US3471365A - Apparatus for impregnating fibrous material - Google Patents
Apparatus for impregnating fibrous material Download PDFInfo
- Publication number
- US3471365A US3471365A US658953A US3471365DA US3471365A US 3471365 A US3471365 A US 3471365A US 658953 A US658953 A US 658953A US 3471365D A US3471365D A US 3471365DA US 3471365 A US3471365 A US 3471365A
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- Prior art keywords
- container
- chamber
- chips
- pressure
- impregnating
- Prior art date
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- 239000002657 fibrous material Substances 0.000 title description 12
- 239000000463 material Substances 0.000 description 54
- 239000000126 substance Substances 0.000 description 41
- 239000007788 liquid Substances 0.000 description 37
- 238000010411 cooking Methods 0.000 description 21
- 230000006835 compression Effects 0.000 description 12
- 238000007906 compression Methods 0.000 description 12
- 239000011148 porous material Substances 0.000 description 10
- 238000009408 flooring Methods 0.000 description 9
- 238000005470 impregnation Methods 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 230000000903 blocking effect Effects 0.000 description 7
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 238000004519 manufacturing process Methods 0.000 description 6
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 6
- 238000007599 discharging Methods 0.000 description 5
- 230000000694 effects Effects 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- 241000196324 Embryophyta Species 0.000 description 4
- 229920001131 Pulp (paper) Polymers 0.000 description 4
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 3
- 238000004891 communication Methods 0.000 description 3
- 230000007246 mechanism Effects 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 235000010265 sodium sulphite Nutrition 0.000 description 3
- 239000012808 vapor phase Substances 0.000 description 3
- 239000002023 wood Substances 0.000 description 3
- 230000004888 barrier function Effects 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 229920002678 cellulose Polymers 0.000 description 2
- 239000001913 cellulose Substances 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 230000002706 hydrostatic effect Effects 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 230000009467 reduction Effects 0.000 description 2
- 229910000029 sodium carbonate Inorganic materials 0.000 description 2
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 description 1
- 241000609240 Ambelania acida Species 0.000 description 1
- 244000025254 Cannabis sativa Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 239000010905 bagasse Substances 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000005489 elastic deformation Effects 0.000 description 1
- 235000019253 formic acid Nutrition 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 235000005985 organic acids Nutrition 0.000 description 1
- AHLBNYSZXLDEJQ-FWEHEUNISA-N orlistat Chemical compound CCCCCCCCCCC[C@H](OC(=O)[C@H](CC(C)C)NC=O)C[C@@H]1OC(=O)[C@H]1CCCCCC AHLBNYSZXLDEJQ-FWEHEUNISA-N 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 238000009931 pascalization Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000007790 scraping Methods 0.000 description 1
- GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 description 1
- 230000003068 static effect Effects 0.000 description 1
- 239000010902 straw Substances 0.000 description 1
- 230000032258 transport Effects 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Images
Classifications
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21C—PRODUCTION OF CELLULOSE BY REMOVING NON-CELLULOSE SUBSTANCES FROM CELLULOSE-CONTAINING MATERIALS; REGENERATION OF PULPING LIQUORS; APPARATUS THEREFOR
- D21C1/00—Pretreatment of the finely-divided materials before digesting
Definitions
- the raw material to be treated in accordance with the present invention is in the first instance constituted by wood disintegrated into chips; but also several varieties of grass, straw, bagasse and the like may be used with satisfactory results.
- the pulp is intended for use in the paper industry and also for the manufacture of fibre board and building elements or other products consisting of or containing such pulp.
- the raw material is subjected to an impregnation stage, at least one cooking step and a subsequent mechanical disintegration step.
- the impregnation step includes a mechanical compression of the material for partial elastic deformation and subsequent expansion thereof below the surface of chemicals containing liquid.
- the material Prior to the mechanical compression the material is heated to a temperature of 60 to 100 C. or even more, preferably by steam.
- air and liquid present between the pieces of material, such as chips, and particularly within the pores of said material is removed and when the mechanical compression ceases and the material is regaining its original volume, liquid is sucked into the pores. If the material in its raw state contains moisture exceeding 0.8 parts per one part of material calculated as completely dry, part of said moisture is pressed out which facilitates the subsequent impregnation with the chemicals-containing liquid.
- the expansion of the material within the liquid is effected while this liquid is subjected to an external superatmospheric pressure.
- the pressure to which the material is subjected during the expansion within the liquid may in this manner be increased to a many times larger pressure than the static pressure exerted by the liquid column itself onto the material.
- the remainder of air within the material is compressed and occupies a correspondingly minor volume for which reason the material will be capable of absorbing more liquid. If the container or conveyor within which the impregnation is made has so great height that the liquid column within the same is 8 metres, for example, the maximum of pressure exterted by the liquid column adjacent to the base of the container will be about 0.8 kilograms per square centimetre.
- the pressure acting on the liquid may, without difiiculty be increased to ten times said value, for example, so as to cause the air remaining in the pores of the ligno-cellulose-containing material to be compressed to a corresponding small volume, which allows additional impregnation liquid to reach the interior of the material.
- the reduction of pressure in the pores of the materials caused by the upwardly directed movement of the material out of the liquid will become so inconsiderable, calculated in per cent, as to become negligible.
- a feature of the invention resides in a plug-forming means by which the material being fed from one container to another is compressed against a pressure-regulatable wall, which can assume the form of a pivoted flap under hydraulic pressure to oppose the movement of the material to a predetermined extent until the material has built up into a plug of the desired density.
- the several cooking steps involved therein may employ the solutions of chemicals having mutually diiierent composition.
- the wood substance is affected by the organic acids usually present in said substances, such as formic acid and acetic acid.
- sodium carbonate or sodium hydroxide or possibly both or some other neutralizing substance are added.
- FIG. 1 shows in elevation, and partly in section, a plant or carrying out the method according to my invention
- FIG. 2 is a sectional view, taken substantially on the line 22 of FIG. 1, looking in the direction of the arrows;
- FIG. 3 shows in elevation and partly in section, a slightly different embodiment of the invention
- FIG. 4 shows in section, the remainder of the plant partly shown in FIG. 3;
- FIG. 5 is a sectional view, taken on the line 5-5 of FIG. 4, and
- FIG. 6 is an enlarged view, partly in section, of the mechanical compressing or plug-forming mechanism and associated parts.
