US20090100846A1 - Cryogenic freeze chamber assembly - Google Patents
Cryogenic freeze chamber assembly Download PDFInfo
- Publication number
- US20090100846A1 US20090100846A1 US11/975,976 US97597607A US2009100846A1 US 20090100846 A1 US20090100846 A1 US 20090100846A1 US 97597607 A US97597607 A US 97597607A US 2009100846 A1 US2009100846 A1 US 2009100846A1
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- United States
- Prior art keywords
- chamber
- assembly
- feedstock
- accordance
- chamber assembly
- Prior art date
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- 238000007710 freezing Methods 0.000 claims abstract description 12
- 230000008014 freezing Effects 0.000 claims abstract description 12
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- 239000007921 spray Substances 0.000 claims description 19
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Images
Classifications
-
- F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
- F25—REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
- F25D—REFRIGERATORS; COLD ROOMS; ICE-BOXES; COOLING OR FREEZING APPARATUS NOT OTHERWISE PROVIDED FOR
- F25D3/00—Devices using other cold materials; Devices using cold-storage bodies
- F25D3/10—Devices using other cold materials; Devices using cold-storage bodies using liquefied gases, e.g. liquid air
- F25D3/11—Devices using other cold materials; Devices using cold-storage bodies using liquefied gases, e.g. liquid air with conveyors carrying articles to be cooled through the cooling space
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29B—PREPARATION OR PRETREATMENT OF THE MATERIAL TO BE SHAPED; MAKING GRANULES OR PREFORMS; RECOVERY OF PLASTICS OR OTHER CONSTITUENTS OF WASTE MATERIAL CONTAINING PLASTICS
- B29B17/00—Recovery of plastics or other constituents of waste material containing plastics
- B29B17/04—Disintegrating plastics, e.g. by milling
- B29B17/0404—Disintegrating plastics, e.g. by milling to powder
- B29B17/0408—Disintegrating plastics, e.g. by milling to powder using cryogenic systems
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/50—Reuse, recycling or recovery technologies
- Y02W30/62—Plastics recycling; Rubber recycling
Definitions
- the present invention is directed to a cryogenic freeze chamber assembly. More specifically, the present invention is directed to a cryogenic freezing chamber assembly which more efficiently chills polymeric particles so that those particles can be effectively comminuted.
- Cryogenic freeze chamber assemblies are extensively utilized in the processing of solid materials which have high impact resistance. That is, solids which resist fracture during comminution processes represent a major obstacle to reprocessing of solid materials.
- the reprocessing of solid materials is an ever more important commercial and environment undertaking.
- a prime example of such materials is vehicle tires. Tires, principally formed of rubber, are excellent examples of impact resistant solids whose comminution is difficult unless its temperature is reduced below the glass transition point. The removal of used tires is very important to good environmental practice and the comminution product, crumb and powder rubbers, represent valuable commercial products.
- cryogenic freeze chamber assemblies Although the utilization of cryogenic freeze chamber assemblies has become more common with the advent of solid comminution processing, present cryogenic freezing chamber assemblies have certain inefficiencies that call for improved design.
- cryogenic freeze chamber assemblies A major concern in the design of cryogenic freeze chamber assemblies is to effectively cool impact resistant particles with minimum use of cryogenic fluid. Indeed, the cost of the cryogenic fluid is probably the major variable cost in the process of comminuting solids. Thus, a design which results in significant reduction in the utilization of cryogenic fluid represents a major aim of artisans working in this art.
- cryogenic freeze chamber assemblies known in the art is meeting the requirement of providing adequate structural strength to withstand stress imposed on chamber assemblies due to the effect of thermal expansion and contraction. Obviously, the utilization of very cold temperatures makes this design aspect of prime importance in the successful and continuous operation of such an assembly.
- Cryogenic freeze chamber assembles designs of the prior art are used in association with redundant apparatus to remove foreign particles present in the feedstock stream. This is due not only to the difficulty of removing foreign particles from such assemblies but, also, to be able to remove such foreign particles from the chamber assembly once they are removed from the feedstock stream.
- a new cryogenic freeze chamber assembly has now been developed which solves many structural and design problems associated with cryogenic freeze chamber assemblies of the prior art.
- the newly developed cryogenic freeze chamber assembly addresses the issue of structural integrity effectuated by thermal expansion and contraction.
- the chamber assembly is fixed at its center to allow movement toward each end rather than the prior art design of concentrating total expansion and contraction at one end. This fixing of the chamber assembly at its center allows for movement toward each end thus minimizing the interfacial stress between stationery interconnecting flexible joints and the chamber assembly.
- cryogenic freeze chamber assembly of the present invention Another aspect of the cryogenic freeze chamber assembly of the present invention is improved utilization of cryogenic fluid.
- Cryogenic fluid is introduced into the freeze chamber assembly in two distinct patterns. The first is a continuous or pulsating spray directed upon the feedstock stream transmitted through the chamber assembly. This spray is controlled as a function of the chamber assembly operating temperature. The second spray is positioned and directed at the multiple and distinct rivulets of falling feedstock particles elevated by rotating agitators. As such, the second of the two cryogenic fluid introductions is limited to specific intervals of time when such introduction effectuates total contact with the total particle surface, maximizing the cooling effect of the cryogenic fluid.
