US3672225A - Gas sampling - Google Patents
Gas sampling Download PDFInfo
- Publication number
- US3672225A US3672225A US63528A US3672225DA US3672225A US 3672225 A US3672225 A US 3672225A US 63528 A US63528 A US 63528A US 3672225D A US3672225D A US 3672225DA US 3672225 A US3672225 A US 3672225A
- Authority
- US
- United States
- Prior art keywords
- tube
- nozzle
- mouth
- static
- means defining
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000005070 sampling Methods 0.000 title claims abstract description 31
- 230000003068 static effect Effects 0.000 claims abstract description 38
- 239000000523 sample Substances 0.000 claims abstract description 25
- 239000012530 fluid Substances 0.000 claims abstract description 18
- 238000011144 upstream manufacturing Methods 0.000 claims description 4
- 239000007789 gas Substances 0.000 description 18
- 230000003189 isokinetic effect Effects 0.000 description 4
- 238000010276 construction Methods 0.000 description 3
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000000428 dust Substances 0.000 description 2
- 239000012717 electrostatic precipitator Substances 0.000 description 2
- 238000005755 formation reaction Methods 0.000 description 2
- 239000013618 particulate matter Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000001419 dependent effect Effects 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000003595 mist Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
- G01N1/2247—Sampling from a flowing stream of gas
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/22—Devices for withdrawing samples in the gaseous state
- G01N1/2247—Sampling from a flowing stream of gas
- G01N2001/225—Sampling from a flowing stream of gas isokinetic, same flow rate for sample and bulk gas
Definitions
- ABSTRACT Apparatus for sampling fluid flow in a conduit comprising a sampling probe having an aerodynamically shaped nozzle and a double static tube axially located within the nozzle and extending beyond its mouth to terminate in a closed, aerodynamically contoured end, the outer wall of the extended portion of the tube being provided with first and second orifices to communicate with the bore of the tube and the annular passage of the tube remote from the extended portion operatively communicating with a pressure sensing device to sense the static pressure of the fluid flow outside the nozzle and the static pressure of the fluid flow entering the mouth of the nozzle.
- This invention relates to apparatus for sampling fluid such as dust or mist-laden effluent gases from chemical or industrial plants, and particularly to an isokinetic sampling probe used in sampling these gases.
- the conventional apparatus for sampling effluent gases comprises a sampling probe having a shaped nozzle, which is inserted into the stream to be sampled.
- the gas is drawn by means of a vacuum pump through the probe and a sampling train consisting of a filter, a cyclone or electrostatic precipitator, followed by a condenser, catch-pot and a rotameter.
- the gas sample must be collected under isokinetic conditions, that is, the velocity of the gas entering the nozzle of the probe should be the same as the velocity of the gas stream from which the sample is taken, otherwise the sample is not truly representative of the effluent stream.
- the velocity of the gas stream must be continuously monitored and, when deviations occur, the sampling rate has to be adjusted accordingly. This is normally done by using Pitot tubes and the readings obtained are converted to velocities by means of slide rules or nomographs supplied with the apparatus.
- the weight of particulate matter collected in the filter is determined and related to volume of gas sampled to obtain the contaminate concentration in the stack gas.
- An improved apparatus for sampling fluid uses a so-called Null Point Probe, that is, a probe having a specially designed nozzle through which the static pressures inside and outside the nozzle can be measured by means of orifices situated in the inner and in the outer walls of the nozzle construction.
- Null Point Probe a probe having a specially designed nozzle through which the static pressures inside and outside the nozzle can be measured by means of orifices situated in the inner and in the outer walls of the nozzle construction.
- a further disadvantage is that the nozzles are not readily interchangeable so that, at high or low gas velocities, the sampling rates are either very high or extremely low respectively.
- a sampling probe having an aerodynamically shaped nozzle and a double static tube as defined herein axially located within the nozzle and extending beyond its mouth to terminate in a closed, aerodynarnically contoured end, the outer wall of the extended portion of the tube being provided with first and second orifices to communicate with the bore and with the annular passage respectively of the tube and the opposite end of the bore and the annular passage of the tube remote from the extended portion operatively communicating with a pressure sensing device to sense the static pressure of the fluid flow outside the nozzle and the static pressure of the fluid flow entering the mouth of the nozzle.
- the first orifices of the double static tube for sensing the pressure outside the nozzle are located, preferably, at a distance of at least 13 tube diameters from the streamlined end of the tube to avoid any eddy or vortex formation within the fluid, which may be caused during its flow past the end of the tube.
