US822398A - Apparatus for treatment of ores and tailings. - Google Patents
Apparatus for treatment of ores and tailings. Download PDFInfo
- Publication number
- US822398A US822398A US26945905A US1905269459A US822398A US 822398 A US822398 A US 822398A US 26945905 A US26945905 A US 26945905A US 1905269459 A US1905269459 A US 1905269459A US 822398 A US822398 A US 822398A
- Authority
- US
- United States
- Prior art keywords
- tailings
- slimes
- trough
- treatment
- reservoirs
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000011282 treatment Methods 0.000 title description 15
- 239000002253 acid Substances 0.000 description 12
- 239000000203 mixture Substances 0.000 description 10
- 150000003839 salts Chemical class 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
- 238000013019 agitation Methods 0.000 description 6
- 239000004020 conductor Substances 0.000 description 5
- 238000000034 method Methods 0.000 description 5
- 239000010953 base metal Substances 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 3
- 229910052802 copper Inorganic materials 0.000 description 3
- 239000010949 copper Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 229910000497 Amalgam Inorganic materials 0.000 description 2
- 230000005484 gravity Effects 0.000 description 2
- 238000002386 leaching Methods 0.000 description 2
- 239000010970 precious metal Substances 0.000 description 2
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- 241000722270 Regulus Species 0.000 description 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 235000011054 acetic acid Nutrition 0.000 description 1
- 229910001919 chlorite Inorganic materials 0.000 description 1
- 229910052619 chlorite group Inorganic materials 0.000 description 1
- QBWCMBCROVPCKQ-UHFFFAOYSA-N chlorous acid Chemical compound OCl=O QBWCMBCROVPCKQ-UHFFFAOYSA-N 0.000 description 1
- ZCDOYSPFYFSLEW-UHFFFAOYSA-N chromate(2-) Chemical compound [O-][Cr]([O-])(=O)=O ZCDOYSPFYFSLEW-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- PCHJSUWPFVWCPO-UHFFFAOYSA-N gold Chemical compound [Au] PCHJSUWPFVWCPO-UHFFFAOYSA-N 0.000 description 1
- 229910052737 gold Inorganic materials 0.000 description 1
- 239000010931 gold Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011872 intimate mixture Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- 235000006408 oxalic acid Nutrition 0.000 description 1
- NNFCIKHAZHQZJG-UHFFFAOYSA-N potassium cyanide Chemical compound [K+].N#[C-] NNFCIKHAZHQZJG-UHFFFAOYSA-N 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000010408 sweeping Methods 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
- 239000011975 tartaric acid Substances 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 239000011701 zinc Substances 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/14—Agglomerating; Briquetting; Binding; Granulating
- C22B1/16—Sintering; Agglomerating
- C22B1/20—Sintering; Agglomerating in sintering machines with movable grates
Definitions
- Figure 1 is a section on the line 1 1, Fig. 2.
- Fig. 2 is a plan view, partly diagrammatic and partly broken away, of my apparatus.
- Fig. 3 is a view, on a larger scale, of a section of the apparatus.
- Figs. 4 and 5 are detail perspective views of the sluice trough and its riffles.
- the invention relates to the treatment of tailings or slimes of the precious metals in connection with the cyaniding process; and it consists in certain improvements upon the invention described in Letters Patent No. 636,114, dated October 3]., 1899, as hereinafter set forth.
- tailings are very slimy or contain copper or other base metals in various combinations which it is desirable to remove a weak solution of nitric, sulfuric, hydrochloric, or other mineral acid
- a weak solution of nitric, sulfuric, hydrochloric, or other mineral acid may be employed, as described in the Letters Patent referred to, or Weak solution of certain salts, such as potassic chromate or any nitrate or chlorite or crude salts from alkaline plains, which would act as solvents in the separation of the base metals referred to; or dilute solutions of organic acids, particularly oxalic acid, tartaric acid, or acetic acid, or of their salts, may be used to act as solvents for the rebellious slimes or slimy tailings which otherwise would prove refractory in the subsequent cyaniding process.
- the letter M indicates the pile. of tailings to be reduced.
- a ledge trough T Around the base of the pile is constructed a ledge trough T, the inner edge of which is in contact with. the pile and the outer portion of which is walled and communicates with a trough U, leading to a set of crushing or pulverizing rolls R.
- a stream of water conveyed through'a pipe C or otherwise is caused to play upon the pile of tailings, which are thereby washed down into the circumscribing trough T and through the trough U to the crushing-rolls, whereby the tailings are pulverized and discharged into the inclined.