- the view-ports which permits viewing of the immediate area about the portion of the chamber within view of the port. Since these view-ports are strategically placed throughout the length of the chamber assembly, the total chamber assembly can be viewed during operation. To insure effectiveness, means to prevent fogging, caused by the cryogenic temperature, the view-ports are provided with heating means in communication with the glass viewing area of the view-port. This heating is automatically effectuated when the view-port cover is opened for viewing.
- the chamber assembly of this invention is designed to permit vertical removal of interior components which simplifies repair and maintenance by vertical replacement of components compared to the horizontal removal of interior components required by freeze chamber assemblies of the prior art.
- Yet another advance associated with the present chamber assembly is a self-contained means for removal of foreign materials present in the feedstock.
- this advance means are provided for removal of foreign materials from the feedstock at the chamber assembly inlet prior to freezing.
- This advance is especially important when the feedstocks are obtained from processed tires or other material which contains fugitive ferrous metal.
- the removal of ferrous metal is important to the reliability and efficiency of not only the freeze chamber assembly but also for the protection of downstream equipment. This is accomplished by the inclusion of magnetic means at the feedstock inlet to attract and remove ferrous metal particles from the feedstock entering the chamber.
- cryogenic freezing chamber assembly in accordance with the present invention cryogenic freezing chamber assembly is provided.
- the assembly includes an elongated chamber, an inlet means for introducing feedstock therein, an inlet means for introducing a cryogenic fluid into the chamber and fixed mounting means disposed midway between the ends of the elongated chamber assembly.
- the chamber assembly includes an elongated chamber, a cryogenic fluid inlet means, a feedstock inlet means, an outlet means for removing feedstock from the chamber and a plurality of view-ports disposed on the chamber surface wherein the view-ports are provided with heating means to maximize clear viewing.
- a cryogenic freeze chamber assembly which includes an elongated chamber, a rotating auger disposed in the chamber, an inlet means for introducing feedstock onto the auger, disposed in the chamber, wherein the auger contains, transports and agitates the feedstock particles, cryogenic fluid introductory means responsive to means provided on the rotating auger for introducing cryogenic fluid into the chamber and feedstock outlet means for removal of the feedstock from the chamber.
- a cryogenic freeze chamber assembly is drawn to an elongated chamber, a feedstock inlet means for introducing feedstock into the chamber, a cryogenic fluid inlet means for introducing cryogenic fluid into the chamber, a feedstock outlet means for removing feedstock below its glass transition temperature from the chamber and a rotating auger, supported by and rotating about end bearing assemblies for transmitting the feedstock from the feedstock inlet means to the feedstock outlet means.
- FIG. 1 is a front sectional view of a cryogenic freeze chamber assembly in accordance with the present invention
- FIG. 2 represents three views of a magnetic bar screen assembly of the cryogenic freeze chamber assembly.
- FIGS. 2 a , 2 b and 2 c provide plan, front elevation and side elevation cross-sectional views, respectively, of the magnetic bar screen assembly;
- FIG. 3 provides three views of a removable bar screen of the magnetic bar screen assembly.
- FIG. 3 a is a plan view
- FIG. 3 b is a front elevation view
- FIG. 3 c is a side elevation view of the removable bar screen;
- FIG. 4 is a front sectional view of a rotary feed valve assembly of the cryogenic freeze chamber assembly
- FIG. 5 is a sectional view of a drive end bearing assembly of the cryogenic freeze chamber assembly
- FIG. 6 are two views of a front end bearing assembly of the cryogenic freeze chamber assembly.
- FIG. 6 a is a front view and
- FIG. 6 b is a front sectional view of that assembly;
- FIG. 7 is a front sectional view of a cryogenic spray head assembly of the cryogenic freeze chamber assembly
- FIG. 8 is a front sectional view of a view-port assembly of the cryogenic freeze chamber assembly
- FIG. 9 are two views of the auger agitator assembly.
- FIG. 9 a illustrates a typical serrated agitator positioned between auger blades and
- FIG. 9 b depicts the serrated agitator tripping magnet in proximity of a sensor;
- FIG. 10 is a sectional view illustrating triggering of cryogenic fluid from the cryogenic spray assembly
- FIG. 11 is a sectional view illustrating a continuous cryogenic fluid spray from the cryogenic spray assembly
- FIG. 12 is a front view, partially in section, illustrating the positioning of expansion mount locations.
- FIG. 13 provides two views of a cryogenic freeze chamber assembly support.
- FIG. 13 a is a sectional view and FIG. 13 b is an exploded view of a portion of that assembly illustrating expansion joint details.
- a cryogenic freeze chamber assembly 100 incorporates major sub-assemblies which represent embodiments of the present invention. These embodiments will be better understood by the description of their operation.
- Feedstock 6 is introduced into the chamber assembly 100 from a feedstock storage silo 62 through an inlet means.
