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US3751011A - Mixing of particulate and fibrous materials - Google Patents

Mixing of particulate and fibrous materials Download PDF

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US3751011A
US3751011A US00220421A US3751011DA US3751011A US 3751011 A US3751011 A US 3751011A US 00220421 A US00220421 A US 00220421A US 3751011D A US3751011D A US 3751011DA US 3751011 A US3751011 A US 3751011A
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materials
dish
mixing
wall surface
fibrous
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R Milik
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/93Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with rotary discs
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/80Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
    • B01F27/808Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with stirrers driven from the bottom of the receptacle
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F29/00Mixers with rotating receptacles
    • B01F29/80Mixers with rotating receptacles rotating about a substantially vertical axis
    • B01F29/82Mixers with rotating receptacles rotating about a substantially vertical axis the receptacle comprising a rotary part, e.g. the bottom, and a stationary part, e.g. the wall, with optional use of a stirrer; the receptacle comprising parts moving in opposite directions
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01FMIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05Stirrers
    • B01F27/11Stirrers characterised by the configuration of the stirrers
    • B01F27/115Stirrers characterised by the configuration of the stirrers comprising discs or disc-like elements essentially perpendicular to the stirrer shaft axis
    • B01F27/1154Stirrers characterised by the configuration of the stirrers comprising discs or disc-like elements essentially perpendicular to the stirrer shaft axis the discs being cup shaped, e.g. semi sphere

Definitions

  • two or more materials are mixed together by supplying the materials to an apparatus comprising a rotary dished platform, which is rotated about a vertical central axis, and a wall which closely surrounds and extends upwards from the rim of the platform, butwhich does not partake of the rotation of the platform, and then rotating the platform with the materials upon it.
  • the surrounding wall is held stationary although it may as an alternative rotate in the same direction as, butmuch more slowly than, the platform or it may rotate counter to the platform.
  • the form of appartus comprising a rotary dished platform and a surrounding stationarywall is known, but it has in the past only been used for grinding powdered material or for surface finishing metal workpieces which are held in a holder above the platform and have grinding chips circulated over them by rotating the platform.
  • FIG. 1 is an axial sectional view through one specific device suitable for use in carrying out the invention.
  • the apparatus adapted for mixing purposes preferably includes, in addition to the rotary platform 3 and the surrounding wall 5, conveyors 35 or other means for supplying the materials to be mixed together to the platform and means for discharging the materials after they have been mixed together.
  • conveyors 35 or other means for supplying the materials to be mixed together to the platform and means for discharging the materials after they have been mixed together Such an apparatus is described and claimed in our copending Application Ser. No. 216,054, filed Jan. 7, 1972.
  • the two or more fibrous materials canbe very uniformly mixed together of a fibrous material can be evenly distributed in other materials and there is no tendency at all for the fibrous material to coagulate into balls or lumps.
  • Examples of the mixing of fibrous materials with other materials are the mixing of glass fibre staple with powdered plastics materials; the mixing of glass fibre staple in concrete mixes; the mixing of asbestosfibre in cement slurry and the mixing of steel wire staple in con.- crete mixes.
  • the method in accordance with the invention has still greater advantages when material with which the ti brous material or materials are to be mixed is of a brittle nature.
  • lfa bladed mixer is used, there is a tendency for the brittle constituent of the mixture to be broken up into smaller particles. This is often not desirable.