- FIGS. 1 and 2 there is therein shown a container 10 erected on a flooring 12 and extending vertically upwardly through a flooring 14 located at a higher level.
- the container 10 has an upper closure member 16, the upper end of which is formed with a steam outlet 18. Chips are supplied to the member 16 from a storage bin (not shown) through a duct 20 from which'the chips fall down into the container 10. If the supply of chips is too great, the excess returns through a duct 22 to the storage bin. Passing through the ducts 20 and 22 is a scraping conveyor (not shown).
- the container 10 thus serves as a kind of zone for softening by means of steam within which zone the chips are gradually heated to a temperature exceeding 70 C. and suitably maintained between C. and C. and in some cases reaching the boiling point of water at atmospheric pressure. Any excess of steam may escape through the outlet 18, but the supply of steam through the pipe 24 is controlled so as to avoid such excess as far as possible.
- the chips softened in the base zone are conveyed by a screw conveyor 29 located in the lower part of the container 10 and driven by an electric motor 27 through a reduction gear 28, into a plug-forming tube 30.
- a pivoted flap 31 (FIG. which, through the intermediary of an arm 32 is loaded by a hydraulic servo-motor 34 and thus assists in subjecting the mass of chips to high pressure.
- the chips are compressed mechanically so as to expel air and water present in the pores of said chips.
- the air and water thus expelled from the chips passes out through apertures 29a provided in the lower portion of the frustoconical housing 30a for the screw conveyor 29.
- the water thus drained from the housing 30a descends into the receptacle 31a and is drained therefrom in any suitable way.
- a container 36 which also extends upwardly through the flooring 14.
- impregation of the chips is effected while the mass of chips is simultaneously conveyed up to the higher floor.
- a vessel 38 within which a solution of chemicals is prepared and is conveyed to a pump 40 and through a pipe 42 up to a container 44 provided with a level control 46 which insures that the solution of chemicals is maintained at a predetermined constant level within this container.
- a tube 48 inter-connects the base parts of the containers 44 and 36 and thus in the container 36 a liquid column is formed reaching to substantially the same level as that in the container 44.
- the mass of chips When the mass of chips is compressed strongly, for example, subjected to a high pressure of 30 to 50 or even to 100 atmospheres in the tube 30 enters the container 36 at its base, it will immediately enter a bath of the chemical solution. The chips expand towards their original volume and the solution is sucked into the pores of the chips.
- the preheating in the base section is intended to facilitate the compression in the plug-forming tube 30 and expansion takes place in the liquid-containing part of the container 36 which insures an extremely good impregnation of the chips with the chemical solution.
- the chips are conveyed upwardly within the container 36 preferably by means of two screw conveyors 50, 52 (FIG. 2.) driven by an electric motor 49, the conveyors having a pitch preferably of the same magnitude as the diameter of the container and being rotated at a low number of rotations such as 5 to revolutions per minute.
- the spacing between the axes of the two screw conveyors should not be substantially larger than the sum of the radii of the screws and may possibly be less in order to produce an effect preventing rotational movement of the chips.
- partitions 54 may be provided which are individually secured by welding and shaped to the periphery of the screws and designed to fill the areas adjacent the zones where the screws meet or engage one another.
- the chips are conveyed upwardly by the screws 50, 52 initially below the level of the liquid in the container 36, and leave the liquid at the top part of the container 36 and are discharged from the container by means of a conveyor 56 extending in a transverse direction and located in the upper end portion of the container 36.
- the liquid column in the container 36 is dimensioned so as to produce a relatively high hydrostatic pressure adjacent the base of the container where the compressed chips are allowed to expand. This pressure may be of the order of 3 to 5 meters and may possibly reach 10 meters water column and assists in forcing the solution of chemicals into the pores of the chips.
- the conveyor 56 delivers the impregnated chips into a hopper-shaped vessel 58. From there the chips fall into a vibrating feeder 60 to a so-called rotating cell feeder 62 having individual pockets separated from one another, the chips content of which is delivered to a container 64 extending downwardly to the lowest flooring of the plant.
- the cell feeder is also so constructed as to prevent direct communication between the closed container 64 and the vibrating feeder 60.
- the pockets of the cell feeder when moving upwards during rotation, contain steam at high pressure, which steam escapes through a duct 66 provided with a centri-cleaner 68 to separate any entrained chips, and thence through a duct 70.
- the lowermost flooring carries a container 72 of the same type as the container 38 and also intended for preparation of a solution of chemicals.
- This solution is fed by a pump 74 through a pipe 76 provided with a valve 78 controlled by a servo-motor 77 to the closed cooking container 64.
- the pipe 76 preferably opens near the middle portion of the container 64 to which steam is also sup plied at the base through a pipe 80 provided with a control valve 82.
- the cell feeder 62 is controlled by two systems of level regulators 84 which may be adjustably mounted on guides 86 and between which the level of the column of chips may fluctuate.
- the level of the solution of chemicals is also controlled by one or more systems of level regulators 88, which may be mounted on the same guides 86 and which actuate the servo-motor 77.
- steam is maintained at a pressure of the order of 8 to 10 kg./cm. and at corresponding temperature.
- the chips initially meet a steam atmosphere and are subjected to cooking in said atmosphere while also being affected by the chemicals with which they were earlier impregnated.
- the chips subsequently descend into the chemical solution in the form of a column of liquid in the container 64 which may be greater in extent than the vapor space provided in said container.
- the cooking is continued in the liquid bath, the chips being progressively exposed to fresh solution of chemicals supplied from the container 72.
- Container 58 houses screw conveyors 100 driven by an electric motor 102.
- the container 98 and the conveyors 100 may be of the same construction as the container 36 and its screw conveyors.
- the container 98 and the conveyors 100 may be of the same construction as the container 36 and its screw conveyors.
- the container 98 Within the container 98 the liquid will be at a level approximately the same or slightly higher than that within the container 64 and the cooking in the liquid phase is thus continued during the upwardly directed movement of the chips within the container 98.
- the container 98 which, in the same manner as the container 64, is closed and heat-insulated with respect to the surrounding atmosphere, has an upper vapor chamber within which a second cooking in the vapor phase may be effected.