- the feedstock 6 may be any solid that is insufficiently brittle so that its temperature must be reduced to below its glass transition point in order to insure proper comminutability.
- Examples of feedstocks within the contemplation of the present invention includes rubbers, plants, soft polymers and the like. Of the feedstocks within the contemplation of the present invention, rubber, such as that provide by chopped vehicle tires, sterols and other plant material are particularly preferred.
- the feedstock inlet means of chamber assembly 100 is provided with a slide gate 200 which is utilized when necessary to change feedstocks, make mechanical adjustments or to clear the chamber. Specifically, slide gate 200 is opened when feedstock 6 flow into chamber assembly 100 is desired and closed to stop feedstock 6 flow therein.
- a magnetic bar screen assembly 300 is provided to capture any tramp ferrous metal traveling with feedstock 6 when that feedstock is chopped tires or other feedstock containing fugitive ferrous metal.
- a magnetic bar screen assembly 300 is provided with two stationery view-ports 4 which permit internal visual inspection of the presence, if any, of captured ferrous metal. Metal removal is accomplished by closing the slide gate 200 , pulling out drawer 3 , by means of draw pull handle 2 , and manually removing the captured metal contaminates from at least one bar magnet 5 of assembly 300 . After removal of the metal contaminates, the drawer 3 is repositioned by holding the drawer 3 , by means of handle 2 , and repositioning the bar magnet assembly 300 into its position in chamber assembly 100 .
- VFD variable frequency driven
- the feedstock 6 rate of introduction into chamber assembly 100 is a function of feedstock characteristics and downstream process requirements. These characteristics may be considered in the control of the VFD valve 400 .
- VFD valve 400 controls the mass rate of feedstock into the assembly 100 by its rotary speed. It also acts as an air lock to prevent air from leaking into chamber assembly 100 .
- the feedstock exiting VFD valve 400 flows through a flexible bellows 19 into the inner portion of the chamber 100 .
- bellows 19 are preferably stainless steel. However, other flexible materials, such as those compatible with low temperature operation, may be used. Bellows are utilized in order to eliminate interfacial stress caused by chamber contraction and expansion due to changes in the temperature of the chamber assembly 100 due to the presence or absence of cryogenic fluid. On average, chamber assembly 100 contracts approximately 1 inch upon contact with cryogenic temperature. To minimize this size reduction, chamber assembly 100 is fixed at its center to reduce contraction length at each end to approximately 1 ⁇ 2 inch. This arrangement permits metered feedstock 6 to discharge through flexible bellows 19 directly into the freezing chamber assembly 100 .
- Conveyor means are provided in the interior portion of chamber assembly 100 .
- the conveyor means may be in the form of an endless belt, a rotating auger or the like.
- conveyor means is provided by a rotating auger 7 .
- the rotating auger 7 is supported by and rotates about two end bearing assemblies. The first of these, the drive end bearing assembly 500 , is mounted on the drive end assembly insert 11 .
- the insert 11 also serves as the drive end cap of chamber assembly 100 .
- the drive end bearing assembly 500 also includes dual bearings 61 , two insulator end caps 10 and a pressure plate 9 .
- the end caps 10 are designed to accommodate “O” ring shaft seals 15 and “O” ring chamber seal 59 .
- a VFD rotor (not shown) is coupled to a rotor drive shaft 14 and keyed with motor drive shear pin 13 .
- the motor drive shaft 14 is tapered to assist in the installation alignment of a slotted male coupling 65 which is affixed to auger drive shaft 7 .
- a tapered tip of motor drive shaft 14 is equipped with a drive key 18 which, when engaged with slotted male coupling 65 , drives auger driver shaft 7 .
- the male coupling slot accommodates expansion and contraction of the auger drive shaft 7 . This arrangement allows for coupling in tight areas without the needs for bolts.
- a stationery feedstock barrier 8 prohibits feedstock 6 from infiltrating the coupling area 60 .
- the other end of the auger shaft 7 terminates in a front end bearing assembly 600 .
- shaft 7 is attached to a front end auger shaft connector 30 and a front end bearing shaft 28 supported by front end bearing 27 as part of a front end bearing block 26 .
- the front end bearing assembly 600 includes a front end assembly insert 25 provided with two insulated “O” ring support seals 32 which are bolted together with insulator support assembly bolts 34 .
- the entire insert 25 is connected to an insulated auger trough 24 by means of a multiplicity of front end assembly insert bolts 33 .
- the front end bearing assembly 600 includes a front end rotating bearing shaft 28 which is sealed by means of “O” ring seals 29 .
- the insulated chamber constituting the front end bearing assembly 600 is itself sealed by means of an “O” ring 59 .
- the assembly 600 further includes a pull handle 31 to assist in the assembly or disassembly of the auger shaft 7 within the insulated trough 24 .
- Front end leaving shaft 28 is extended a distance “G,” as shown in FIG. 6 , to compensate for contraction changes.
- the purpose of chamber assembly 100 to reduce temperature of the feedstock 6 to below the glass transition point, is accomplished by spraying the feedstock 6 with a cryogenic fluid.
- the cryogenic fluid usually a cryogenic liquid, is chemically inert whose vaporization temperature is cryogenic at atmospheric pressure.
