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US2598102A - Heat insulating material - Google Patents

Heat insulating material Download PDF

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Publication number
US2598102A
US2598102A US6614148A US2598102A US 2598102 A US2598102 A US 2598102A US 6614148 A US6614148 A US 6614148A US 2598102 A US2598102 A US 2598102A
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US
United States
Prior art keywords
magnesia
fibers
fiberglass
binder
slag wool
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
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Inventor
Baxter Mason
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JAMES D AKINS
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JAMES D AKINS
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Publication date
Application filed by JAMES D AKINS filed Critical JAMES D AKINS
Priority to US6614148 priority Critical patent/US2598102A/en
Application granted granted Critical
Publication of US2598102A publication Critical patent/US2598102A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • CCHEMISTRY; METALLURGY
    • C04CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04BLIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B30/00Compositions for artificial stone, not containing binders
    • C04B30/02Compositions for artificial stone, not containing binders containing fibrous materials
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02WCLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W30/00Technologies for solid waste management
    • Y02W30/50Reuse, recycling or recovery technologies
    • Y02W30/91Use of waste materials as fillers for mortars or concrete

Definitions

  • the present invention relates to improvements in heat insulating material, and has particular reference to a binder for such materials as magnesia, diatomaceous earth, calcium silicate and others of similar character.
  • the principal object of the invention is to provide a binder comprising fiberglass fiber and slag wool pellets combined in such a manner that the fiberglass will embed itself into and through the slag wool pellets and will cling thereto so that the two can be mixed with an aqueous suspension containing any one of the above-mentioned materials and will be dispersed throughout the mixture, the pellets serving to hold the fiberglass fibers in suspension and to cause their uniform distribution in a promiscuous arrangement throughout the mass and to be held in this arrangement until the whole mixture can be dried by heat or by air.
  • This allows the fiberglass fiber which has great strength to act as a binder that will hold the mass in solid form, while the slag wool primarily serves as an agent to separate and hold in suspension the fiberglass fiber.
  • the principal binder used at the present time in connection with magnesia is asbestos fiber which in the well-known product known as 85% magnesia is mixed into the magnesia in the proportions of approximately 15% of asbestos fiber to 85% of magnesia.
  • This binder is also largely used in connection with diatomaceous earth and other insulating materials.
  • This mixture, heat dried, when removed from the molds is very white and has an appearance that is remarkably similar to the present forms of 85% magnesia.
  • diatomaceous earth would provide an insulation of greater range, it is slightly heavier and does not have the extremely white color that is very desirable.
  • the resulting mixture which I refer to as a binder, is then mixed into an aqueous suspension containing magnesia, diatomaceous earth, calcium silicate or any other suitable insulating materials and will disperse throughout this mixture, the slag wool serving to hold the glass fibers in suspension until the whole mixture can be dried by heat or by air.
  • I preferably use the binder and the insulating material in approximately equal proportions.
  • the mixing can be accomplished by any suitable machinery conventionally used for this purpose.
  • the pre-mixing of the fiberglass fibers with the slag wool pellets tends to keep the fibers separate and in suspension during the final mixing process with the insulating material, and the thorough distribution of the fiberglass fibers through the final product eliminates shrinkage and cracking in the drying process as well as in the later use of the material.
  • My final product provides an efiicient and strong insulation capable of resisting a high temperature range.
  • My binder can also readily be used with cement in the manufacture of shingles and boards or in ply of wool.
  • a binder for magnesia and the like comprising an intimate mixture of fiberglass fibers having great strength and heat resistance and suflicient affinity for each other to prevent their free dispersion in an aqueous solution of the magnesia, and slag wool pellets having fibers of less strength and heat resistance, said fiberglass fibersbeingembeddedin, through and around the V slag wool pelletsin a substantiallycomplete state of"v dispersion whereby the -'-fiberglass-- fibers are prevented from matting when the binder is mixed in anaqueoussolution ofthe said magnesia.
  • a heat insulating body comprising as major, ingredients magnesia and a binder, comprisingian intimate mixture-offiberglass fibers having "great-- strength and heat resistance and sufficient ;affinityioreach other to prevent their free dispersion in an aqueous solution of the magnesia, and slag wool pellets having fibers of less strength and heat resistance, said fiberglass fibers being embedded in, through and around the slag wool pellets in a substantially complete state of dispersion whereby the fiberglass fibers are prevented from matting when the binder is mixed in'an aqueous solutionof the :said magnesia.