- the second orifices for sensing the pressure of the fluid flow entering the nozzle are located, preferably, on or adjacent the outside of the plane of the mouth of the nozzle. This position has been determined to avoid a pressure drop within the nozzle. Additionally, these second orifices should be at a distance of at least 21 tube diameters from the streamlined end of the tube to avoid possible interference caused by the first orifices.
- the pressure sensing orifices in the tube have a diameter, preferably, of not more than one tenth of the external diameter of the tube.
- the nozzle which is part of the probe, may be replaced without difliculty, since the pressure sensing devices are not located in the body of the nozzle.
- FIG. 1 is a cross section of the assembled sampling probe
- FIG. 2 is an enlarged cross section of the double static tube, forming part of the probe.
- the sampling probe l is shown with detachable nozzle 2 and a double static tube 3.
- the first pressure sensing orifices 4 and the second pressure sensing orifices 5 in the wall surrounding the central passage of the extended portion of the double static tube 3 are in communication with a pressure sensing device via manifold 6 and tubes 7.
- FIG. 2 illustrates the detailed construction of double static tube 3 and shows the location of the pressure sensing orifices 4 and 5 in relation to the streamlined end 9 of the tube.
- the frontal portion 8 of the tube may be made of solid material.
- the apparatus is used in conjunction with a standard filter, cyclone or electrostatic precipitator and a vacuum pump. Any sensitive sensing device may be used to measure the pressure difference between the first and second sensing orifices.
- the size of the nozzle used is dependent on the velocity of the gas stream and, preferably, is selected to give a sampling flow rate of between 5 I and 6 cubic meters per hour under isokinetic conditions, so that the sampling periods for collecting a representative sample are between 5 and 10 minutes.
- Water vapor if present in the gas flow, may condense in the cold parts of the sampling probe and a heated mantle 10 may be provided around these parts to prevent this condensation.
- the probe was tested in an experimental duct with sampling velocities ranging from 5 to 25 meters per second and four sizes of nozzles were used to cover this range.
- sampling flow rate was measured on an accurate rotameter and the difference between this measured flow rate and the flow rate calculated from the velocity and the nozzle means defining a closed, aerodynamically contoured end;
- said double static tube including means defining a longitudinal bore terminating short of said closed, aerodynamically contoured end;
- said first and second orifices being axially displaced from one another along said double static tube;
- a pressure sensing device for sensing the static pressure of the fluid flow outside the nozzle and the static pressure of the fluid flow entering the mouth of the nozzle;
- conduit means independently communicating said bore and said annular passage to said pressure sensing device remotely of and upstream of the mouth of the nozzle as inputs to said pressure sensing device.
- Apparatus as claimed in claim 1 in which the second orifice for sensing the static pressure inside the nozzle is located no further upstream than a radial plane across the mouth of the nozzle at a distance of at least 2! tube diameters from the end of the tube 4.
- Apparatus as claimed in claim 1 in which each of the pressure sensing orifices in the tube has a diameter of not more than one tenth of the external diameter of the tube.
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biomedical Technology (AREA)
- Molecular Biology (AREA)
- Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
Apparatus for sampling fluid flow in a conduit comprising a sampling probe having an aerodynamically shaped nozzle and a double static tube axially located within the nozzle and extending beyond its mouth to terminate in a closed, aerodynamically contoured end, the outer wall of the extended portion of the tube being provided with first and second orifices to communicate with the bore of the tube and the annular passage of the tube remote from the extended portion operatively communicating with a pressure sensing device to sense the static pressure of the fluid flow outside the nozzle and the static pressure of the fluid flow entering the mouth of the nozzle.
Description
United States Patent Louis 1 June 27, 1972 54] GAS SAMPLING 2,452,224 10/1948 Collett, Jr
[72] Inventor: Rodney Brian Louis, Johannesburg, Re-
33:52: et pub! Smth Afnca 3,050,996 8/1962 Henderson ..73/182 [73] Assignee: African Explosives and Chemical Industries Limited Primary Examiner-Louis R. Prince Assistant Examinerwilliam A. Henry, II [22] Flled' 1970 Attorney-Cushman, Darby and Cushman Appl. No.: 63,528
[57] ABSTRACT Apparatus for sampling fluid flow in a conduit comprising a sampling probe having an aerodynamically shaped nozzle and a double static tube axially located within the nozzle and extending beyond its mouth to terminate in a closed, aerodynamically contoured end, the outer wall of the extended portion of the tube being provided with first and second orifices to communicate with the bore of the tube and the annular passage of the tube remote from the extended portion operatively communicating with a pressure sensing device to sense the static pressure of the fluid flow outside the nozzle and the static pressure of the fluid flow entering the mouth of the nozzle.