- sluice-trough B which is designed to extend for a long distance, according to the character of the work. This distance may vary from a fraction of a mile to several miles.
- This trough is provided with a riflie-bottom (L and is designed. to ef fect an agitation by gravity of the mixture flowing along its bottom.
- a tank D which contains a solution of acid or of acid salts, as hereinbefore mentioned.
- a pipe I) conveys the weak acid solution to the head of the trough B, where it enters the. mixture of particles of tailings and water from the crushing-rolls and is conveyed with such mixture, with. which it becomes intimately mixed, to the settling-reservoirs at the lower level.
- the pipe I) is provided with a valve 0 to regulate the flow of the acid solution.
- a water-supply pipe (Z which conveys water to the mixture in the trough.
- the sluice-trough B is preferably made V form in cross-section and is designed to be without joint or crevice between its walls. To that end the sections are cut entire from a log in such wise that several sections can be cut from the same log. In the sections are placed the movable angular bottom pieces at, having a stepped or riffle surface e.
- each step of the riffle-surface is designed to be usually about eighteen inches and the rise from step to step about two inches, more or less.
- the sluice-trough B may be caused to branch at points where the diluting -water pipes discharge in order to carry the mixture easily. These troughs finally discharge into the first reservoir or reservoirs E, which are designed for the purpose of settling the sands or particles of the tailings from the slimes or lighter mixture which is conveyed over by the overflow troughs or pipes f to the settling reservoir or reservoirs for such slimes, (indicated at F.)
- tors f into a tank or reservoir M, in which the last traces of the slimes are settled from the base liquids, which are decanted and run through a series of wooden troughs K, containing iron-scraps, on whi oh the metallic copper will be deposited and saved as a precipitate, and other chemical compounds of value may also be saved by proper appliances.
- the sands and slimes settled in reservoirs E and F are sluiced by the hydraulic stream through the bottom conductors or sluices G into final reservoirs H, wherein the preliminary treatment is concluded, and the sands and slimes are dried and cultivated and made ready for cyanid treatment.
- the tailings and slimes are first pulverized and thoroughly mixed by rolls, then mixed with a solution of acids or acid salts in proper amount to rovide for solution of the base contents of t e same, then agitating the mixture by running it through sluices or conductors for a considerable distance into settling-reservoirs and freeing the same from base solutions, whereby they are left in condition to be successfully treated by the cyanid process. and slimes can thus be treated and prepared in an economical manner on an extended scale, so that gold and silver can be extracted by the cyanid process cheaply and effectively.
- the preliminary treatment described is designed to be effected at about one-eighth or one-tenth the cost of a preliminary treatment in a closed plant.
- the sands and slimes be ing settled for the main part in separate reservoirs facilitate special separate cyanid treatments, especially for the slimes.
- the extraction of the precious metals by subsequent cyaniding is designed to reach a higher percentage than heretofore practicable.
- the rifi'les in the sluicing-troughs being removable they can be easily and conveniently cleaned of amalgam by lifting them out of the troughs and sweeping such amalgam material into uicksilver-troughs placed at intervals along t e line of troughs.
- the zinc slime resulting from cyaniding is designed to yield about half the cost of consumption of potassium cyanid per ton of tailings worked in mercury by retortingthe same before melting into reguluses and bullion bars.
- Apparatus for preliminary treatment of tailings and slimes consisting of an inclined rifiied troughor conductor having at its upper end a water-supply, and pulverizingrolls, and a tank holding a weak solution of solvent acids or acid salts, a dilution-water conductor near the lower end of said trough, and at its lower end settling-reservoirs for sands and for slimes,final reservoirs for basemetal solutions and separate terminal reservoirs for the sands and for the slimes, substantially as specified.
- Apparatus for the treatment of tailings and slimes preliminary to cyaniding consisting of an inclined riffie-bottom trough or conductor, at the upper end thereof a water-supply, pulverizing-rolls and a tank for a weak solution of solvent acids or acid salts, at the lower end thereof settling-reservoirs for sands and slimes, and an intermediate water-discharge near the settling-reservoirs, substantially as specified.
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
Description
PATENTED JUNE 5, 1906.
A. SODERLING. APPARATUS FOR TREATMENT OF ORES AND TAILINGS.
APPLICATION FILED JULY13.l905
3 SHEETS-SHEET 1.
i alto'ompq .mnREw n nmww co. PKOYO-LITHQGVIAFMERS.AWSHYNGYON. u x
PATENTEDJUNE 5, 1906.
