US906098A - Sterilization of grain by fumigation. - Google Patents
Sterilization of grain by fumigation. Download PDFInfo
- Publication number
- US906098A US906098A US41483408A US1908414834A US906098A US 906098 A US906098 A US 906098A US 41483408 A US41483408 A US 41483408A US 1908414834 A US1908414834 A US 1908414834A US 906098 A US906098 A US 906098A
- Authority
- US
- United States
- Prior art keywords
- grain
- fumigation
- parts
- sterilization
- spores
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000003958 fumigation Methods 0.000 title description 4
- 230000001954 sterilising effect Effects 0.000 title description 4
- 238000004659 sterilization and disinfection Methods 0.000 title description 3
- 235000013339 cereals Nutrition 0.000 description 11
- 238000000034 method Methods 0.000 description 7
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 3
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Inorganic materials [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 3
- 235000010333 potassium nitrate Nutrition 0.000 description 3
- 229910052717 sulfur Inorganic materials 0.000 description 3
- 239000011593 sulfur Substances 0.000 description 3
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- 235000019270 ammonium chloride Nutrition 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 239000003517 fume Substances 0.000 description 2
- GSNBWTFAGXSQCO-UHFFFAOYSA-N fumigatin Chemical compound COC1=C(O)C(=O)C(C)=CC1=O GSNBWTFAGXSQCO-UHFFFAOYSA-N 0.000 description 2
- 230000000266 injurious effect Effects 0.000 description 2
- 230000003071 parasitic effect Effects 0.000 description 2
- 235000007319 Avena orientalis Nutrition 0.000 description 1
- 244000075850 Avena orientalis Species 0.000 description 1
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 241000235319 Havinthus Species 0.000 description 1
- 240000005979 Hordeum vulgare Species 0.000 description 1
- 235000007340 Hordeum vulgare Nutrition 0.000 description 1
- 241000209140 Triticum Species 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 239000013543 active substance Substances 0.000 description 1
- 238000004061 bleaching Methods 0.000 description 1
- 239000003575 carbonaceous material Substances 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- JCYWCSGERIELPG-UHFFFAOYSA-N imes Chemical class CC1=CC(C)=CC(C)=C1N1C=CN(C=2C(=CC(C)=CC=2C)C)[C]1 JCYWCSGERIELPG-UHFFFAOYSA-N 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 125000000449 nitro group Chemical group [O-][N+](*)=O 0.000 description 1
- 230000001717 pathogenic effect Effects 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K33/00—Medicinal preparations containing inorganic active ingredients
- A61K33/24—Heavy metals; Compounds thereof
- A61K33/34—Copper; Compounds thereof
Definitions
- My invention has reference to an improved process of treating grain, more especially wheat, barley and oats, for the purpose of destroying the blight and other parasitic fungi adhering to it.
- the grain is inclosed on all sides, an is there under a temperature of about 60 centigrade subjected -to the action of previously in a suitably manner developed fumes of a powder substantiallyconsisting of 18 parts sulfur, 15 parts saltpeter, 15 parts sal-ammoniac, 15 parts colophony and 15 parts copper vitriol.
- the temperature is only inconsidera ly elevated, the apparatus is not thoroughly closed, and the grains themselves are not heated to any great extent. In my process, on the other hand, it is of the utmost importance that the temperature be sufficiently raised to about 60 centigrade, so as to completely vaporize the less volatile ingredients of the mixture.
- the higher temperature is of essential influence upon the efficiency .of the whole process.
Landscapes
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Description
To all whom it may concern:
JACOB BLOOH, OF BERLIN, GERMANY.
STERILIZATION OF GRAIN BY FUMIGATION.
, Specification of Letters Patent.
Patented Dec. 8, 1908.
Application filed February 7, 1908. Serial No. 414,834.
Be it known that I, JAooB BLOCH, merchant, a subject of the German Emperor, and a resident of Berlin, Germany, have invented certain newand useful Improvements in the Sterilization of Grain by Fumigation, of which the following is a specification.
My invention has reference to an improved process of treating grain, more especially wheat, barley and oats, for the purpose of destroying the blight and other parasitic fungi adhering to it.
According to most prior processes the rain is treated with liquids, more articuarly with a solution ofco per vitrio which is, for instance, spraye over the grain. Such processes, however, possess numerous disadvantages; for the li uid acts very irregularly, many of the individual grains being inadequately acted upon, so that the spores are not completely annihilated. Furt ermore, the after-drying of the treated material is attended with much trouble and expense and the workmen, moreover, are exposed to the injurious action of the vitriol or other solution used. Again, mixtures of sulfur, saltpeter and carbonaceous substances have been burned for the purpose of bleaching the grain, in order to impart to old grain a fresher appearance. There has, however, been no intention here of destroying pathogenic spores, nor could this be accomplished,
since by combination of the said substances the only gaseous products that result are carbon oxid, carbon dioxid and nitro en, 7 e. gases hardly exerting a sterilizing e ect. According to the present invention, on the contrary, the grain is inclosed on all sides, an is there under a temperature of about 60 centigrade subjected -to the action of previously in a suitably manner developed fumes of a powder substantiallyconsisting of 18 parts sulfur, 15 parts saltpeter, 15 parts sal-ammoniac, 15 parts colophony and 15 parts copper vitriol.
necessary in prior apparatuses.
laced in a chamber In this manner the parasitic spores on the grain will be annihilated, without, however, the germinating ower of the grain being injuriously affected In the well-known fumigatin process the temperature is only inconsidera ly elevated, the apparatus is not thoroughly closed, and the grains themselves are not heated to any great extent. In my process, on the other hand, it is of the utmost importance that the temperature be sufficiently raised to about 60 centigrade, so as to completely vaporize the less volatile ingredients of the mixture.
The higher temperature is of essential influence upon the efficiency .of the whole process. The grains sweat and thus the active agent adheres the better; but at the same time the degreeof humidity is not such as would call for special drying after the fumigation. The high temperature in itself, moreover, greatly aids in the annihilation of the spores.
Uniform action is promoted by the walls, joints etc. of the a paratus being made with a closer fit than as been customary or In this manner, too, the esca e from the apparatus of fumes injurious to t e health of the workmen is prevented, even after long use-of the contrivance.
. Havin thus described my invention, I declare t at what I claim as new is The process of fumigating rain, consisting in submitting the latter to f imes generated from a mixture containing substantially 18 parts sulfur, 15 parts saltpeter, '15 parts colophony, 15 parts sal-ammoniac and 15 parts JACOB BLOCH.
Witnesses:
. HENRY HASPER,
WOLDEMAR HAUcrr.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US41483408A US906098A (en) | 1908-02-07 | 1908-02-07 | Sterilization of grain by fumigation. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US41483408A US906098A (en) | 1908-02-07 | 1908-02-07 | Sterilization of grain by fumigation. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US906098A true US906098A (en) | 1908-12-08 |
Family
ID=2974533
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US41483408A Expired - Lifetime US906098A (en) | 1908-02-07 | 1908-02-07 | Sterilization of grain by fumigation. |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US906098A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2948585A (en) * | 1960-08-09 | Substances to seeds |
-
1908
- 1908-02-07 US US41483408A patent/US906098A/en not_active Expired - Lifetime
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2948585A (en) * | 1960-08-09 | Substances to seeds |
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