- the chips thus treated are fed from the top portion of the container 98 by a horizontal conveyor 104 to a mechanical disintegrator 106 provided with two grinding discs mutually rotatable and disposed within a zone 108 of the plant.
- the ground material or pulp then passes through a conduit 110 to a centri-cleaner 112 after which it may be subjected to further treatment such as a further mechanical grinding step.
- the defibrator 106 may suitably be of a known kind.
- the mechanical disintegration in the embodiment shown is effected subsequent to the last cooking step and under the same conditions regarding temperature and pressure. The disintegration may, however, also be effected under atmospheric conditions.
- FIG. 3 The embodiment of the invention disclosed in FIG. 3 is similar in most respects to that shown in FIG. 1, a primary difference being that the several containers 10, 36, 64 and 98 are arranged on the same flooring or level. These elements may have such longitudinal dimension as to project from the flooring 12 upwardly through higher fioorings 14 and 16 respectively.
- the chips enter through duct 20 to the container through the vertical discharge tube a.
- the latter communicates with the container 10 through a rotating cell feeder 2211 having individual pockets separated from one another, the chips content of each of which is separately delivered to the container 10 through the top thereof.
- the cell feeder is in connection with a duct 24a through which steam or air present in the pockets escapes into the surrounding atmosphere during the movement of the pockets upwardly from the container 10.
- the cell feeder 22 blocks free communication between the top portion of the vertical container 10 and the surrounding atmosphere. Steam flows upwardly in the container in a direction opposite to that of the chips descending within the container, the steam being introduced into the base portion of the container through the pipe 26 controlled by the valve 28.
- the raw material is preheated by means of steam to a temperature usually kept below 100 C. and reaching higher temperature in some cases to 120 to 130 C., or even more. Simultaneously with the heating of the chips by the steam, part of the air present in the individual in the pores thereof, or between the chips, is expelled.
- the cell feeder 22a provides for the feed of the air thus expelled from the container 10, to the conduit 24a.
- atmospheric pressure, or a slighter pressure may be maintained.
- the upper level of the column of chips in the container 10 may fluctuate and be controlled within limits defined by level regulators 62a in the known manner. These regulators are adjustably mounted on guides 32a and actuate the driving motor of the cell feeder.
- the plug-forming mechanism located at the base of the container 10 is substantially similar to that shown in FIG. 6, except for the reversal of position of the hydraulic servo-motor 34.
- the flap 31 forms a wall against which the material is compressed to form a plug of the desired density, the flap having a regulatable pressure opposing the material until the required build-up is attained and then allowing the material to move forwardly into the container 36.
- the materials proceed into the container 36 in the manner described in the previous embodiment of FIG. 1.
- a solution of chemicals prepared in the vessel 38 is fed into the base part of the conveyor 36 through a tube 42a and pump unit 40.
- the tube 42a may be surrounded by a heating coil 60a to effect a heating of the solution flowing towards the container 36.
- the liquid is caused to rise to a level controlled by the level regulators 36a, which in the illustrated embodiment of the apparatus, as shown in FIG. 3, actuate the pump 49.
- the horizontal conveyor 64 to the cooker 64 which has a vertical dimension of substantially the same magnitude as the container 10 and the container 36 respectively.
- the quantity of chips housed in the cooker 64 is controlled by level regulators 84 which in turn govern the feeding speed of the screw feeder 29.
- Solution of chemicals is supplied to the cooker 64 from a storage vessel 72 through the tube 76 provided with the pump 74 and a valve 78 controlled by the servoactuated motor 77.
- the tube 76 may open into the cooker 64 substantially in the middle zone thereof.
- the level regulator 88 positioned below the regulator 84 is intended to actuate the servo-motor 77 to effect control of the liquid level within the cooker 64.
- Said regulators are mounted adjustably in the vertical direction on guides 86.
- Steam under pressure, as described in conjunction with FIG. 1, is supplied to the cooker 64 through a conduit 82 controlled by a valve 84a. Air collecting in the system may be intermittently removed through an escape tube 86a controlled by a valve 87a.
- the chemicals containing liquid admitted to the container 36 has preferably a relatively low temperature such as to C. in order to avoid heating of the raw material to higher temperatures prior to its thorough impregnation with the chemicals containing liquid. If, however, the disadvantageous effects caused by high temperatures such as alteration of color of the pulp into brown, beginning hydrolysis or similar effects are negligible, the liquid when pumped into the container 36 may have a temperature of 150 to 180 C. and even a still higher temperature.
- all reaction vessels or containers 10, 36, 64 and 98 may be interconnected to equalize the pressure prevailing therein.
- the pressure-equalizing tube 103 has branch connection tubes 128, to the containers 36 and 10 respectively.
- the tubes controlling valves denoted by 132, 134, 136, and 138 respectively are provided for each of the tubes controlling valves denoted by 132, 134, 136, and 138 respectively.
- a valve con trols a tube 142 through which water vapor may be supplied or which may also serve as a discharge conduit.
- the same pressure may thus be maintained, or if desired, pressure differences may be produced if the containers by suitable adjustment of the valves.
- the ligno-cellulose-containing material treated in this way may be directly blown out into the centri-cleaner 112 (FIG. 4) or any other suitable receiving apparatus.
- a mechanical disintegrating apparatus 106 constructed as a disc refiner, for example, is interposed ahead of said cleaner.
- the discharge side of the apparatus 106 is connected with the centricleaner 112 through conduit 110 and behind the centri-cleaner a conveyor transports the materials to a hopper 151 forming part of a de-Watering device 114, from which the cooking liquid expelled by compression is drawn off through a tube 116 whereas the pulp product is discharged by means of a conveyor 118.
- This product may be diluted with water in a vessel 120 and is refined in a second disc refiner 122 whereupon it is fed into a storage vessel 124 to be conveyed further to a papermaking machine by means of a pulp pump 126, for example.
- the chemicals used in the treatment of the lignocellulose-containing material may be of any known kind and have suitably mutually different composition in the liquids used in the impregnating steps.
- the impregnating liquid in the container 36 may substantially consist of sodium sulphite and sodium carbonate in the presence of which chemicals, the treatment in the vapor phase within the upper zones of the container 36 and the cooker 64 is effected.