A. SODERLING. APPARATUS FOR TREATMENT OF ORES AND TAILINGS.
APPLICATION FILED JULY 13.19054 3 SHEETS-SHEET 2 No. 822,398. PATENTED JUNE 5, 1906. A. SODERLING.
APPARATUS FOR TREATMENT OF ORES AND TAILINGS.
APPLICATION FILED JULY 13. 1905.
3 SHEETS-SHEET 3.
' 3140M: WWW a w fdmfla ay 1 @Jw/n. 00
-Bodie, in the county of Mono and State of AUGUST SODERLING, OF BODIE, CALIFORNIA.
APPARATUS FOR TREATMENT OF ORES AND TAILINGS.
Specification of Letters Patent.
Patented June 5, 1906.
Application tiled July 18,1905. Serial No: 269.459.
To all whom, it may concern,-
Be it known that I, AUGUST 'SODERLING, a citlzen of the United States, and a resident of California, have made a certain new and useful Invention in the Treatment of Ores and Tailings; and. I declare the following to be a full, clear, and exact description of the same, such as will enable others skilled in the art to which it appertains to make and use the invention, reference being had to the accompanying drawings, and to letters of reference marked thereon, which form a part of this specification.
Figure 1 is a section on the line 1 1, Fig. 2. Fig. 2 is a plan view, partly diagrammatic and partly broken away, of my apparatus. Fig. 3 is a view, on a larger scale, of a section of the apparatus. Figs. 4 and 5 are detail perspective views of the sluice trough and its riffles.
The invention relates to the treatment of tailings or slimes of the precious metals in connection with the cyaniding process; and it consists in certain improvements upon the invention described in Letters Patent No. 636,114, dated October 3]., 1899, as hereinafter set forth.
In cases where tailings are very slimy or contain copper or other base metals in various combinations which it is desirable to remove a weak solution of nitric, sulfuric, hydrochloric, or other mineral acid may be employed, as described in the Letters Patent referred to, or Weak solution of certain salts, such as potassic chromate or any nitrate or chlorite or crude salts from alkaline plains, which would act as solvents in the separation of the base metals referred to; or dilute solutions of organic acids, particularly oxalic acid, tartaric acid, or acetic acid, or of their salts, may be used to act as solvents for the rebellious slimes or slimy tailings which otherwise would prove refractory in the subsequent cyaniding process. In this leaching process in order to effect an intimate mixture of the particles of the tailings and the chemical solution necessary to proper economic results agitation of the mixture is required, which is provided for by means of steps or rifiles in the bottom of the trough or conveyer whereby the mixture is conducted to the settling-reservoirs. The agitation occasioned by the falling of the mixture from one step or riflie of the trough to another during a course of a mile or several miles has been found sufficient for the purpose when the riffles or steps are each about eighteen inches in length. This plan of agitation by gravity is particularly adapted to this preliminary treatment because of its economic character. After agitation with the dilute solution and before cyaniding an alkaline wash or leaching may be used when required.
In the accompanying drawings, illustrating a plant for carrying out this preliminary treatment upon a large scale, the letter M indicates the pile. of tailings to be reduced. Around the base of the pile is constructed a ledge trough T, the inner edge of which is in contact with. the pile and the outer portion of which is walled and communicates with a trough U, leading to a set of crushing or pulverizing rolls R.
A stream of water conveyed through'a pipe C or otherwise is caused to play upon the pile of tailings, which are thereby washed down into the circumscribing trough T and through the trough U to the crushing-rolls, whereby the tailings are pulverized and discharged into the inclined. sluice-trough B, which is designed to extend for a long distance, according to the character of the work. This distance may vary from a fraction of a mile to several miles. This trough is provided with a riflie-bottom (L and is designed. to ef fect an agitation by gravity of the mixture flowing along its bottom.
At the upper level, where the pile of tailings is located and near the crushing-rolls, is placed a tank D, which contains a solution of acid or of acid salts, as hereinbefore mentioned. From this tank a pipe I) conveys the weak acid solution to the head of the trough B, where it enters the. mixture of particles of tailings and water from the crushing-rolls and is conveyed with such mixture, with. which it becomes intimately mixed, to the settling-reservoirs at the lower level. The pipe I) is provided with a valve 0 to regulate the flow of the acid solution. In order still further to dilute this solution, near the end of the sluice-trough or at a point of branching there is provided a water-supply pipe (Z, which conveys water to the mixture in the trough.