  • a concrete mix containing glass or other fibre may also contain a brittle aggregate such. as a lightweight expanded clay aggregate and the grading of the grain sizes of the aggregate is important to produce a satisfactory mix. It is important therefore once the brittle expanded clay aggregate has been graded that its particles should not be shattered to reduce the grain size during mixing.
  • EXAMPLE I EXAMPLE u Granules or beads of polyethylene to be mixed with asbestos fibres in proportions by weight of percent and 20 percent respectively were supplied to the platform of the machine and were mixed for 5 seconds.
  • asbestos fibres were found to be uniformly distributed throughout the beads of polyethylene.
  • EXAMPLE IV As a first step in the production of synthetic wood chip board, fibrous wood chips and liquid resin bonding agent with a hardener added were supplied to the platform in amounts of 90 percent and 10 percent by weight and were mixed together for 5 seconds. The fibrous wood chips were found to be uniformly coated and impregnated with the resin ready for moulding into the board.
  • EXAMPLE VI Fibrous wood pulp and liquid resin in proportions of 95 percent and 5 percent by weight respectively was supplied to the platform and were mixed together as a preliminary step in the production of paper or cardboard.
  • EXAMPLE VII Vegetable fibres together with other vegetable residues were supplied together with a small proportion of powdered vitamin material were supplied to the platform and were mixed together for up to l seconds. It was found that the vitamin material was evenly distributed throughout the vegetable matter to form a step in the production of cattle food.
  • EXAMPLE VIII A technique for reinforcing concrete by the mixing into the concrete of steel wire staple having a length of about 1 inch has recently been developed, but extreme difficulties have been encountered in the preparation of the mix. For a satisafactory product, it is essential that the steel wire staple should be uniformly distributed throughout the mix, but in practice with known concrete mixers of either the drum or the pan type, the
  • EXAMPLE X Cement, water and glass fibre having a fibre length of approximately lr inches were supplied to the platform in proportions of 2; l; 4 by weight and were mixed together for a period of 8 seconds.
  • the resultant fibrous slurry was found to be extremely homogeneous and useful for. forming fibre reinforced sheeting or other products somewhat similar to those made from asbestos cement.
  • EXAMPLE XI Cement, perlite granules, water, and glass fibre having a fibre length of approximately 1% inches were supplied to the platform in proportions of l; 2; l; 2 by weight and were mixed for approximately 8 seconds. After hardening and the curing, the resultant product had a much lower density than normal concrete containing stone aggregate, but an appreciably higher tensile strength.
  • EXAMPLE XII The ingredients of a conventional concrete mix consisting of cement, sand and coarse aggregate in proportions by weight of 1; 2; 4; together with water to give a water/cement ratio of approximately 0.25 and in addition 5 percent by weight of the total mix of polypropylene filament staple were supplied to the platform and were mixed for 10 seconds. After hardening and curing, the resultant concrete had a compressive strength substantially the same as that for an equivalent mix without the polypropylene, but a substantially greater tensile strength.
  • a method of mixing together at least two materials, at least one of which is fibrous comprising the steps of supplying said materials to a circular dish-shaped surface, which is substantially free of projections and has its edge surrounded by a wall surface extending upwardly from said edge, and rotating said dish-shaped surface about a vertical central axis and thereby imparting a rotation to said materials and flinging said materials centrifugally outwards and upwards against said wall surface, contact with said wall surface retarding the rotation of said materials and directing said materials inwards towards said axis whence they fall downwards again onto said dish-shaped surface, whereby said materials form a toroidally shaped mass around said dish-shaped surface and said materials circulate along a helical path around said toroidally shaped mass.
  • a method as claimed in claiml further comprising-the step of holding said wall surface stationary.

