersion having a non-solvent content of about 35% by weight.
' March 28, 1972 HAMLlN ETAL T896,051
PROCESS FOR FORMING COLLOIDAL POLYMERIC DISPERSIONS FOR MAKING MICROPOROUS MATERIALS Filed Nov. 12, 1970 lk J ATTORNEY
US896051D 1970-11-12 1970-11-12 Zjl fxx mss mss^h disperstbzg,osi for making microporous materials Pending UST896051I4 (en)

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US8913670A 1970-11-12 1970-11-12

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Cited By (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4054625A (en) 1972-08-30 1977-10-18 Crown Zellerbach Corporation Process for making fibers
US5164429A (en) * 1987-08-25 1992-11-17 Stranco, Inc. Polymer activation apparatus
US5284626A (en) * 1987-08-25 1994-02-08 Stranco, Inc. Polymer activation apparatus
US5338779A (en) * 1992-09-18 1994-08-16 Stranco, Inc Dry polymer activation apparatus and method
US6409926B1 (en) 1999-03-02 2002-06-25 United States Filter Corporation Air and water purification using continuous breakpoint halogenation and peroxygenation
US6419817B1 (en) 2000-06-22 2002-07-16 United States Filter Corporation Dynamic optimization of chemical additives in a water treatment system
US6423234B1 (en) 1999-03-02 2002-07-23 United States Filter Corporation Air and water purification using continuous breakpoint halogenation
US20030038277A1 (en) * 2001-08-09 2003-02-27 Roy Martin Calcium hypochlorite of reduced reactivity
US20030160004A1 (en) * 2002-02-26 2003-08-28 Roy Martin Free radical generator and method
US20030160005A1 (en) * 2002-02-26 2003-08-28 Roy Martin Enhanced air and water purification using continuous breakpoint halogenation with free oxygen radicals
US6620315B2 (en) 2001-02-09 2003-09-16 United States Filter Corporation System for optimized control of multiple oxidizer feedstreams
US6645400B2 (en) 2000-06-22 2003-11-11 United States Filter Corporation Corrosion control utilizing a hydrogen peroxide donor
US6716359B1 (en) 2000-08-29 2004-04-06 United States Filter Corporation Enhanced time-based proportional control
US20080245738A1 (en) * 2007-04-03 2008-10-09 Siemens Water Technologies Corp. Method and system for providing ultrapure water
US20110024365A1 (en) * 2009-07-30 2011-02-03 Zhee Min Jimmy Yong Baffle plates for an ultraviolet reactor
US20110180485A1 (en) * 2006-06-06 2011-07-28 Fluid Lines Ultraviolet light activated oxidation process for the reduction of organic carbon in semiconductor process water
US20110210266A1 (en) * 2007-04-03 2011-09-01 Siemens Water Technologies Corp. Method of irradiating a liquid
US20110210048A1 (en) * 2007-04-03 2011-09-01 Siemens Water Technologies Corp. System for controlling introduction of a reducing agent to a liquid stream
US20110210267A1 (en) * 2007-04-03 2011-09-01 Siemens Water Technologies Corp. Actinic radiation reactor
US20110210077A1 (en) * 2007-04-03 2011-09-01 Siemens Water Technologies Corp. Method and system for providing ultrapure water
US20110209530A1 (en) * 2007-04-03 2011-09-01 Siemens Water Technologies Corp. Method for measuring a concentration of a compound in a liquid stream
US8877067B2 (en) 2011-05-26 2014-11-04 Evoqua Water Technologies Llc Method and arrangement for a water treatment
US10343939B2 (en) 2006-06-06 2019-07-09 Evoqua Water Technologies Llc Ultraviolet light activated oxidation process for the reduction of organic carbon in semiconductor process water
US12103874B2 (en) 2006-06-06 2024-10-01 Evoqua Water Technologies Llc Ultraviolet light activated oxidation process for the reduction of organic carbon in semiconductor process water