5 Claims, 2 Drawing Figures P R ESSURE SENSING PATENTEDJum I972 3.672.225
EEEEJ' P'A'TENTEDJum 1972 3. 672,225
/l diw GAS SAMPLING This invention relates to apparatus for sampling fluid such as dust or mist-laden effluent gases from chemical or industrial plants, and particularly to an isokinetic sampling probe used in sampling these gases.
Sampling probes used for determining the dust or mist in stack gases often produce unreliable results or are difficult to handle and, in view of present legislation covering atmospheric pollution in many countries, hinder the routine analyses of effluent gases which have to be carried outin view of this legislation. It is important, therefore, that apparatus be of simple construction and be easy to manipulate.
The conventional apparatus for sampling effluent gases comprises a sampling probe having a shaped nozzle, which is inserted into the stream to be sampled. The gas is drawn by means of a vacuum pump through the probe and a sampling train consisting of a filter, a cyclone or electrostatic precipitator, followed by a condenser, catch-pot and a rotameter.
' The particulate matter is trapped in the filter and water vapor, if present, is condensed in the condenser.
The gas sample must be collected under isokinetic conditions, that is, the velocity of the gas entering the nozzle of the probe should be the same as the velocity of the gas stream from which the sample is taken, otherwise the sample is not truly representative of the effluent stream. To ensure these conditions, the velocity of the gas stream must be continuously monitored and, when deviations occur, the sampling rate has to be adjusted accordingly. This is normally done by using Pitot tubes and the readings obtained are converted to velocities by means of slide rules or nomographs supplied with the apparatus. At the end of the sampling period, the weight of particulate matter collected in the filter is determined and related to volume of gas sampled to obtain the contaminate concentration in the stack gas.
An improved apparatus for sampling fluid uses a so-called Null Point Probe, that is, a probe having a specially designed nozzle through which the static pressures inside and outside the nozzle can be measured by means of orifices situated in the inner and in the outer walls of the nozzle construction. By maintaining these inside and outside pressures equal, isokinetic conditions are obtained. The use of these nozzles obviates the measurement individually of the velocity of the gas stream and of the sampling rate. Nevertheless, it has been found that the static pressures measured via the sensing orifices on the inside and outside of the nozzle are influenced by the nozzle shape. The shape of the nozzle causes eddy and vortex formations on the outside, as well as a pressure loss on the inside of the nozzle. Consequently, erratic results are obtained when using these nozzles.
A further disadvantage is that the nozzles are not readily interchangeable so that, at high or low gas velocities, the sampling rates are either very high or extremely low respectively.
It is the principal purpose of the present invention to provide a null point sampling probe, which largely or wholly eliminates the difficulties encountered in the prior art.
We have now discovered that these undesirable influences afiecting static pressures because of the shape of the nozzle may be avoided by sensing the static pressures outside, and at the entrance to, the nozzle. This advance in the art is achieved by means of a double tube comprising two concentric tubes which provide an axial bore and an annular passage surrounding the wall of that bore. This new feature, which is introduced as part of a null point probe, we designate by the expression double static tube.
Accordingly, we provide apparatus for sampling fluid flow in a conduit comprising a sampling probe having an aerodynamically shaped nozzle and a double static tube as defined herein axially located within the nozzle and extending beyond its mouth to terminate in a closed, aerodynarnically contoured end, the outer wall of the extended portion of the tube being provided with first and second orifices to communicate with the bore and with the annular passage respectively of the tube and the opposite end of the bore and the annular passage of the tube remote from the extended portion operatively communicating with a pressure sensing device to sense the static pressure of the fluid flow outside the nozzle and the static pressure of the fluid flow entering the mouth of the nozzle.
The first orifices of the double static tube for sensing the pressure outside the nozzle are located, preferably, at a distance of at least 13 tube diameters from the streamlined end of the tube to avoid any eddy or vortex formation within the fluid, which may be caused during its flow past the end of the tube.
The second orifices for sensing the pressure of the fluid flow entering the nozzle are located, preferably, on or adjacent the outside of the plane of the mouth of the nozzle. This position has been determined to avoid a pressure drop within the nozzle. Additionally, these second orifices should be at a distance of at least 21 tube diameters from the streamlined end of the tube to avoid possible interference caused by the first orifices.
The pressure sensing orifices in the tube have a diameter, preferably, of not more than one tenth of the external diameter of the tube.
The nozzle, which is part of the probe, may be replaced without difliculty, since the pressure sensing devices are not located in the body of the nozzle.