- cryogens within the contemplation of the present invention include argon, carbon dioxide, nitrogen and other inert gases. Of these, the most effective, in terms of cryogenic temperature, inertness and low cost, is liquid nitrogen.
- Each cryogen spray head assembly 700 which is preferably constructed of stainless steel or the like, includes a cryogen feed pipe 36 welded to a tapered plug 37 , which fits into a matching tapered threaded plug receiver 39 .
- the tapered plug receiver 39 is welded to a support pipe 40 which, in turn, is welded to the top of the cryogenic freezing chamber assembly 100 .
- the top of the assembly 100 constitutes a plurality of flat trough covers 23 .
- FIG. 7 illustrates covers 23 c which are provided in assemblies 700 .
- a screw cap 38 is utilized to hold the tapered plug 37 in position so that each spray nozzle can be accessed, inspected and oriented.
- Two alignments identifiers 64 are positioned on the centerline of a cryogen freeze pipe 36 .
- Identifier 64 aids in properly directing the cryogen spray from nozzles 41 and 42 , one located above tapered plug 37 and the other above a jam nut 63 .
- Jam nut 63 serves to lock the nozzles' position.
- the spray nozzle type utilized in each spray head assembly 700 depends on the function of the cryogenic spray.
- a directional nozzle 41 is illustrated in FIG. 7 . However, a 45° nozzle may be utilized depending upon its location.
- the discharge pressure and velocity of the cryogenic fluid emitting from nozzle 41 can be varied depending upon the type and mass flow rate of feedstock 6 .
- Each view-port assembly 800 includes a mounting frame 46 , holding double-layered heated glass 44 cushioned between a gasket 45 , which, in a preferred embodiment, is silicone rubber. Each view-port assembly 800 is protected by an insulated latch cover 43 .
- a preferred conveyor means for transporting feedstock 6 through the insulated trough 24 of chamber assembly 100 is a rotating auger.
- an auger agitator assembly 900 preferably employed as the conveyor means in chamber assembly 100 , includes an auger drive shaft 7 to which auger blades 47 are attached.
- the auger blades 47 are uniquely connected, preferably by welding, to serrated agitators 48 .
- the serrated agitators 48 attached to auger blades 47 , follow an orbital path as they first intersect and pass through feedstock 6 at the bottom of the trough 24 portion of the chamber assembly 100 .
- Continued auger drive shaft 7 rotation elevates feedstock 6 from its safe angle of repose to a level where it begins to slide off serrated agitator 48 .
- the feedstock 6 is discharged from a gear tooth-shaped edge, it flows in rivulets and feedstock 6 is thus easily and effectively sprayed with the cryogenic fluid as it falls free from serrated agitator 48 .
- Spray is directed from the cryogenic spray head assembly 700 , from nozzles 41 or 42 .
- directional nozzles 41 are employed in spraying feedstock 6 as it moves horizontally along the bottom of the trough 24 as illustrated in FIG. 11 .
- the 45° nozzles 42 are utilized in spraying feedstock 6 as it falls in rivulets from serrated edges 48 , as illustrated in FIG. 10 .
- cryogenic spray is activated only when serrated agitator 48 embedded magnetic 49 triggers a stationery magnetic switch 50 mounted on the side of insulated auger trough 24 . Timing between switch activation and cryogenic fluid spray initiation can be varied or turned off entirely depending upon feedstock requirements. It is emphasized that transported feedstock 6 is also subjected to cryogenic fluid contact from spray-head assemblies 700 , by means of directional nozzles 41 , as it traverses along the bottom of the insulated trough-shaped chamber 24 . The directional nozzles 41 also serve to maintain set operational temperature.
- chamber assembly 100 includes a fixed mounting at its center so that maximum thermal contraction is approximately 1 ⁇ 2 inch at each end. Because of differential temperatures, insulated auger trough 64 and auger drive shaft 7 expansions and contractions are not equal and must be compensated. Thus, the front end of auger drive shaft 7 is free to float with thermal expansions within the front end bearing assembly 600 . This is illustrated by gap G. That is, rotating shaft 28 can move, due to thermal expansion, by a length G, as illustrated in FIG. 6 b.
- each assembly 1000 includes a pair of support brackets 51 and a brace bracket strap 57 to connect the support brackets 51 for additional stability.
- the support brackets 51 are fastened to the auger trough 24 portion of the chamber assembly 100 , preferably by welding, providing expansion and contraction mobility.
- Expansion and contraction capability of the chamber assembly 100 is provided by the chamber support assembly 1000 and expansion joint arrangement 1000 a .
- Expansion joint subassembly 1000 a is depicted in FIGS. 13 a and 13 b .
- Each support bracket 51 connected to the auger trough 24 portion of chamber assembly 100 , is free to move horizontally depending on the expansion and contraction of the assembly 100 .
- Each support bracket 51 is welded to a pressure plate 53 , which is bolted to an upper slip plate 54 .
- a lower slip plate 55 is bolted to cross-mounting plate 56 which is bolted to a platform structural steel support.