- the cooking liquid prepared in the container 38 may contain sodium sulphite and sodium hydroxide or sodium sulphide.
- the particular composition employed may be used in both embodiments of the invention.
- a plug of material formed in the feeding device 29 to 34 is normally suificient to act as a barrier preventing vapor and liquid from escaping through said device. If, however, this barrier for some reason or other should cease to be operative and as a consequence the pressure in the container 10 should rise, the cell feeders 22a will prevent raw material, liquid and vapor from escaping out of the system which means that open communication between the system operating under high pressure and the surrounding atmosphere will not be established under such conditions.
- An apparatus for treating lignocellulose-containing fibrous material for the production of paper pulp including:
- conveyor means for conveying the expanded and impregnated material upwardly in said impregnating chamber
- An apparatus for treating lignocellulose-containing fibrous material for the production of paper pulp including (a) a steam treating chamber;
- said means (g) further includes means to drain oif liquid discharged from said fibrous plugs by said compression.
- said means (g) includes a continuous conveyor in said passage, a plate movable into and out of blocking position relative to said passage, and force means biasing said plate toward blocking position but releasing said plate when the compression of said fibrous plug reaches a desired maximum.
- An apparatus for treating lignocellulose-containing fibrous material for the production of paper pulp including (a) a steam treating chamber;
- said compression chamber further includes means to drain off liquid discharge from said fibrous plugs by said compression.
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- Paper (AREA)
- Dry Formation Of Fiberboard And The Like (AREA)
Description
Oct. 7, 1969 A. J. A. ASPLUND 3,471,365
APPARATUS FOR IMPREGNATING FIBROUS MATERIAL Original Filed May 16, 1966 4 Sheets-Sheet 1 Fig. 1.
' INVENTOR. i?!) Ai/lforAg/I/Ufld Oct. 7, 1969 A. J. A. ASPLUND 3,471,355
APPARATUS FOR IMPREGNATING FIBHOUS MATERIAL I Eriginal Filed May 16, 1966 I 4 Sheets-Sheet 5 I N VEN TOR.
Oct. 7, 1969 A. J. A. ASPLUND 3,471,365
APPARATUS FOR IMPREGNATING FIBROUS MATERIAL Original Filed May 16, 1966 4 Sheets-Sheet 4.
Fig.6.
( i ak Alli/ United States Patent 3,471,365 APPARATUS FOR IMPREGNATING FIBROUS MATERIAL Arne Johan Arthur Asplund, 11 Grevagen,
Bromma, Sweden Continuation of application Ser. No. 550,560, May 16,
1966. This application Aug. 7, 1967, Ser. No. 658,953
Int. Cl. D21c 7/00 US. Cl. 162-237 Claims ABSTRACT OF THE DISCLOSURE I Apparatus for treating lignocellulose-containing material for the production of paper pulp in which the lignocellulose-containing material is introduced into a steam treating chamber from which is conveyed into an impregnating chamber where it is subjected to steam and chemicals under elevated pressure, the steam treating chamber and the impregnating chamber being interconnected by a conduit in which the material is compressed incrementally into a series of plugs and sequentially discharged into the pressurized impregnating chamber where they expand to enhance the absorption of the impregnating chemicals.
This application is a continuation of Ser. No. 550,560 filed May 16, 1966, which is a division of application Ser. No. 237,911, filed Nov. 15, 1962, both now abandoned.
The raw material to be treated in accordance with the present invention is in the first instance constituted by wood disintegrated into chips; but also several varieties of grass, straw, bagasse and the like may be used with satisfactory results. The pulp is intended for use in the paper industry and also for the manufacture of fibre board and building elements or other products consisting of or containing such pulp.
According to the present invention, the raw material is subjected to an impregnation stage, at least one cooking step and a subsequent mechanical disintegration step. The impregnation step includes a mechanical compression of the material for partial elastic deformation and subsequent expansion thereof below the surface of chemicals containing liquid. Prior to the mechanical compression the material is heated to a temperature of 60 to 100 C. or even more, preferably by steam. By the compression, air and liquid present between the pieces of material, such as chips, and particularly within the pores of said material, is removed and when the mechanical compression ceases and the material is regaining its original volume, liquid is sucked into the pores. If the material in its raw state contains moisture exceeding 0.8 parts per one part of material calculated as completely dry, part of said moisture is pressed out which facilitates the subsequent impregnation with the chemicals-containing liquid.
According to one feature of my invention the expansion of the material within the liquid is effected while this liquid is subjected to an external superatmospheric pressure. The pressure to which the material is subjected during the expansion within the liquid may in this manner be increased to a many times larger pressure than the static pressure exerted by the liquid column itself onto the material. As a consequence, the remainder of air within the material is compressed and occupies a correspondingly minor volume for which reason the material will be capable of absorbing more liquid. If the container or conveyor within which the impregnation is made has so great height that the liquid column within the same is 8 metres, for example, the maximum of pressure exterted by the liquid column adjacent to the base of the container will be about 0.8 kilograms per square centimetre. According to the teaching of the present in- 3,471,365 Patented Oct. 7, 1969 ice vention, the pressure acting on the liquid may, without difiiculty be increased to ten times said value, for example, so as to cause the air remaining in the pores of the ligno-cellulose-containing material to be compressed to a corresponding small volume, which allows additional impregnation liquid to reach the interior of the material. The reduction of pressure in the pores of the materials caused by the upwardly directed movement of the material out of the liquid will become so inconsiderable, calculated in per cent, as to become negligible.
A feature of the invention resides in a plug-forming means by which the material being fed from one container to another is compressed against a pressure-regulatable wall, which can assume the form of a pivoted flap under hydraulic pressure to oppose the movement of the material to a predetermined extent until the material has built up into a plug of the desired density.
According to the present invention, the several cooking steps involved therein may employ the solutions of chemicals having mutually diiierent composition. For example, in the production of pulp by cooking wood chips in solutions of sodium sulphite which is quite neutral, the wood substance is affected by the organic acids usually present in said substances, such as formic acid and acetic acid. In order to avoid the hydrolysis thus caused, sodium carbonate or sodium hydroxide or possibly both or some other neutralizing substance are added.