An embodiment of the apparatus will be described with reference to the accompanying drawings, in which FIG. 1 is a cross section of the assembled sampling probe, and
FIG. 2 is an enlarged cross section of the double static tube, forming part of the probe.
In FIG. 1, the sampling probe l is shown with detachable nozzle 2 and a double static tube 3. The first pressure sensing orifices 4 and the second pressure sensing orifices 5 in the wall surrounding the central passage of the extended portion of the double static tube 3 are in communication with a pressure sensing device via manifold 6 and tubes 7.
FIG. 2 illustrates the detailed construction of double static tube 3 and shows the location of the pressure sensing orifices 4 and 5 in relation to the streamlined end 9 of the tube. The frontal portion 8 of the tube may be made of solid material.
The apparatus is used in conjunction with a standard filter, cyclone or electrostatic precipitator and a vacuum pump. Any sensitive sensing device may be used to measure the pressure difference between the first and second sensing orifices.
The size of the nozzle used is dependent on the velocity of the gas stream and, preferably, is selected to give a sampling flow rate of between 5 I and 6 cubic meters per hour under isokinetic conditions, so that the sampling periods for collecting a representative sample are between 5 and 10 minutes.
Water vapor, if present in the gas flow, may condense in the cold parts of the sampling probe and a heated mantle 10 may be provided around these parts to prevent this condensation.
The probe was tested in an experimental duct with sampling velocities ranging from 5 to 25 meters per second and four sizes of nozzles were used to cover this range.
The sampling flow rate was measured on an accurate rotameter and the difference between this measured flow rate and the flow rate calculated from the velocity and the nozzle means defining a closed, aerodynamically contoured end;
said double static tube including means defining a longitudinal bore terminating short of said closed, aerodynamically contoured end;
a means defining a first orifice communicating the exterior of the double static tube, toward said end from said mouth, with said bore;
means defining an annular passage in said double static tube surrounding said bore, but being separated therefrom;
means defining a second orifice communicating the exterior of the double static tube, toward said end from said mouth, with said annular passage;
said first and second orifices being axially displaced from one another along said double static tube;
a pressure sensing device for sensing the static pressure of the fluid flow outside the nozzle and the static pressure of the fluid flow entering the mouth of the nozzle;
conduit means independently communicating said bore and said annular passage to said pressure sensing device remotely of and upstream of the mouth of the nozzle as inputs to said pressure sensing device.
2. Apparatus as claimed in claim 1 in which the first orifice for sensing the static pressure outside the nozzle is located at a distance of at least 13 tube diameters from the end of the tube.
3. Apparatus as claimed in claim 1 in which the second orifice for sensing the static pressure inside the nozzle is located no further upstream than a radial plane across the mouth of the nozzle at a distance of at least 2! tube diameters from the end of the tube 4. Apparatus as claimed in claim 1 in which each of the pressure sensing orifices in the tube has a diameter of not more than one tenth of the external diameter of the tube.
5. Apparatus as claimed in claim 1 in which the nozzle of the probe is detachably connected thereto, so as to be interchangeable with other noules of different dimensions and shapes.
* t F l
Claims (5)
1. Apparatus for sampling fluid flow in a conduit, comprising: a sampling probe, including means defining a tubular nozzle having means defining a mouth; a double static tube extending axially within said nozzle and extending out past the mouth thereof to terminate in means defining a closed, aerodynamically contoured end; said double static tube including means defining a longitudinal bore terminating short of said closed, aerodynamically contoured end; a means defining a first orifice communicating the exterior of the double static tube, toward said end from said mouth, with said bore; means defining an annular passage in said double static tube surrounding said bore, but being separated therefrom; means defining a second orifice communicating the exterior of the double static tube, toward said end from said mouth, with said annular passage; said first and second orifices being axially displaced from one another along said double static tube; a pressure sensing device for sensing the static pressure of the fluid flow outside the nozzle and the static pressure of the fluid flow entering the mouth of the nozzle; conduit means independently communicating said bore and said annular passage to said pressure sensing device remotely of and upstream of the mouth of the nozzle as inputs to said pressure sensing device.
2. Apparatus as claimed in claim 1 in which the first orifice for sensing the static pressure outside the nozzle is located at a distance of at least 13 tube diameters from the end of the tube.
3. Apparatus as claimed in claim 1 in which the second orifice for sensing the static pressure inside the nozzle is located no further upstream than a radial plane across the mouth of the nozzle at a distance of at least 21 tube diameters from the end of the tube.