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Porous Artificial Stone Or Porous Ceramic Products (AREA)

Description

Patented May 27, 1952 HEAT INSULATING MATERIAL Mason Baxter, San Francisco, Calif., assignor to James D. Akins, Los Angeles, Calif.
No Drawing. Application December 18, 194
Serial No. 66,141
Claims. (Cl. 106-121) The present invention relates to improvements in heat insulating material, and has particular reference to a binder for such materials as magnesia, diatomaceous earth, calcium silicate and others of similar character.
The principal object of the invention is to provide a binder comprising fiberglass fiber and slag wool pellets combined in such a manner that the fiberglass will embed itself into and through the slag wool pellets and will cling thereto so that the two can be mixed with an aqueous suspension containing any one of the above-mentioned materials and will be dispersed throughout the mixture, the pellets serving to hold the fiberglass fibers in suspension and to cause their uniform distribution in a promiscuous arrangement throughout the mass and to be held in this arrangement until the whole mixture can be dried by heat or by air. This allows the fiberglass fiber which has great strength to act as a binder that will hold the mass in solid form, while the slag wool primarily serves as an agent to separate and hold in suspension the fiberglass fiber.
The principal binder used at the present time in connection with magnesia is asbestos fiber which in the well-known product known as 85% magnesia is mixed into the magnesia in the proportions of approximately 15% of asbestos fiber to 85% of magnesia. This binder is also largely used in connection with diatomaceous earth and other insulating materials.
It appears, however, that the supply of asbestos fiber is rather limited and is not sufficient to keep up with the demand due to the tremendous expansion of the industry. Although there are other fibers of an organic nature which are capable of providing the strength necessary to bind the insulation, they usually are not capable to resist the temperature which a good insulation must protect.
There is, however, one fiber which has both the necessary strength and the desired resistance to high temperatures, and that is fiberglas fiber. Up to the present time, however, no one has been able to find a way to keep this fiber tin suspension when mixed with an aqueous solution. The fiberglass fiber has a high affinity for itself and is difiicult to separate, and will mat and flow together when wet.
With this in mind, and having noted the even higher afiinity that fiberglass has for slag wool, I
the solution with which it is mixed. Accordingly, using the granulated type of wool, handrolled over a wire screen to further separate the very small shot pellets, and mixing it with the proper lengths of fiberglass fibers, I found that theglass fiber would separate even further into many thousands of strands and would imbed itself into, around and through the pellets of slag wool in such a manner that the mixture could be wet and mixed with magnesiaor diatomaceous earth and then poured or forced into molds.
This mixture, heat dried, when removed from the molds is very white and has an appearance that is remarkably similar to the present forms of 85% magnesia. Although the use of diatomaceous earth would provide an insulation of greater range, it is slightly heavier and does not have the extremely white color that is very desirable.
In carrying out my invention, I mix, by hand or by the use of suitable machinery, fiberglass fibers of approximately inch length with slag wool pellets in such a manner that the fiberglass will imbed itself into, through and around the slag wool pellets and will cling thereto in the form of extremely fine strands uniformly distributed through the slag wool pellets in promiscuous order. While I do not desire to limit myself to any specific proportions, I preferably use about one pound of fiberglass fiber to fifty pounds of slag wool. The resulting mixture, which I refer to as a binder, is then mixed into an aqueous suspension containing magnesia, diatomaceous earth, calcium silicate or any other suitable insulating materials and will disperse throughout this mixture, the slag wool serving to hold the glass fibers in suspension until the whole mixture can be dried by heat or by air. In forming the latter mixture I preferably use the binder and the insulating material in approximately equal proportions. The mixing can be accomplished by any suitable machinery conventionally used for this purpose.
The pre-mixing of the fiberglass fibers with the slag wool pellets tends to keep the fibers separate and in suspension during the final mixing process with the insulating material, and the thorough distribution of the fiberglass fibers through the final product eliminates shrinkage and cracking in the drying process as well as in the later use of the material. My final product provides an efiicient and strong insulation capable of resisting a high temperature range.
My binder can also readily be used with cement in the manufacture of shingles and boards or in ply of wool. By'comparison with 85% -mag-' nesia, I believe that a product using wool and magnesia would have a lower K factor, a better' temperature range, lower costs of produc:
tion, and less shrinkage in the manufacture and,
when used at high temperatures.
1 claim:
1. A binder for magnesia and the like, comprising an intimate mixture of fiberglass fibers having great strength and heat resistance and suflicient affinity for each other to prevent their free dispersion in an aqueous solution of the magnesia, and slag wool pellets having fibers of less strength and heat resistance, said fiberglass fibersbeingembeddedin, through and around the V slag wool pelletsin a substantiallycomplete state of"v dispersion whereby the -'-fiberglass-- fibers are prevented from matting when the binder is mixed in anaqueoussolution ofthe said magnesia.
2; Aibi-nder as-defined in claim 1 in which the ingredients-are mixed substantially in the proportiorr of one pound of fiberglass-fibers to fifty pounds I of slag -;woolpellets.
8. A heat insulating body comprising as major, ingredients magnesia and a binder, comprisingian intimate mixture-offiberglass fibers having "great-- strength and heat resistance and sufficient ;affinityioreach other to prevent their free dispersion in an aqueous solution of the magnesia, and slag wool pellets having fibers of less strength and heat resistance, said fiberglass fibers being embedded in, through and around the slag wool pellets in a substantially complete state of dispersion whereby the fiberglass fibers are prevented from matting when the binder is mixed in'an aqueous solutionof the :said magnesia.
4. A heat insulating body as defined in claim 3 in which the magnesia and the binder are mixed in about equal proportions by weight.
5. A heat insulating body as defined in claim 3, in'which the fiberglass fibers and the slag wool 1' pellets in the binder are mixed substantially in the proportions of one to fifty by weight.
MASON BAXTER.
REFERENCES CITED The following references are of record in the filfeoi this-patent:
UNITED STATES PATENTS Number Name Date 1,960,880 Smith May 29, 1934 1,996,082 Powell Ap a. 2, 1935 Re. 19,919. Rechtner Apr. f7, 1936 2,060,295, Finefr'ock Nov., 10,1936 2,477,555. Roberts, July, 26,1949,
FOREIGN" PATENTS Number Country Date 457,523 Great Britain 1936 830,030, France 193 8