- Brackets 52 affixed to cross-mounting plate 56 .
- Horizontal movement of brackets 51 attached to trough 24 are permitted free movement between upper and lower slip plates 54 and 55 .
- a fixed mounting support 58 is welded to a pressure plate 53 which is bolted to cross-mounting plate 56 , as shown in FIG. 13 c .
- the cross mounting plate 56 affixed to platform structural steel support, restrains the center of chamber assembly 100 allowing expansion and contraction to occur at either end.
- Discharge device 21 is again preferably provided by flexible bellows.
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Abstract
Description
- 1. Field of the Invention
- The present invention is directed to a cryogenic freeze chamber assembly. More specifically, the present invention is directed to a cryogenic freezing chamber assembly which more efficiently chills polymeric particles so that those particles can be effectively comminuted.
- 2. Background of the Prior Art
- Cryogenic freeze chamber assemblies are extensively utilized in the processing of solid materials which have high impact resistance. That is, solids which resist fracture during comminution processes represent a major obstacle to reprocessing of solid materials. The reprocessing of solid materials is an ever more important commercial and environment undertaking. A prime example of such materials is vehicle tires. Tires, principally formed of rubber, are excellent examples of impact resistant solids whose comminution is difficult unless its temperature is reduced below the glass transition point. The removal of used tires is very important to good environmental practice and the comminution product, crumb and powder rubbers, represent valuable commercial products.
- Although the utilization of cryogenic freeze chamber assemblies has become more common with the advent of solid comminution processing, present cryogenic freezing chamber assemblies have certain inefficiencies that call for improved design.
- A major concern in the design of cryogenic freeze chamber assemblies is to effectively cool impact resistant particles with minimum use of cryogenic fluid. Indeed, the cost of the cryogenic fluid is probably the major variable cost in the process of comminuting solids. Thus, a design which results in significant reduction in the utilization of cryogenic fluid represents a major aim of artisans working in this art.
- Another problem associated with cryogenic freeze chamber assemblies known in the art is meeting the requirement of providing adequate structural strength to withstand stress imposed on chamber assemblies due to the effect of thermal expansion and contraction. Obviously, the utilization of very cold temperatures makes this design aspect of prime importance in the successful and continuous operation of such an assembly.
- Yet another problem associated with prior art chamber assemblies is the difficulty of identifying blockages in the continuous processing of solid materials. Oftentimes, plugging occurs during that processing. Quick removal of such blockages by rapid identification and elimination of the blockage is essential to successful operation of cryogenic freeze chamber assembles.
- Still an additional problem associated with operation of a cryogenic freeze chamber assembly, common to the operation of major processing assembles, is easy assembly and disassembly to permit maintenance and repair. Thus, easier removal and reassembly of internal components of the subassemblies that constitute a cryogenic freeze chamber assembly is another concern in this art.
- Cryogenic freeze chamber assembles designs of the prior art are used in association with redundant apparatus to remove foreign particles present in the feedstock stream. This is due not only to the difficulty of removing foreign particles from such assemblies but, also, to be able to remove such foreign particles from the chamber assembly once they are removed from the feedstock stream.
- These and other structural advantages are highly desired in the art.
- A new cryogenic freeze chamber assembly has now been developed which solves many structural and design problems associated with cryogenic freeze chamber assemblies of the prior art.
- The newly developed cryogenic freeze chamber assembly addresses the issue of structural integrity effectuated by thermal expansion and contraction. The chamber assembly is fixed at its center to allow movement toward each end rather than the prior art design of concentrating total expansion and contraction at one end. This fixing of the chamber assembly at its center allows for movement toward each end thus minimizing the interfacial stress between stationery interconnecting flexible joints and the chamber assembly.
- Another aspect of the cryogenic freeze chamber assembly of the present invention is improved utilization of cryogenic fluid. Cryogenic fluid is introduced into the freeze chamber assembly in two distinct patterns. The first is a continuous or pulsating spray directed upon the feedstock stream transmitted through the chamber assembly. This spray is controlled as a function of the chamber assembly operating temperature. The second spray is positioned and directed at the multiple and distinct rivulets of falling feedstock particles elevated by rotating agitators. As such, the second of the two cryogenic fluid introductions is limited to specific intervals of time when such introduction effectuates total contact with the total particle surface, maximizing the cooling effect of the cryogenic fluid.
- Yet another major problem associated with cryogenic freeze chamber assemblies, overcome by the chamber assembly of the present invention, is the quick resolution of process downtime caused by blockages in the chamber. In order to remove or otherwise address blockages of solid particles moving through the freeze chamber assembly it is critical that the chamber be capable of inspection without interruption caused by disassembly of the Ofm.fal
- Ofm.fal
- ports which permits viewing of the immediate area about the portion of the chamber within view of the port. Since these view-ports are strategically placed throughout the length of the chamber assembly, the total chamber assembly can be viewed during operation. To insure effectiveness, means to prevent fogging, caused by the cryogenic temperature, the view-ports are provided with heating means in communication with the glass viewing area of the view-port. This heating is automatically effectuated when the view-port cover is opened for viewing.