The sluice-trough B is preferably made V form in cross-section and is designed to be without joint or crevice between its walls. To that end the sections are cut entire from a log in such wise that several sections can be cut from the same log. In the sections are placed the movable angular bottom pieces at, having a stepped or riffle surface e. The
length of each step of the riffle-surface is designed to be usually about eighteen inches and the rise from step to step about two inches, more or less.
The sluice-trough B may be caused to branch at points where the diluting -water pipes discharge in order to carry the mixture easily. These troughs finally discharge into the first reservoir or reservoirs E, which are designed for the purpose of settling the sands or particles of the tailings from the slimes or lighter mixture which is conveyed over by the overflow troughs or pipes f to the settling reservoir or reservoirs for such slimes, (indicated at F.)
All the water, acid slimes, tailings, and other matter brought down by the sluicetrough are collected in the reservoirs E and F, where the copper and other base-metal salts dissolved in the water being by this time, throu h the agitation eifected in the sluicetroug s, fully separated and in solution are decanted off through the overflow-conduc-.
tors f into a tank or reservoir M, in which the last traces of the slimes are settled from the base liquids, which are decanted and run through a series of wooden troughs K, containing iron-scraps, on whi oh the metallic copper will be deposited and saved as a precipitate, and other chemical compounds of value may also be saved by proper appliances.
The sands and slimes settled in reservoirs E and F are sluiced by the hydraulic stream through the bottom conductors or sluices G into final reservoirs H, wherein the preliminary treatment is concluded, and the sands and slimes are dried and cultivated and made ready for cyanid treatment. In this manner it Will be seen that the tailings and slimes are first pulverized and thoroughly mixed by rolls, then mixed with a solution of acids or acid salts in proper amount to rovide for solution of the base contents of t e same, then agitating the mixture by running it through sluices or conductors for a considerable distance into settling-reservoirs and freeing the same from base solutions, whereby they are left in condition to be successfully treated by the cyanid process. and slimes can thus be treated and prepared in an economical manner on an extended scale, so that gold and silver can be extracted by the cyanid process cheaply and effectively.
Large bodies of tailings The preliminary treatment described is designed to be effected at about one-eighth or one-tenth the cost of a preliminary treatment in a closed plant. The sands and slimes be ing settled for the main part in separate reservoirs facilitate special separate cyanid treatments, especially for the slimes. As the slimes and tailings are thoroughly oxidized in the preliminary treatment, the extraction of the precious metals by subsequent cyaniding is designed to reach a higher percentage than heretofore practicable. The rifi'les in the sluicing-troughs being removable they can be easily and conveniently cleaned of amalgam by lifting them out of the troughs and sweeping such amalgam material into uicksilver-troughs placed at intervals along t e line of troughs. Through this preliminary treatment the zinc slime resulting from cyaniding is designed to yield about half the cost of consumption of potassium cyanid per ton of tailings worked in mercury by retortingthe same before melting into reguluses and bullion bars.
Having described my invention, what I claim, and desire to secure by Letters Patent, 1s-
1. Apparatus for preliminary treatment of tailings and slimes, consisting of an inclined rifiied troughor conductor having at its upper end a water-supply, and pulverizingrolls, and a tank holding a weak solution of solvent acids or acid salts, a dilution-water conductor near the lower end of said trough, and at its lower end settling-reservoirs for sands and for slimes,final reservoirs for basemetal solutions and separate terminal reservoirs for the sands and for the slimes, substantially as specified.
2. Apparatus for the treatment of tailings and slimes preliminary to cyaniding consisting of an inclined riffie-bottom trough or conductor, at the upper end thereof a water-supply, pulverizing-rolls and a tank for a weak solution of solvent acids or acid salts, at the lower end thereof settling-reservoirs for sands and slimes, and an intermediate water-discharge near the settling-reservoirs, substantially as specified.
In testimony whereof I affix my signature in presence of two witnesses.
AUGUST SODERLING. Witnesses N. H. GREGORY, M. Y. S. KIRKWOOD.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US26945905A US822398A (en) | 1905-07-13 | 1905-07-13 | Apparatus for treatment of ores and tailings. |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US26945905A US822398A (en) | 1905-07-13 | 1905-07-13 | Apparatus for treatment of ores and tailings. |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US822398A true US822398A (en) | 1906-06-05 |
Family
ID=2890877
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US26945905A Expired - Lifetime US822398A (en) | 1905-07-13 | 1905-07-13 | Apparatus for treatment of ores and tailings. |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US822398A (en) |
-
1905
- 1905-07-13 US US26945905A patent/US822398A/en not_active Expired - Lifetime
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