Claims (1)

  1. 3. A HEAT INSULATING BODY COMPRISING AS MAJOR INGREDIENTS MAGNESIA AND A BINDER, COMPRISING AN INTIMATE MIXTURE OF FIBERGLASS FIBERS HAVING GREAT STRENGTH AND HEAT RESISTANCE AND SUFFICIENT AFFINITY FOR EACH OTHER TO PREVENT THEIR FREE DISPERISION IN AQUEOUS SOLUTION OF THE MAGNESIA, AND SLAG WOOL PELLETS HAVING FIBERS OF LESS STRENGTH AND HEAT RESISTANCE, SAID FIBERGLASS FIBERS BEING EMBEDDED IN, THROUGH AND AROUND THE SLAG WOOL PELLETS IN A SUBSTANTIALLY COMPLETE STATE OF DISPERSION WHEREBY THE FIBERGLASS FIBERS ARE PREVENTED FROM MATTING WHEN THE BINDER IS MIXED IN AN AQUEOUS SOLUTION OF THE SAID MAGNESIA.
US6614148 1948-12-18 1948-12-18 Heat insulating material Expired - Lifetime US2598102A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2703762A (en) * 1951-04-28 1955-03-08 Owens Corning Fiberglass Corp Reinforced inorganic molded products
US2781274A (en) * 1951-04-28 1957-02-12 Owens Corning Fiberglass Corp Reinforced inorganic molded products
US3110545A (en) * 1958-12-01 1963-11-12 Horizons Inc Inorganic fibers and preparation thereof
US20080211134A1 (en) * 2006-11-08 2008-09-04 Outotec Oyj Method and apparatus for making spiral separators using sequential heating and cooling

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1960880A (en) * 1933-02-01 1934-05-29 Coast Insulating Company Acoustical material
US1996082A (en) * 1931-08-26 1935-04-02 Johns Manville Mineral wool product and method of making same
USRE19919E (en) * 1936-04-07 Composition material
US2060295A (en) * 1934-06-22 1936-11-10 American Gypsum Co Acoustical or insulating plaster
GB457523A (en) * 1935-05-27 1936-11-27 Noel Phillips Improvements in or relating to moulding mixtures
FR830030A (en) * 1936-10-07 1938-07-19 Material and articles composed of hydraulic binders and fibrous substances
US2477555A (en) * 1944-08-18 1949-07-26 Owens Corning Fiberglass Corp Mineral fiber mat and process of manufacture

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
USRE19919E (en) * 1936-04-07 Composition material
US1996082A (en) * 1931-08-26 1935-04-02 Johns Manville Mineral wool product and method of making same
US1960880A (en) * 1933-02-01 1934-05-29 Coast Insulating Company Acoustical material
US2060295A (en) * 1934-06-22 1936-11-10 American Gypsum Co Acoustical or insulating plaster
GB457523A (en) * 1935-05-27 1936-11-27 Noel Phillips Improvements in or relating to moulding mixtures
FR830030A (en) * 1936-10-07 1938-07-19 Material and articles composed of hydraulic binders and fibrous substances
US2477555A (en) * 1944-08-18 1949-07-26 Owens Corning Fiberglass Corp Mineral fiber mat and process of manufacture

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2703762A (en) * 1951-04-28 1955-03-08 Owens Corning Fiberglass Corp Reinforced inorganic molded products
US2781274A (en) * 1951-04-28 1957-02-12 Owens Corning Fiberglass Corp Reinforced inorganic molded products
US3110545A (en) * 1958-12-01 1963-11-12 Horizons Inc Inorganic fibers and preparation thereof
US20080211134A1 (en) * 2006-11-08 2008-09-04 Outotec Oyj Method and apparatus for making spiral separators using sequential heating and cooling

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