- Still another issue associated with prior art cryogenic freeze chamber assemblies, addressed by the improved design of the chamber assembly of the present invention, is ease of assembly and disassembly of components of the overall chamber assembly. The chamber assembly of this invention is designed to permit vertical removal of interior components which simplifies repair and maintenance by vertical replacement of components compared to the horizontal removal of interior components required by freeze chamber assemblies of the prior art.
- Yet another advance associated with the present chamber assembly is a self-contained means for removal of foreign materials present in the feedstock. In this advance means are provided for removal of foreign materials from the feedstock at the chamber assembly inlet prior to freezing. This advance is especially important when the feedstocks are obtained from processed tires or other material which contains fugitive ferrous metal. The removal of ferrous metal is important to the reliability and efficiency of not only the freeze chamber assembly but also for the protection of downstream equipment. This is accomplished by the inclusion of magnetic means at the feedstock inlet to attract and remove ferrous metal particles from the feedstock entering the chamber.
- In accordance with the present invention cryogenic freezing chamber assembly is provided. The assembly includes an elongated chamber, an inlet means for introducing feedstock therein, an inlet means for introducing a cryogenic fluid into the chamber and fixed mounting means disposed midway between the ends of the elongated chamber assembly.
- In accordance with the another embodiment of the present invention the chamber assembly includes an elongated chamber, a cryogenic fluid inlet means, a feedstock inlet means, an outlet means for removing feedstock from the chamber and a plurality of view-ports disposed on the chamber surface wherein the view-ports are provided with heating means to maximize clear viewing.
- In yet accordance with another embodiment of the present invention a cryogenic freeze chamber assembly is provided which includes an elongated chamber, a rotating auger disposed in the chamber, an inlet means for introducing feedstock onto the auger, disposed in the chamber, wherein the auger contains, transports and agitates the feedstock particles, cryogenic fluid introductory means responsive to means provided on the rotating auger for introducing cryogenic fluid into the chamber and feedstock outlet means for removal of the feedstock from the chamber.
- In still further accordance with the present invention a cryogenic freeze chamber assembly is drawn to an elongated chamber, a feedstock inlet means for introducing feedstock into the chamber, a cryogenic fluid inlet means for introducing cryogenic fluid into the chamber, a feedstock outlet means for removing feedstock below its glass transition temperature from the chamber and a rotating auger, supported by and rotating about end bearing assemblies for transmitting the feedstock from the feedstock inlet means to the feedstock outlet means.
- The instant invention may be better understood by reference to the accompanying drawings of which:
-
FIG. 1 is a front sectional view of a cryogenic freeze chamber assembly in accordance with the present invention; -
FIG. 2 represents three views of a magnetic bar screen assembly of the cryogenic freeze chamber assembly.FIGS. 2 a, 2 b and 2 c provide plan, front elevation and side elevation cross-sectional views, respectively, of the magnetic bar screen assembly; -
FIG. 3 provides three views of a removable bar screen of the magnetic bar screen assembly.FIG. 3 a is a plan view,FIG. 3 b is a front elevation view andFIG. 3 c is a side elevation view of the removable bar screen; -
FIG. 4 is a front sectional view of a rotary feed valve assembly of the cryogenic freeze chamber assembly; -
FIG. 5 is a sectional view of a drive end bearing assembly of the cryogenic freeze chamber assembly; -
FIG. 6 are two views of a front end bearing assembly of the cryogenic freeze chamber assembly.FIG. 6 a is a front view andFIG. 6 b is a front sectional view of that assembly; -
FIG. 7 is a front sectional view of a cryogenic spray head assembly of the cryogenic freeze chamber assembly; -
FIG. 8 is a front sectional view of a view-port assembly of the cryogenic freeze chamber assembly; -
FIG. 9 are two views of the auger agitator assembly.FIG. 9 a illustrates a typical serrated agitator positioned between auger blades andFIG. 9 b depicts the serrated agitator tripping magnet in proximity of a sensor; -
FIG. 10 is a sectional view illustrating triggering of cryogenic fluid from the cryogenic spray assembly; -
FIG. 11 is a sectional view illustrating a continuous cryogenic fluid spray from the cryogenic spray assembly; -
FIG. 12 is a front view, partially in section, illustrating the positioning of expansion mount locations; and -
FIG. 13 provides two views of a cryogenic freeze chamber assembly support. -
FIG. 13 a is a sectional view andFIG. 13 b is an exploded view of a portion of that assembly illustrating expansion joint details. - A cryogenic
freeze chamber assembly 100 incorporates major sub-assemblies which represent embodiments of the present invention. These embodiments will be better understood by the description of their operation. -