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Preparation Of Clay, And Manufacture Of Mixtures Containing Clay Or Cement (AREA)

Abstract

Two or more materials, at least one of which is fibrous are mixed together by supplying the materials onto a dish-shaped circular surface which is free of projections, closely surrounding the edge of the circular surface with a wall which extends upwards from the surface and rotating the surface with the materials upon it and thus flinging the materials outwards centrifugally and causing them by the dished shape of the surface to be deflected upwards over the face of the wall which slows down the rotation applied to the materials by the rotating surface and directs the materials inwards again towards the centre of the surface whence they are flung centrifugally outwards so that the materials form a toroidally shaped mass around the edge of the surface and the materials circulate around the toroid following a helical path.

Description

United States Patent 1191 Milik Aug. 7, 1973 MIXING ()F PARTICULATE AND FIBROUS l l Primary ExaminerRObcrt W. Jenkins MATERIALS Attorney-Joseph F. Brisebois et a1.
75 Inventor: Rudolf F. L. Milik, Welw n Garden I 1 City England y 57 ABSTRACT I Two or more materials, at least one of which is fibrous [73] Ass1gnee: Design Link, Hertfordshire, England are mixed together by supplying the materials onto a 221 i d; Jam 24 1972 dish-shaped circular surface which is free of projections, closely surrounding the edge of the circular sur [2]] Appl' 220,421 face with a wall which extends upwards from the surface and rotating the surface with the materials upon it 521 US. (:1. 259/146, 259/8 and thus flinging the materials outwards eenhifugally 51 Int. Cl. B28c 5/06 and Causing them y the dished Shape Of the surface to [58] Field of Search 259/145, 146, 148, be deflected upwards Over the face Of the well which 25 3 5 7 2, 1 14 slows down the rotation applied to the materials by the rotating surface and directs the materials inwards again 5 References Cited towards the centre of the surface whence they are flung UNITED STATES PATENTS centrifugally outwards so that the materials form a tol 758 200 5/1930 Pf ff 259/148 roidally shaped mass around the edge of the surface e er and the materials circulate around the toroid following 2,843,080 7/l958 Woodruff .1 259/3 r 3,163,402 12/1964 Yamashita 259/3 3 helm Path 5 Claims, 1 Drawing Figure O l 1. 1-1 ?7 Q8 30 u I X l l l 55 A 29 z I i i I 5 j F *5 l 5 i i t IE 3/ 2/ A I a i /0 MIXING OF PARTICULATE AND FIBROUS MATERIALS The mixing together of different fibrous materials or the mixing of fibrous materials with other materials such as powders, granulates and liquids has in the past caused very great difficulties because conventional mixers employing rotating blades tend to catch the fibres on the edges of the blades and separate them from the mix thus causing segregation of the fibres from the other constituents of the mixture if any and they also tend to cause inter-twining or balling of the fibres into coagulated lumps. Thus with all conventional forms of mixer it has been found that a homogeneous mixture of two or more fibrous materials or a homogeneous dispersion of fribrous material in other materials is impossible to achieve.
It has now been discovered that by using a form of apparatus which has not previously been used for mixing purposes, two or more different fibrous materials or a fibrous material together with other materials can be mixed together extremely rapidly and efficiently and also in an extremelyuniform manner.
Thus, according to the present invention, two or more materials, at least one of which is fibrous are mixed together by supplying the materials to an apparatus comprising a rotary dished platform, which is rotated about a vertical central axis, and a wall which closely surrounds and extends upwards from the rim of the platform, butwhich does not partake of the rotation of the platform, and then rotating the platform with the materials upon it.
Preferably the surrounding wall is held stationary although it may as an alternative rotate in the same direction as, butmuch more slowly than, the platform or it may rotate counter to the platform.
With this arrangement the materials to be mixed together are flung outwards centrifugally and owing to the dished shaped of the platform, the materials are forced upwards against the surrounding wall. The contact of the materials with the wall tends to slow down their rotation and to direct the materials inwards again towards the centre of the platform where the materials fall downwards onto the platform andare then flung outwards once again. The result is that the materials tend to form a toroidally shaped mass around the edge of the platform and the materials circulate around the toroid following a helical path. The movement of the materials around this path is of an extremely complex nature and the speed of particle movement of the vari ous materials varies so much that extremely rapid mixing together of the materials results giving rise to a uniform mixture in a matter of only a few seconds.
The form of appartus comprising a rotary dished platform and a surrounding stationarywall is known, but it has in the past only been used for grinding powdered material or for surface finishing metal workpieces which are held in a holder above the platform and have grinding chips circulated over them by rotating the platform.
One embodiment of suitable apparatus is illustrated in the accompanying drawing, in which:
FIG. 1 is an axial sectional view through one specific device suitable for use in carrying out the invention.
The apparatus adapted for mixing purposes preferably includes, in addition to the rotary platform 3 and the surrounding wall 5, conveyors 35 or other means for supplying the materials to be mixed together to the platform and means for discharging the materials after they have been mixed together. Such an apparatus is described and claimed in our copending Application Ser. No. 216,054, filed Jan. 7, 1972.
Using the method in accordance with the present invention, the two or more fibrous materials canbe very uniformly mixed together of a fibrous material can be evenly distributed in other materials and there is no tendency at all for the fibrous material to coagulate into balls or lumps.