With the above described objects and others to be hereinafter set forth in view, I have devised the arrangement of parts and method steps to be described and more particularly pointed out in the claims appended hereto.
In the accompanying drawings, wherein illustrative embodiments of the invention are disclosed,
FIG. 1 shows in elevation, and partly in section, a plant or carrying out the method according to my invention;
FIG. 2 is a sectional view, taken substantially on the line 22 of FIG. 1, looking in the direction of the arrows;
FIG. 3 shows in elevation and partly in section, a slightly different embodiment of the invention;
FIG. 4 shows in section, the remainder of the plant partly shown in FIG. 3;
FIG. 5 is a sectional view, taken on the line 5-5 of FIG. 4, and
FIG. 6 is an enlarged view, partly in section, of the mechanical compressing or plug-forming mechanism and associated parts.
Referring to the embodiment of the invention shown in FIGS. 1 and 2, there is therein shown a container 10 erected on a flooring 12 and extending vertically upwardly through a flooring 14 located at a higher level. The container 10 has an upper closure member 16, the upper end of which is formed with a steam outlet 18. Chips are supplied to the member 16 from a storage bin (not shown) through a duct 20 from which'the chips fall down into the container 10. If the supply of chips is too great, the excess returns through a duct 22 to the storage bin. Passing through the ducts 20 and 22 is a scraping conveyor (not shown). Steam is supplied to the container 10 through a pipe 24 connected to the lower part of the container and provided with a valve 26 and thus flows upwards in the opposite direction to the chips, descending within the container 10 for the purpose of producing a softening of said chips. The container 10 thus serves as a kind of zone for softening by means of steam within which zone the chips are gradually heated to a temperature exceeding 70 C. and suitably maintained between C. and C. and in some cases reaching the boiling point of water at atmospheric pressure. Any excess of steam may escape through the outlet 18, but the supply of steam through the pipe 24 is controlled so as to avoid such excess as far as possible.
The chips softened in the base zone are conveyed by a screw conveyor 29 located in the lower part of the container 10 and driven by an electric motor 27 through a reduction gear 28, into a plug-forming tube 30. Inside this tube is disposed a pivoted flap 31 (FIG. which, through the intermediary of an arm 32 is loaded by a hydraulic servo-motor 34 and thus assists in subjecting the mass of chips to high pressure. In this part of the apparatus the chips are compressed mechanically so as to expel air and water present in the pores of said chips. The air and water thus expelled from the chips passes out through apertures 29a provided in the lower portion of the frustoconical housing 30a for the screw conveyor 29. The water thus drained from the housing 30a descends into the receptacle 31a and is drained therefrom in any suitable way.
Mounted on the flooring 12 is another container 36 which also extends upwardly through the flooring 14. In the container 36 impregation of the chips is effected while the mass of chips is simultaneously conveyed up to the higher floor. On a still lower flooring 37 stands a vessel 38 within which a solution of chemicals is prepared and is conveyed to a pump 40 and through a pipe 42 up to a container 44 provided with a level control 46 which insures that the solution of chemicals is maintained at a predetermined constant level within this container. A tube 48 inter-connects the base parts of the containers 44 and 36 and thus in the container 36 a liquid column is formed reaching to substantially the same level as that in the container 44.
When the mass of chips is compressed strongly, for example, subjected to a high pressure of 30 to 50 or even to 100 atmospheres in the tube 30 enters the container 36 at its base, it will immediately enter a bath of the chemical solution. The chips expand towards their original volume and the solution is sucked into the pores of the chips. The preheating in the base section is intended to facilitate the compression in the plug-forming tube 30 and expansion takes place in the liquid-containing part of the container 36 which insures an extremely good impregnation of the chips with the chemical solution.
The chips are conveyed upwardly within the container 36 preferably by means of two screw conveyors 50, 52 (FIG. 2.) driven by an electric motor 49, the conveyors having a pitch preferably of the same magnitude as the diameter of the container and being rotated at a low number of rotations such as 5 to revolutions per minute. The spacing between the axes of the two screw conveyors should not be substantially larger than the sum of the radii of the screws and may possibly be less in order to produce an effect preventing rotational movement of the chips. To the same end, partitions 54 may be provided which are individually secured by welding and shaped to the periphery of the screws and designed to fill the areas adjacent the zones where the screws meet or engage one another.
The chips are conveyed upwardly by the screws 50, 52 initially below the level of the liquid in the container 36, and leave the liquid at the top part of the container 36 and are discharged from the container by means of a conveyor 56 extending in a transverse direction and located in the upper end portion of the container 36. The liquid column in the container 36 is dimensioned so as to produce a relatively high hydrostatic pressure adjacent the base of the container where the compressed chips are allowed to expand. This pressure may be of the order of 3 to 5 meters and may possibly reach 10 meters water column and assists in forcing the solution of chemicals into the pores of the chips.
This preliminary impregnation of the chips by the solution of chemicals is followed by a cooking or boiling of the chips. The conveyor 56 delivers the impregnated chips into a hopper-shaped vessel 58. From there the chips fall into a vibrating feeder 60 to a so-called rotating cell feeder 62 having individual pockets separated from one another, the chips content of which is delivered to a container 64 extending downwardly to the lowest flooring of the plant. The cell feeder is also so constructed as to prevent direct communication between the closed container 64 and the vibrating feeder 60. The pockets of the cell feeder when moving upwards during rotation, contain steam at high pressure, which steam escapes through a duct 66 provided with a centri-cleaner 68 to separate any entrained chips, and thence through a duct 70.
The lowermost flooring carries a container 72 of the same type as the container 38 and also intended for preparation of a solution of chemicals. This solution is fed by a pump 74 through a pipe 76 provided with a valve 78 controlled by a servo-motor 77 to the closed cooking container 64. The pipe 76 preferably opens near the middle portion of the container 64 to which steam is also sup plied at the base through a pipe 80 provided with a control valve 82. r
The cell feeder 62 is controlled by two systems of level regulators 84 which may be adjustably mounted on guides 86 and between which the level of the column of chips may fluctuate. The level of the solution of chemicals is also controlled by one or more systems of level regulators 88, which may be mounted on the same guides 86 and which actuate the servo-motor 77. In the cooking container 64 steam is maintained at a pressure of the order of 8 to 10 kg./cm. and at corresponding temperature. During their downward passage within the container 64 the chips initially meet a steam atmosphere and are subjected to cooking in said atmosphere while also being affected by the chemicals with which they were earlier impregnated. The chips subsequently descend into the chemical solution in the form of a column of liquid in the container 64 which may be greater in extent than the vapor space provided in said container. The cooking is continued in the liquid bath, the chips being progressively exposed to fresh solution of chemicals supplied from the container 72.