Feedstock 6 is introduced into thechamber assembly 100 from afeedstock storage silo 62 through an inlet means. Thefeedstock 6 may be any solid that is insufficiently brittle so that its temperature must be reduced to below its glass transition point in order to insure proper comminutability. Examples of feedstocks within the contemplation of the present invention includes rubbers, plants, soft polymers and the like. Of the feedstocks within the contemplation of the present invention, rubber, such as that provide by chopped vehicle tires, sterols and other plant material are particularly preferred. - The feedstock inlet means of
chamber assembly 100 is provided with aslide gate 200 which is utilized when necessary to change feedstocks, make mechanical adjustments or to clear the chamber. Specifically,slide gate 200 is opened whenfeedstock 6 flow intochamber assembly 100 is desired and closed to stopfeedstock 6 flow therein. - In view of the importance of chopped vehicle tires as a potential feedstock, a magnetic
bar screen assembly 300 is provided to capture any tramp ferrous metal traveling withfeedstock 6 when that feedstock is chopped tires or other feedstock containing fugitive ferrous metal. - A magnetic
bar screen assembly 300 is provided with two stationery view-ports 4 which permit internal visual inspection of the presence, if any, of captured ferrous metal. Metal removal is accomplished by closing theslide gate 200, pulling out drawer 3, by means of draw pull handle 2, and manually removing the captured metal contaminates from at least onebar magnet 5 ofassembly 300. After removal of the metal contaminates, the drawer 3 is repositioned by holding the drawer 3, by means of handle 2, and repositioning thebar magnet assembly 300 into its position inchamber assembly 100. - Once past the magnetic
bar screen assembly 300, thefeedstock 6 is introduced, in a controlled manner, into the cryogenicfreeze chamber assembly 100 through a variable frequency driven (VFD)rotary valve 400. Thefeedstock 6 rate of introduction intochamber assembly 100 is a function of feedstock characteristics and downstream process requirements. These characteristics may be considered in the control of theVFD valve 400.VFD valve 400 controls the mass rate of feedstock into theassembly 100 by its rotary speed. It also acts as an air lock to prevent air from leaking intochamber assembly 100. The feedstock exitingVFD valve 400 flows through a flexible bellows 19 into the inner portion of thechamber 100. - It should be appreciated that bellows 19, as well as other bellows, discussed below, are preferably stainless steel. However, other flexible materials, such as those compatible with low temperature operation, may be used. Bellows are utilized in order to eliminate interfacial stress caused by chamber contraction and expansion due to changes in the temperature of the
chamber assembly 100 due to the presence or absence of cryogenic fluid. On average,chamber assembly 100 contracts approximately 1 inch upon contact with cryogenic temperature. To minimize this size reduction,chamber assembly 100 is fixed at its center to reduce contraction length at each end to approximately ½ inch. This arrangement permitsmetered feedstock 6 to discharge throughflexible bellows 19 directly into the freezingchamber assembly 100. - Conveyor means are provided in the interior portion of
chamber assembly 100. The conveyor means may be in the form of an endless belt, a rotating auger or the like. In a preferred embodiment illustrated in the drawings, conveyor means is provided by arotating auger 7. Therotating auger 7 is supported by and rotates about two end bearing assemblies. The first of these, the driveend bearing assembly 500, is mounted on the driveend assembly insert 11. Theinsert 11 also serves as the drive end cap ofchamber assembly 100. - The drive
end bearing assembly 500 also includesdual bearings 61, two insulator end caps 10 and apressure plate 9. The end caps 10 are designed to accommodate “O” ring shaft seals 15 and “O”ring chamber seal 59. A VFD rotor (not shown) is coupled to arotor drive shaft 14 and keyed with motordrive shear pin 13. Themotor drive shaft 14 is tapered to assist in the installation alignment of a slottedmale coupling 65 which is affixed to augerdrive shaft 7. A tapered tip ofmotor drive shaft 14 is equipped with adrive key 18 which, when engaged with slottedmale coupling 65, drivesauger driver shaft 7. The male coupling slot accommodates expansion and contraction of theauger drive shaft 7. This arrangement allows for coupling in tight areas without the needs for bolts. A stationery feedstock barrier 8 prohibitsfeedstock 6 from infiltrating thecoupling area 60. - The other end of the
auger shaft 7 terminates in a frontend bearing assembly 600. Specifically,shaft 7 is attached to a front endauger shaft connector 30 and a frontend bearing shaft 28 supported by front end bearing 27 as part of a frontend bearing block 26. The frontend bearing assembly 600 includes a frontend assembly insert 25 provided with two insulated “O” ring support seals 32 which are bolted together with insulatorsupport assembly bolts 34. Theentire insert 25 is connected to aninsulated auger trough 24 by means of a multiplicity of front end assembly insertbolts 33. The frontend bearing assembly 600 includes a front end rotating bearingshaft 28 which is sealed by means of “O” ring seals 29. The insulated chamber constituting the frontend bearing assembly 600 is itself sealed by means of an “O”ring 59. Theassembly 600 further includes apull handle 31 to assist in the assembly or disassembly of theauger shaft 7 within theinsulated trough 24. Frontend leaving shaft 28 is extended a distance “G,” as shown inFIG. 6 , to compensate for contraction changes. - The purpose of