We have found that the speed of rotation of the dished platform may vary over quite wide limits, but preferably the speed of rotation is such that the peripheral speed of the platform is about 400 ft. per minute. This corresponds to an angular speed of about 60 revolutions per minute with a platform having a diameter of 2 ft.
Examples of the mixing of fibrous materials with other materials are the mixing of glass fibre staple with powdered plastics materials; the mixing of glass fibre staple in concrete mixes; the mixing of asbestosfibre in cement slurry and the mixing of steel wire staple in con.- crete mixes. a
The method in accordance with the invention has still greater advantages when material with which the ti brous material or materials are to be mixed is of a brittle nature. lfa bladed mixer is used, there is a tendency for the brittle constituent of the mixture to be broken up into smaller particles. This is often not desirable. For example, a concrete mix containing glass or other fibre may also contain a brittle aggregate such. as a lightweight expanded clay aggregate and the grading of the grain sizes of the aggregate is important to produce a satisfactory mix. It is important therefore once the brittle expanded clay aggregate has been graded that its particles should not be shattered to reduce the grain size during mixing.
Some examples of methods of mixing in accordance with the invention using any one of the pieces of apparatus described and illustrated in our co'pending Application Ser. No. 216,054, filed Jan. 7!, 1972, with a platform diameter of 2 ft. and a speed of rotation of 60 revolutions per minute for a time of only a few seconds are as follows:
EXAMPLE I EXAMPLE u Granules or beads of polyethylene to be mixed with asbestos fibres in proportions by weight of percent and 20 percent respectively were supplied to the platform of the machine and were mixed for 5 seconds. The
asbestos fibres were found to be uniformly distributed throughout the beads of polyethylene.
EXAMPLE III Example II was repeated, but using beads of polystyrene in place of the polyethylene. The same result was achieved.
EXAMPLE IV EXAMPLE V As a first step in the production of synthetic wood chip board, fibrous wood chips and liquid resin bonding agent with a hardener added were supplied to the platform in amounts of 90 percent and 10 percent by weight and were mixed together for 5 seconds. The fibrous wood chips were found to be uniformly coated and impregnated with the resin ready for moulding into the board.
EXAMPLE VI Fibrous wood pulp and liquid resin in proportions of 95 percent and 5 percent by weight respectively was supplied to the platform and were mixed together as a preliminary step in the production of paper or cardboard.
EXAMPLE VII Vegetable fibres together with other vegetable residues were supplied together with a small proportion of powdered vitamin material were supplied to the platform and were mixed together for up to l seconds. It was found that the vitamin material was evenly distributed throughout the vegetable matter to form a step in the production of cattle food.
EXAMPLE VIII A technique for reinforcing concrete by the mixing into the concrete of steel wire staple having a length of about 1 inch has recently been developed, but extreme difficulties have been encountered in the preparation of the mix. For a satisafactory product, it is essential that the steel wire staple should be uniformly distributed throughout the mix, but in practice with known concrete mixers of either the drum or the pan type, the
EXAMPLE IX Sand, stone aggregate, cement, water and glass fibre in proportions by weight of: 2; 4; 2; l; 2, respectively were supplied to the platform and were mixed for 8 seconds. The resultant concrete mix was extremely homogeneous and was found to have the glass fibre uniformly distributed throughout.
EXAMPLE X Cement, water and glass fibre having a fibre length of approximately lr inches were supplied to the platform in proportions of 2; l; 4 by weight and were mixed together for a period of 8 seconds. The resultant fibrous slurry was found to be extremely homogeneous and useful for. forming fibre reinforced sheeting or other products somewhat similar to those made from asbestos cement.
EXAMPLE XI Cement, perlite granules, water, and glass fibre having a fibre length of approximately 1% inches were supplied to the platform in proportions of l; 2; l; 2 by weight and were mixed for approximately 8 seconds. After hardening and the curing, the resultant product had a much lower density than normal concrete containing stone aggregate, but an appreciably higher tensile strength.
EXAMPLE XII The ingredients of a conventional concrete mix consisting of cement, sand and coarse aggregate in proportions by weight of 1; 2; 4; together with water to give a water/cement ratio of approximately 0.25 and in addition 5 percent by weight of the total mix of polypropylene filament staple were supplied to the platform and were mixed for 10 seconds. After hardening and curing, the resultant concrete had a compressive strength substantially the same as that for an equivalent mix without the polypropylene, but a substantially greater tensile strength.
I claim:
1. A method of mixing together at least two materials, at least one of which is fibrous, said method comprising the steps of supplying said materials to a circular dish-shaped surface, which is substantially free of projections and has its edge surrounded by a wall surface extending upwardly from said edge, and rotating said dish-shaped surface about a vertical central axis and thereby imparting a rotation to said materials and flinging said materials centrifugally outwards and upwards against said wall surface, contact with said wall surface retarding the rotation of said materials and directing said materials inwards towards said axis whence they fall downwards again onto said dish-shaped surface, whereby said materials form a toroidally shaped mass around said dish-shaped surface and said materials circulate along a helical path around said toroidally shaped mass.
2. A method as claimed in claiml, further comprising-the step of holding said wall surface stationary.
3. A method as claimed in claim 1, wherein said materials include glass fibre staple and powdered plastics material.
4. A method as claimed in claim 1, in which said materials include cement, granular aggregate, water and steel wire staple which, after mixing, form concrete.
5. A method as claimed in claim 4, in which said aggregate includes expanded clay or other brittle material.
' K t k k