Adjacent to the base of the container 74 conveyors 90 driven through suitable transmission 94 by an electric motor 92 feed the chips to a further conveyor 96 opening into a container 98 standing adjacent to the container 64. Container 58 houses screw conveyors 100 driven by an electric motor 102. The container 98 and the conveyors 100 may be of the same construction as the container 36 and its screw conveyors. Within the container 98 the liquid will be at a level approximately the same or slightly higher than that within the container 64 and the cooking in the liquid phase is thus continued during the upwardly directed movement of the chips within the container 98. The container 98 which, in the same manner as the container 64, is closed and heat-insulated with respect to the surrounding atmosphere, has an upper vapor chamber within which a second cooking in the vapor phase may be effected.
The chips thus treated are fed from the top portion of the container 98 by a horizontal conveyor 104 to a mechanical disintegrator 106 provided with two grinding discs mutually rotatable and disposed within a zone 108 of the plant. The ground material or pulp then passes through a conduit 110 to a centri-cleaner 112 after which it may be subjected to further treatment such as a further mechanical grinding step. The defibrator 106 may suitably be of a known kind. The mechanical disintegration in the embodiment shown is effected subsequent to the last cooking step and under the same conditions regarding temperature and pressure. The disintegration may, however, also be effected under atmospheric conditions.
The embodiment of the invention disclosed in FIG. 3 is similar in most respects to that shown in FIG. 1, a primary difference being that the several containers 10, 36, 64 and 98 are arranged on the same flooring or level. These elements may have such longitudinal dimension as to project from the flooring 12 upwardly through higher fioorings 14 and 16 respectively. In this embodiment, the chips enter through duct 20 to the container through the vertical discharge tube a. The latter communicates with the container 10 through a rotating cell feeder 2211 having individual pockets separated from one another, the chips content of each of which is separately delivered to the container 10 through the top thereof. The cell feeder is in connection with a duct 24a through which steam or air present in the pockets escapes into the surrounding atmosphere during the movement of the pockets upwardly from the container 10. It is readily understood that the cell feeder 22 blocks free communication between the top portion of the vertical container 10 and the surrounding atmosphere. Steam flows upwardly in the container in a direction opposite to that of the chips descending within the container, the steam being introduced into the base portion of the container through the pipe 26 controlled by the valve 28. g
In the container 10 the raw material is preheated by means of steam to a temperature usually kept below 100 C. and reaching higher temperature in some cases to 120 to 130 C., or even more. Simultaneously with the heating of the chips by the steam, part of the air present in the individual in the pores thereof, or between the chips, is expelled. The cell feeder 22a provides for the feed of the air thus expelled from the container 10, to the conduit 24a. Within the container 10 atmospheric pressure, or a slighter pressure, may be maintained. The upper level of the column of chips in the container 10 may fluctuate and be controlled within limits defined by level regulators 62a in the known manner. These regulators are adjustably mounted on guides 32a and actuate the driving motor of the cell feeder.
The plug-forming mechanism located at the base of the container 10 is substantially similar to that shown in FIG. 6, except for the reversal of position of the hydraulic servo-motor 34. By means of this mechanism, the flap 31 forms a wall against which the material is compressed to form a plug of the desired density, the flap having a regulatable pressure opposing the material until the required build-up is attained and then allowing the material to move forwardly into the container 36. The materials proceed into the container 36 in the manner described in the previous embodiment of FIG. 1.
In the present embodiment, a solution of chemicals prepared in the vessel 38 is fed into the base part of the conveyor 36 through a tube 42a and pump unit 40. The tube 42a may be surrounded by a heating coil 60a to effect a heating of the solution flowing towards the container 36. Within the container 36 the liquid is caused to rise to a level controlled by the level regulators 36a, which in the illustrated embodiment of the apparatus, as shown in FIG. 3, actuate the pump 49. In this embodiment the horizontal conveyor 64 to the cooker 64 which has a vertical dimension of substantially the same magnitude as the container 10 and the container 36 respectively. The quantity of chips housed in the cooker 64 is controlled by level regulators 84 which in turn govern the feeding speed of the screw feeder 29. Solution of chemicals is supplied to the cooker 64 from a storage vessel 72 through the tube 76 provided with the pump 74 and a valve 78 controlled by the servoactuated motor 77. The tube 76 may open into the cooker 64 substantially in the middle zone thereof. The level regulator 88 positioned below the regulator 84 is intended to actuate the servo-motor 77 to effect control of the liquid level within the cooker 64. Said regulators are mounted adjustably in the vertical direction on guides 86. Steam under pressure, as described in conjunction with FIG. 1, is supplied to the cooker 64 through a conduit 82 controlled by a valve 84a. Air collecting in the system may be intermittently removed through an escape tube 86a controlled by a valve 87a.
When the chip material strongly compressed within the plug-forming tube 38 expands again in the base part of the conveyor-container 36 chemicals containing solution is sucked up into the pores of the material. At the same time the chips areexposed to an elevated pressure which partly is determined by the liquid column formed in the container 36 and partly by the vapor pressure produced in the top part of said container. This latter pressure may be more than ten times larger than the pressure exerted by the liquid column. As a result, the air still present in the pores of the chips will be compressed to a corresponding degree and replaced by solution of chemicals so as to insure an almost perfect impregnation of the chips.
The chemicals containing liquid admitted to the container 36 has preferably a relatively low temperature such as to C. in order to avoid heating of the raw material to higher temperatures prior to its thorough impregnation with the chemicals containing liquid. If, however, the disadvantageous effects caused by high temperatures such as alteration of color of the pulp into brown, beginning hydrolysis or similar effects are negligible, the liquid when pumped into the container 36 may have a temperature of 150 to 180 C. and even a still higher temperature.
