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UST878013I4 - Defensive publication - Google Patents

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Publication number
UST878013I4
UST878013I4 US878013DH UST878013I4 US T878013 I4 UST878013 I4 US T878013I4 US 878013D H US878013D H US 878013DH US T878013 I4 UST878013 I4 US T878013I4
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United States
Prior art keywords
defensive publication
carbodiimide
incorporated
emulsions
pat
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    • GPHYSICS
    • G03PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
    • G03CPHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
    • G03C1/00Photosensitive materials
    • G03C1/005Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein
    • G03C1/06Silver halide emulsions; Preparation thereof; Physical treatment thereof; Incorporation of additives therein with non-macromolecular additives
    • G03C1/30Hardeners

Definitions

  • Photographic silver halide emulsions containing an incorporated pyrazolone magenta dye-forming coupler can be hardened with an incorporated carbodiimide hardener. Photographic elements comprising such emulsions, when exposed and processed, produce prints having low stain and high maximum density.
  • Carbodiimide hardening agents including those described in Sheehan US. Pat. 2,938,892 issued May 31, 1960, Sheehan US. Pat. 3,135,- 748 issued June 2, 1964, and Brunken German Pat. 7218 issued May 10, 1954, can be used.
  • Suitable carbodiimide hardening agents can be represented by the formula where each of R and R is an organic radical such as alkyl, alkoxy, allyl, aryl or heterocyclic groups.
  • Suitable carbodiimide hardening agents which are incorporated in the photographic materials described herein are 1,3-dimethylcarbodiimide, 1-methyl-3-methoxymethylcarbodiimide, dicyclohexylcarbodiimide and l-ethyl-3-[3-dirnethylaminopropyl] carbodiimide hydrochloride.
  • a process for preparing the aforementioned photographic silver halide materials from coating compositions comprising incorporated pyrazolone magenta dye-forming couplers and carbodiimide hardening agents is also disclosed.
  • the emulsions of the invention can be used in photographic elements in layers containing high-speed chemically sensitized and spectrally sensitized silver halide emulsions, anti-foggants, coating aids, plasticizers, conventional hardeners and the like, such as described in Dunn U.S. Pat. 3,297,446 (columns 4-9).

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  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Spectroscopy & Molecular Physics (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • General Physics & Mathematics (AREA)
  • Silver Salt Photography Or Processing Solution Therefor (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)

Description

DEFENSIVE PUBLICATION UNITED STATES PATENT OFFICE Published at the request of the applicant or owner in accordance with the Notice of Dec. 16. 1969, 869 O.G. 687. The abstracts of Defensive Publication applications are identified by distinctly numbered series and are arranged chronologically. The heading of each abstract indicates the number of pages of specification, including claims and sheets of drawings contained in the application as originally filed. The files of these applications are available to the public for inspection and reproduction may be purchased for 30 cents a sheet.
Defensive Publication applications have not been examined as to the merits of alleged invention. The Patent Ofiice makes no assertion as to the novelty of the disclosed subject matter.
PUBLISHED SEPTEMBER 29, 1970 T878,013 CARBODIIMIDE HARDENERS IN INCORPORATED COUPLER EMULSIONS Edwin Nicholai Oftedahl and Mary Katherine DeSeyn, both of Kodak Park Division, Rochester, N.Y. 14650 Filed Feb. 24, 1969, Ser. No. 801,772 Int. Cl. G03c 1/40 US. Cl. 96-100 No Drawing. 10 Pages Specification Photographic silver halide emulsions containing an incorporated pyrazolone magenta dye-forming coupler can be hardened with an incorporated carbodiimide hardener. Photographic elements comprising such emulsions, when exposed and processed, produce prints having low stain and high maximum density. Carbodiimide hardening agents including those described in Sheehan US. Pat. 2,938,892 issued May 31, 1960, Sheehan US. Pat. 3,135,- 748 issued June 2, 1964, and Brunken German Pat. 7218 issued May 10, 1954, can be used. Suitable carbodiimide hardening agents can be represented by the formula where each of R and R is an organic radical such as alkyl, alkoxy, allyl, aryl or heterocyclic groups. Typical examples of suitable carbodiimide hardening agents which are incorporated in the photographic materials described herein are 1,3-dimethylcarbodiimide, 1-methyl-3-methoxymethylcarbodiimide, dicyclohexylcarbodiimide and l-ethyl-3-[3-dirnethylaminopropyl] carbodiimide hydrochloride.
A process for preparing the aforementioned photographic silver halide materials from coating compositions comprising incorporated pyrazolone magenta dye-forming couplers and carbodiimide hardening agents is also disclosed.
The emulsions of the invention can be used in photographic elements in layers containing high-speed chemically sensitized and spectrally sensitized silver halide emulsions, anti-foggants, coating aids, plasticizers, conventional hardeners and the like, such as described in Dunn U.S. Pat. 3,297,446 (columns 4-9).
US878013D 1969-02-24 1969-02-24 Defensive publication Pending UST878013I4 (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US80177269A 1969-02-24 1969-02-24

Publications (1)

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UST878013I4 true UST878013I4 (en) 1970-09-29

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Family Applications (1)

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US878013D Pending UST878013I4 (en) 1969-02-24 1969-02-24 Defensive publication

Country Status (2)

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US (1) UST878013I4 (en)
FR (1) FR2032350A1 (en)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2517408A1 (en) * 1975-04-19 1976-11-04 Agfa Gevaert Ag PROCESS FOR THE PRODUCTION OF COLOR PHOTOGRAPHIC SILVER HOLGENIDE EMULSION LAYERS, PROCESSABLE AT INCREASED TEMPERATURES
DE2539729A1 (en) * 1975-09-06 1977-03-17 Agfa Gevaert Ag COLOR PHOTOGRAPHIC MATERIAL

Also Published As

Publication number Publication date
FR2032350A1 (en) 1970-11-27

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