4. Apparatus as claimed in claim 1 in which each of the pressure sensing orifices in the tube has a diameter of not more than one tenth of the external diameter of the tube.
5. Apparatus as claimed in claim 1 in which the nozzle of the probe is detachably connecTed thereto, so as to be interchangeable with other nozzles of different dimensions and shapes.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ZA695850A ZA695850B (en) | 1969-08-15 | 1969-08-15 | Improvements in gas sampling |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US3672225A true US3672225A (en) | 1972-06-27 |
Family
ID=25561423
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US63528A Expired - Lifetime US3672225A (en) | 1969-08-15 | 1970-08-13 | Gas sampling |
Country Status (3)
| Country | Link |
|---|---|
| US (1) | US3672225A (en) |
| GB (1) | GB1267885A (en) |
| ZA (1) | ZA695850B (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3841145A (en) * | 1971-11-15 | 1974-10-15 | Rader Companies | Method and apparatus for measuring particulate emissions in gas flow |
| EP0023110A1 (en) * | 1979-07-09 | 1981-01-28 | Exxon Research And Engineering Company | Method and device for isokinetic sampling and installation provided with such a device |
| US5463908A (en) * | 1992-03-30 | 1995-11-07 | Rosolia; Antonio | Apparatus for sampling and registering fluids in pipelines |
| US5907109A (en) * | 1998-05-05 | 1999-05-25 | Tedeschi; Rinaldo R. | Vehicle emission sampling probe apparatus |
| RU2194958C2 (en) * | 2000-06-19 | 2002-12-20 | Жданов Владимир Федорович | Probe measuring differential and gauge pressure of gas or liquid in pipe-line |
| CN1313811C (en) * | 2003-11-21 | 2007-05-02 | 中国石油天然气股份有限公司 | Solid dust sampling probe in pipeline |
| US20110203350A1 (en) * | 2008-11-06 | 2011-08-25 | Stanislaw Kaminski | Method for measuring dust concentration in flowing gas and device for measuring dust concentration in flowing gas |
| US20120186366A1 (en) * | 2011-01-26 | 2012-07-26 | Energy & Environmental Research Center | Measurement of multimetals and total halogens in a gas stream |
| US11085854B2 (en) * | 2018-03-16 | 2021-08-10 | Huazhong University Of Science And Technology | Non-water-cooled high temperature aerosol quantitative dilution sampling probe |
-
1969
- 1969-08-15 ZA ZA695850A patent/ZA695850B/en unknown
-
1970
- 1970-08-13 GB GB39093/70A patent/GB1267885A/en not_active Expired
- 1970-08-13 US US63528A patent/US3672225A/en not_active Expired - Lifetime
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3841145A (en) * | 1971-11-15 | 1974-10-15 | Rader Companies | Method and apparatus for measuring particulate emissions in gas flow |
| EP0023110A1 (en) * | 1979-07-09 | 1981-01-28 | Exxon Research And Engineering Company | Method and device for isokinetic sampling and installation provided with such a device |
| US5463908A (en) * | 1992-03-30 | 1995-11-07 | Rosolia; Antonio | Apparatus for sampling and registering fluids in pipelines |
| US5907109A (en) * | 1998-05-05 | 1999-05-25 | Tedeschi; Rinaldo R. | Vehicle emission sampling probe apparatus |
| RU2194958C2 (en) * | 2000-06-19 | 2002-12-20 | Жданов Владимир Федорович | Probe measuring differential and gauge pressure of gas or liquid in pipe-line |
| CN1313811C (en) * | 2003-11-21 | 2007-05-02 | 中国石油天然气股份有限公司 | Solid dust sampling probe in pipeline |
| US20110203350A1 (en) * | 2008-11-06 | 2011-08-25 | Stanislaw Kaminski | Method for measuring dust concentration in flowing gas and device for measuring dust concentration in flowing gas |
| US8567266B2 (en) * | 2008-11-06 | 2013-10-29 | Stanislaw Kaminski | Method and device for measuring dust concentration in flowing gas |
| US20120186366A1 (en) * | 2011-01-26 | 2012-07-26 | Energy & Environmental Research Center | Measurement of multimetals and total halogens in a gas stream |
| US11085854B2 (en) * | 2018-03-16 | 2021-08-10 | Huazhong University Of Science And Technology | Non-water-cooled high temperature aerosol quantitative dilution sampling probe |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2040593B2 (en) | 1973-01-18 |
| GB1267885A (en) | 1972-03-22 |
| ZA695850B (en) | 1971-03-31 |
| DE2040593A1 (en) | 1971-02-25 |
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