In the portion of the container 36 located above the regulators 36a and also in the portion of the cooker 64 above the regulator 88 an atmosphere of water vapor is formed. The impregnated chips are thus initially subjected to cooking in a vapor phase and are subsequently cooked in a liquid phase formed in the zone of the cooker 64 located below the regulator 88.
From the base portion of the container or cooker 64 the chips are conveyed into the container or conveyor 98 as described in connection with FIG. 1.
In the illustrated apparatus, all reaction vessels or containers 10, 36, 64 and 98 may be interconnected to equalize the pressure prevailing therein. To this end the pressure-equalizing tube 103 has branch connection tubes 128, to the containers 36 and 10 respectively. For each of the tubes controlling valves denoted by 132, 134, 136, and 138 respectively, are provided. A valve con trols a tube 142 through which water vapor may be supplied or which may also serve as a discharge conduit. In the various containers the same pressure may thus be maintained, or if desired, pressure differences may be produced if the containers by suitable adjustment of the valves.
The ligno-cellulose-containing material treated in this way may be directly blown out into the centri-cleaner 112 (FIG. 4) or any other suitable receiving apparatus. In the embodiment shown in FIG. 4, a mechanical disintegrating apparatus 106 constructed as a disc refiner, for example, is interposed ahead of said cleaner. The discharge side of the apparatus 106 is connected with the centricleaner 112 through conduit 110 and behind the centri-cleaner a conveyor transports the materials to a hopper 151 forming part of a de-Watering device 114, from which the cooking liquid expelled by compression is drawn off through a tube 116 whereas the pulp product is discharged by means of a conveyor 118. This product may be diluted with water in a vessel 120 and is refined in a second disc refiner 122 whereupon it is fed into a storage vessel 124 to be conveyed further to a papermaking machine by means of a pulp pump 126, for example.
The chemicals used in the treatment of the lignocellulose-containing material may be of any known kind and have suitably mutually different composition in the liquids used in the impregnating steps. The impregnating liquid in the container 36 may substantially consist of sodium sulphite and sodium carbonate in the presence of which chemicals, the treatment in the vapor phase within the upper zones of the container 36 and the cooker 64 is effected. The cooking liquid prepared in the container 38 may contain sodium sulphite and sodium hydroxide or sodium sulphide. The particular composition employed may be used in both embodiments of the invention.
If a higher pressure is maintained in the container 36 than in the container 10 a plug of material formed in the feeding device 29 to 34 is normally suificient to act as a barrier preventing vapor and liquid from escaping through said device. If, however, this barrier for some reason or other should cease to be operative and as a consequence the pressure in the container 10 should rise, the cell feeders 22a will prevent raw material, liquid and vapor from escaping out of the system which means that open communication between the system operating under high pressure and the surrounding atmosphere will not be established under such conditions.
What is claimed is:
1. An apparatus for treating lignocellulose-containing fibrous material for the production of paper pulp, including:
(a) a steam treating chamber;
(b) conveying means opening into said steam treating chamber and feeding the lignocellulose-containing material in the form of particles into an upper portion of said chamber;
(c) a conduit means connected to said chamber and a steam source connected to said conduit for introducing steam into said chamber;
((1) an elongated, upwardly extending, impregnating chamber and a second conduit means connected thereto feeding impregnating chemicals into said chamber, said chamber having a substantial volume of impregnating chemical therein;
(e) means for feeding chemicals to said second conduit means;
(f) means exteriorly of said impregnating chamber and opening thereinto for creating an elevated pressure on the impregnating chemical in the lower portion of said chamber;
(g) a material conduit interconnecting the lower portions of said two chambers;
(h) means in said conduit for receiving fibrous material from said steam treatment chamber, for compressing said material incrementally into a series of plugs, and for sequentially discharging each plug into said pressurized impregnating chamber, whereby said fibrous material expands and absorbs impregnating chemicals;
(i) conveyor means for conveying the expanded and impregnated material upwardly in said impregnating chamber; and
(j) outlet means in the upper portion of said impregnating chamber for discharging the impregnated material.
2. A structure as set forth in claim 1, wherein said means in (f) for creating an elevated pressure in the lower portion of said impregnating chamber comprises:
(a) a pressure tight cooking chamber having a steam source connected thereto, and a material inlet; and
(b) a pressure sealed transfer conduit extending .rom
said material inlet to said outlet means of said impregnating chamber.
3. An apparatus for treating lignocellulose-containing fibrous material for the production of paper pulp, including (a) a steam treating chamber;
(b) conveying means opening into said steam treating chamber and feeding the lignocellulose-containing material in the form of particles into an upper portion of said chamber;
(c) a conduit means connected to said chamber and a steam source connected to said conduit for introducing steam into said chamber;
(d) an elongated, upwardly extending, impregnating chamber and a second conduit means connected thereto feeding impregnating chemicals into said chamber, said chamber having a column of impregnating chemical therein exerting an elevated hydrostatic pressure in the lower portion of said chamber;
(e) means for feeding chemicals to said second conduit means;
(f) a material conduit interconnecting the lower portions of said two chambers;
(g) means in said conduit for receiving fibrous material from said steam treatment chamber, for compressing said material incrementally into a Series of plugs, and for sequentially discharging each plug into said pressurized impregnating chamber, whereby said fibrous material expands and absorbs impregnating chemicals;
(h) conveyor means for conveying the expanded and impregnated material upwardly in said impregnating chamber; and
(i) outlet means in the upper portion of said impregnating chamber for discharging the impregnated material.
4. Apparatus as set forth in claim 3, wherein said means (g) further includes means to drain oif liquid discharged from said fibrous plugs by said compression.
5. Apparatus as set forth in claim 3, wherein said means (g) includes a continuous conveyor in said passage, a plate movable into and out of blocking position relative to said passage, and force means biasing said plate toward blocking position but releasing said plate when the compression of said fibrous plug reaches a desired maximum.