Claims (5)

1. A method of mixing together at least two materials, at least one of which is fibrous, said method comprising the steps of supplying said materials to a circular dish-shaped surface, which is substantially free of projections and has its edge surrounded by a wall surface extending upwardly from said edge, and rotating said dish-shaped surface about a vertical central axis and thereby imparting a rotation to said materials and flinging said materials centrifugally outwards and upwards against said wall surface, contact with said wall surface retarding the rotation of said materials and directing said materials inwards towards said axis whence they fall downwards again onto said dish-shaped surface, whereby said materials form a toroidally shaped mass around said dish-shaped surface and said materials circulate along a helical path around said toroidally shaped mass.
2. A method as claimed in claim 1, further comprising the step of holding said wall surface stationary.
3. A method as claimed in claim 1, wherein said materials include glass fibre staple and powdered plastics material.
4. A method as claimed in claim 1, in which said materials include cement, granular aggregate, water and steel wire staple which, after mixing, form concrete.
5. A method as claimed in claim 4, in which said aggregate includes expanded clay or other brittle material.
US00220421A 1972-01-24 1972-01-24 Mixing of particulate and fibrous materials Expired - Lifetime US3751011A (en)

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3863904A (en) * 1972-01-18 1975-02-04 Design Link Mixing of fragile granular materials
US4092737A (en) * 1975-08-11 1978-05-30 Bertil Sandell Method for preparing fibers for mixing into a sprayed concrete mass and a device for performing the method
EP0101255A3 (en) * 1982-08-05 1984-07-25 Croker Limited Improvements in mixing machines
US6641296B1 (en) * 1997-04-24 2003-11-04 Jean-Luc Jouvin Method for mixing alginate using a rotatable elliptical bowl
US20130058186A1 (en) * 2010-03-10 2013-03-07 Wetend Technologies Oy Method and apparatus for mixing various flows into a process liquid flow
CN102985475A (en) * 2010-07-02 2013-03-20 那甘提普·普瓦鲁多姆 Homogeneous biodegradable mixture for shaped bodies and method for its preparation

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1758200A (en) * 1926-03-19 1930-05-13 United States Gypsum Co Wet mixing method and apparatus
US2843080A (en) * 1955-08-02 1958-07-15 Gen Foods Corp Popcorn flavoring apparatus
US3163402A (en) * 1958-03-31 1964-12-29 Yamashita Hachiro Apparatus for substantially instantly mixing and kneading various materials

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1758200A (en) * 1926-03-19 1930-05-13 United States Gypsum Co Wet mixing method and apparatus
US2843080A (en) * 1955-08-02 1958-07-15 Gen Foods Corp Popcorn flavoring apparatus
US3163402A (en) * 1958-03-31 1964-12-29 Yamashita Hachiro Apparatus for substantially instantly mixing and kneading various materials

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3863904A (en) * 1972-01-18 1975-02-04 Design Link Mixing of fragile granular materials
US4092737A (en) * 1975-08-11 1978-05-30 Bertil Sandell Method for preparing fibers for mixing into a sprayed concrete mass and a device for performing the method
EP0101255A3 (en) * 1982-08-05 1984-07-25 Croker Limited Improvements in mixing machines
US6641296B1 (en) * 1997-04-24 2003-11-04 Jean-Luc Jouvin Method for mixing alginate using a rotatable elliptical bowl
US20130058186A1 (en) * 2010-03-10 2013-03-07 Wetend Technologies Oy Method and apparatus for mixing various flows into a process liquid flow
US9339774B2 (en) * 2010-03-10 2016-05-17 Wetend Technologies Oy Method and apparatus for mixing various flows into a process liquid flow
CN102985475A (en) * 2010-07-02 2013-03-20 那甘提普·普瓦鲁多姆 Homogeneous biodegradable mixture for shaped bodies and method for its preparation
US20130199408A1 (en) * 2010-07-02 2013-08-08 Ngamtip Poovarodom Homogeneous Biodegradable Mixture for Shaped-Bodies: Method for Preparing

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