Cited By (41)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4054625A (en) 1972-08-30 1977-10-18 Crown Zellerbach Corporation Process for making fibers
US5284627A (en) * 1987-08-25 1994-02-08 Stranco, Inc. Polymer activation apparatus
US5284626A (en) * 1987-08-25 1994-02-08 Stranco, Inc. Polymer activation apparatus
US5164429A (en) * 1987-08-25 1992-11-17 Stranco, Inc. Polymer activation apparatus
US5338779A (en) * 1992-09-18 1994-08-16 Stranco, Inc Dry polymer activation apparatus and method
US6409926B1 (en) 1999-03-02 2002-06-25 United States Filter Corporation Air and water purification using continuous breakpoint halogenation and peroxygenation
US6423234B1 (en) 1999-03-02 2002-07-23 United States Filter Corporation Air and water purification using continuous breakpoint halogenation
US6419817B1 (en) 2000-06-22 2002-07-16 United States Filter Corporation Dynamic optimization of chemical additives in a water treatment system
US6645400B2 (en) 2000-06-22 2003-11-11 United States Filter Corporation Corrosion control utilizing a hydrogen peroxide donor
US6716359B1 (en) 2000-08-29 2004-04-06 United States Filter Corporation Enhanced time-based proportional control
US6620315B2 (en) 2001-02-09 2003-09-16 United States Filter Corporation System for optimized control of multiple oxidizer feedstreams
US6623647B2 (en) 2001-02-09 2003-09-23 United States Filter Corporation Methods of optimized control of multiple oxidizer feedstreams
US20040224088A1 (en) * 2001-08-09 2004-11-11 United States Filter Corporation Calcium hypochlorite of reduced reactivity
US20030038277A1 (en) * 2001-08-09 2003-02-27 Roy Martin Calcium hypochlorite of reduced reactivity
US6776926B2 (en) 2001-08-09 2004-08-17 United States Filter Corporation Calcium hypochlorite of reduced reactivity
US7285223B2 (en) 2002-02-26 2007-10-23 Siemens Water Technologies Holding Corp. Enhanced air and water purification using continuous breakpoint halogenation with free oxygen radicals
US20030160005A1 (en) * 2002-02-26 2003-08-28 Roy Martin Enhanced air and water purification using continuous breakpoint halogenation with free oxygen radicals
US20050109709A1 (en) * 2002-02-26 2005-05-26 Usfilter Corporation Enhanced air and water purification using continuous breakpoint halogenation with free oxygen radicals
US6991735B2 (en) 2002-02-26 2006-01-31 Usfilter Corporation Free radical generator and method
US7108781B2 (en) 2002-02-26 2006-09-19 Usfilter Corporation Enhanced air and water purification using continuous breakpoint halogenation with free oxygen radicals
US20030160004A1 (en) * 2002-02-26 2003-08-28 Roy Martin Free radical generator and method
US12103874B2 (en) 2006-06-06 2024-10-01 Evoqua Water Technologies Llc Ultraviolet light activated oxidation process for the reduction of organic carbon in semiconductor process water
US10550020B2 (en) 2006-06-06 2020-02-04 Evoqua Water Technologies Llc Ultraviolet light activated oxidation process for the reduction of organic carbon in semiconductor process water
US10343939B2 (en) 2006-06-06 2019-07-09 Evoqua Water Technologies Llc Ultraviolet light activated oxidation process for the reduction of organic carbon in semiconductor process water
US20110180485A1 (en) * 2006-06-06 2011-07-28 Fluid Lines Ultraviolet light activated oxidation process for the reduction of organic carbon in semiconductor process water
US8652336B2 (en) 2006-06-06 2014-02-18 Siemens Water Technologies Llc Ultraviolet light activated oxidation process for the reduction of organic carbon in semiconductor process water
US20110210077A1 (en) * 2007-04-03 2011-09-01 Siemens Water Technologies Corp. Method and system for providing ultrapure water
US9365435B2 (en) 2007-04-03 2016-06-14 Evoqua Water Technologies Llc Actinic radiation reactor
US20110210048A1 (en) * 2007-04-03 2011-09-01 Siemens Water Technologies Corp. System for controlling introduction of a reducing agent to a liquid stream
US20110209530A1 (en) * 2007-04-03 2011-09-01 Siemens Water Technologies Corp. Method for measuring a concentration of a compound in a liquid stream
US20080245738A1 (en) * 2007-04-03 2008-10-09 Siemens Water Technologies Corp. Method and system for providing ultrapure water
US20110210266A1 (en) * 2007-04-03 2011-09-01 Siemens Water Technologies Corp. Method of irradiating a liquid
US8741155B2 (en) 2007-04-03 2014-06-03 Evoqua Water Technologies Llc Method and system for providing ultrapure water
US8753522B2 (en) 2007-04-03 2014-06-17 Evoqua Water Technologies Llc System for controlling introduction of a reducing agent to a liquid stream
US20080245737A1 (en) * 2007-04-03 2008-10-09 Siemens Water Technologies Corp. Method and system for providing ultrapure water
US8961798B2 (en) 2007-04-03 2015-02-24 Evoqua Water Technologies Llc Method for measuring a concentration of a compound in a liquid stream
US20110210267A1 (en) * 2007-04-03 2011-09-01 Siemens Water Technologies Corp. Actinic radiation reactor
US9764968B2 (en) 2007-04-03 2017-09-19 Evoqua Water Technologies Llc Method and system for providing ultrapure water
US20110024365A1 (en) * 2009-07-30 2011-02-03 Zhee Min Jimmy Yong Baffle plates for an ultraviolet reactor
US8591730B2 (en) 2009-07-30 2013-11-26 Siemens Pte. Ltd. Baffle plates for an ultraviolet reactor
US8877067B2 (en) 2011-05-26 2014-11-04 Evoqua Water Technologies Llc Method and arrangement for a water treatment

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