6. An apparatus for treating lignocellulose-containing fibrous material for the production of paper pulp, including (a) a steam treating chamber;
(b) conveying means opening into said steam treating chamber and feeding the lignocellulose-containing material in the form of particles into an upper portion of said chamber;
(c) a conduit means connected to said chamber and a steam source connected to said conduit for introducing steam into said chamber;
(d) an elongated, upwardly extending, impregnating chamber and a second conduit means connected thereto feeding impregnating chemicals into said chamber, said chamber having a column of impregnating chemical therein exerting an elevated, hydrostatic pressure in the lower portion of said chamber;
(e) means for feeding chemicals to said second conduit means;
(f) a material conduit interconnecting the lower portions of said two chambers;
(g) conveyor means in said conduit receiving fibrous material from said steam treatment chamber and forcing said material into a compression chamber to thereby form a compressed plug, said compression chamber having a movable blocking means blocking the outlet thereof;
(h) a force means acting on said blocking means to bias it into blocking position but releasable when said compressed plug has reached a preset pressure to suddenly eject said plug into said impregnating chamber whereby said fibers are expanded and impregnated;
(i) conveying means for conveying the thus expanded and impregnated material upwardly in said impregnating chamber; and
(j) outlet means in the upper portion of said impregnating :chamber for discharging the impregnated material.
7. An apparatus as set forth in claim 6, wherein said compression chamber further includes means to drain off liquid discharge from said fibrous plugs by said compression.
9 10 8. A structure as set forth in claim 6 wherein Said in said cooking chamber, and a material inlet; and blocking means comprises a pivoted plate and said force (b) a sealed, pressure tight, transfer conduit extendmeans comprises a piston and cylinder acting on said ing between and connected to said outlet means from plate, the force exerted by said cylinder being adjustsaid impregnating chamber and said material inlet of able. 5 said cooking chamber,
9. A structure as set forth in claim 3, further including whereby said elevated steam pressure will increase (a) a sealed cooking chamber having a steam source the pressure on the impregnating chemical in said connected thereto providing an elevated pressure impregnating chamber. in said cooking chamber, and a material inlet; and (b) a sealed, pressure tight, transfer conduit extend- 10 References Cited ing between and connected to said outlet means UNITED STATES PATENTS friam sa1d impregnating chamber and sa1d materlal 2,008,892 7/1935 Asplund 162 18 1n et of sa1d cooking chamber, whereby said elevated steam pressure will increase 2093267 9/1937 Dunbar 162237 X the pressure on the impregnating chemical in said 15 2905240 9/1959 sandbelg 162-19 X impregnating chamber. 10. A structure as set forth in claim 6, further including (a) a sealed cooking chamber having a steam source connected thereto providing an elevated pressure 20 HOWARD R. CAINE, Primary Examiner US. Cl. X.R.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US65895367A | 1967-08-07 | 1967-08-07 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US3471365A true US3471365A (en) | 1969-10-07 |
Family
ID=24643422
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US658953A Expired - Lifetime US3471365A (en) | 1967-08-07 | 1967-08-07 | Apparatus for impregnating fibrous material |
Country Status (1)
| Country | Link |
|---|---|
| US (1) | US3471365A (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3619348A (en) * | 1969-09-05 | 1971-11-09 | Defibrator Ab | Process for continuous cellulose cooking |
| US4096027A (en) * | 1976-02-19 | 1978-06-20 | Kamyr Inc. | System for presteaming wood chips at or near atmospheric pressure with minimum displacement of air |
| US4124440A (en) * | 1977-05-23 | 1978-11-07 | Kamyr Inc. | Chip bin steam distributor with a vibrating discharge |
| EP0161330A1 (en) * | 1984-05-01 | 1985-11-21 | Oliver Armas Laakso | Chip presteaming and air washing |
| US5172867A (en) * | 1991-09-09 | 1992-12-22 | Kamyr, Inc. | Utilization of a paper pulp digester as a structural support |
| WO1997040194A1 (en) * | 1996-04-25 | 1997-10-30 | Union Camp Corporation | Improved method for biological pretreatment of wood chips |
| US20100317053A1 (en) * | 2009-06-15 | 2010-12-16 | Andritz Inc. | Process machinery for feeding pre-treated lignocellulosic materials into bioreactors for bio-fuels and biochemicals |
| US9644317B2 (en) | 2014-11-26 | 2017-05-09 | International Paper Company | Continuous digester and feeding system |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2008892A (en) * | 1932-03-29 | 1935-07-23 | Defibrator Ab | Method of manufacture of pulp |
| US2093267A (en) * | 1934-11-20 | 1937-09-14 | Chemipulp Process Inc | Treatment of fibrous material |
| US2905240A (en) * | 1954-12-10 | 1959-09-22 | Waldorf Paper Prod Co | Apparatus for impregnating wood chips |
-
1967
- 1967-08-07 US US658953A patent/US3471365A/en not_active Expired - Lifetime
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2008892A (en) * | 1932-03-29 | 1935-07-23 | Defibrator Ab | Method of manufacture of pulp |
| US2093267A (en) * | 1934-11-20 | 1937-09-14 | Chemipulp Process Inc | Treatment of fibrous material |
| US2905240A (en) * | 1954-12-10 | 1959-09-22 | Waldorf Paper Prod Co | Apparatus for impregnating wood chips |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3619348A (en) * | 1969-09-05 | 1971-11-09 | Defibrator Ab | Process for continuous cellulose cooking |
| US4096027A (en) * | 1976-02-19 | 1978-06-20 | Kamyr Inc. | System for presteaming wood chips at or near atmospheric pressure with minimum displacement of air |
| US4124440A (en) * | 1977-05-23 | 1978-11-07 | Kamyr Inc. | Chip bin steam distributor with a vibrating discharge |
| EP0161330A1 (en) * | 1984-05-01 | 1985-11-21 | Oliver Armas Laakso | Chip presteaming and air washing |
| US4632729A (en) * | 1984-05-01 | 1986-12-30 | Laakso Oliver A | Chip presteaming and air washing |
| US5172867A (en) * | 1991-09-09 | 1992-12-22 | Kamyr, Inc. | Utilization of a paper pulp digester as a structural support |
| WO1997040194A1 (en) * | 1996-04-25 | 1997-10-30 | Union Camp Corporation | Improved method for biological pretreatment of wood chips |
| US20100317053A1 (en) * | 2009-06-15 | 2010-12-16 | Andritz Inc. | Process machinery for feeding pre-treated lignocellulosic materials into bioreactors for bio-fuels and biochemicals |
| US9644317B2 (en) | 2014-11-26 | 2017-05-09 | International Paper Company | Continuous digester and feeding system |
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