chamber assembly 100, to reduce temperature of thefeedstock 6 to below the glass transition point, is accomplished by spraying thefeedstock 6 with a cryogenic fluid. The cryogenic fluid, usually a cryogenic liquid, is chemically inert whose vaporization temperature is cryogenic at atmospheric pressure. Examples of cryogens within the contemplation of the present invention include argon, carbon dioxide, nitrogen and other inert gases. Of these, the most effective, in terms of cryogenic temperature, inertness and low cost, is liquid nitrogen. - Contact between the
feedstock 6 and the cryogen is effectuated by means of a multiplicity of cryogenspray head assemblies 700. Each cryogenspray head assembly 700, which is preferably constructed of stainless steel or the like, includes acryogen feed pipe 36 welded to a taperedplug 37, which fits into a matching tapered threadedplug receiver 39. The taperedplug receiver 39 is welded to asupport pipe 40 which, in turn, is welded to the top of the cryogenic freezingchamber assembly 100. The top of theassembly 100 constitutes a plurality of flat trough covers 23.FIG. 7 illustratescovers 23 c which are provided inassemblies 700. Ascrew cap 38 is utilized to hold the taperedplug 37 in position so that each spray nozzle can be accessed, inspected and oriented. Twoalignments identifiers 64 are positioned on the centerline of acryogen freeze pipe 36.Identifier 64 aids in properly directing the cryogen spray from 41 and 42, one located above taperednozzles plug 37 and the other above ajam nut 63.Jam nut 63 serves to lock the nozzles' position. The spray nozzle type utilized in eachspray head assembly 700 depends on the function of the cryogenic spray. Adirectional nozzle 41 is illustrated inFIG. 7 . However, a 45° nozzle may be utilized depending upon its location. The discharge pressure and velocity of the cryogenic fluid emitting fromnozzle 41 can be varied depending upon the type and mass flow rate offeedstock 6. - It is common to encounter feedstock blockages during operation. Even in the absence of blockages and other operational problems, verification of feedstock movement and conditioning is vital in controlling operating parameters in
chamber assembly 100. Thus, strategically located heated view-port assemblies 800 are included inchamber assembly 100. These view-port assemblies 800 are welded to the trough covers 23, specifically covers 23 a and 23 b. As such, they provide visual access, from the top of theassembly 100, to activities occurring in the interior of trough-shapedchamber 24. Each view-port assembly 800 includes a mountingframe 46, holding double-layeredheated glass 44 cushioned between agasket 45, which, in a preferred embodiment, is silicone rubber. Each view-port assembly 800 is protected by aninsulated latch cover 43. When thelatch cover 43 is opened for viewing, heat is supplied to insure the absence of clouding or frosting. This is accomplished by including a heating element (not shown) in thedouble glass 44 component of the view-ports assemblies 800. The heating element is activated by a switch turned on by the opening oflatch cover 43. The heating element is switched off by the closing oflatch cover 43. It is emphasized that the disposition of the view-port assemblies 800 in the figures is illustrative and actual disposition of those view-port assemblies are function of the design and operation ofchamber 100. - As stated above, a preferred conveyor means for transporting
feedstock 6 through theinsulated trough 24 ofchamber assembly 100 is a rotating auger. More specifically, anauger agitator assembly 900, preferably employed as the conveyor means inchamber assembly 100, includes anauger drive shaft 7 to whichauger blades 47 are attached. Theauger blades 47 are uniquely connected, preferably by welding, toserrated agitators 48. Theserrated agitators 48, attached to augerblades 47, follow an orbital path as they first intersect and pass throughfeedstock 6 at the bottom of thetrough 24 portion of thechamber assembly 100. Continuedauger drive shaft 7 rotation elevatesfeedstock 6 from its safe angle of repose to a level where it begins to slide offserrated agitator 48. Because thefeedstock 6 is discharged from a gear tooth-shaped edge, it flows in rivulets andfeedstock 6 is thus easily and effectively sprayed with the cryogenic fluid as it falls free fromserrated agitator 48. Spray is directed from the cryogenicspray head assembly 700, from 41 or 42. Specifically,nozzles directional nozzles 41 are employed in sprayingfeedstock 6 as it moves horizontally along the bottom of thetrough 24 as illustrated inFIG. 11 . The 45°nozzles 42 are utilized in sprayingfeedstock 6 as it falls in rivulets fromserrated edges 48, as illustrated inFIG. 10 . - It is emphasized that cryogenic spray is activated only when
serrated agitator 48 embedded magnetic 49 triggers a stationerymagnetic switch 50 mounted on the side ofinsulated auger trough 24. Timing between switch activation and cryogenic fluid spray initiation can be varied or turned off entirely depending upon feedstock requirements. It is emphasized that transportedfeedstock 6 is also subjected to cryogenic fluid contact from spray-head assemblies 700, by means ofdirectional nozzles 41, as it traverses along the bottom of the insulated trough-shapedchamber 24. Thedirectional nozzles 41 also serve to maintain set operational temperature. - To better explain the expansion features of
chamber 100 it is again emphasized that a typical cryogenic freezingchamber assembly 100 will contract about 1 inch when exposed to cryogenic temperature, which approximates −346° F. To compensate for this contraction, and thus reduce undue stress on connecting equipment, flexible bellows are used at the inlets and outlets of feedstock flow. To further mitigate temperature-induced stress,chamber assembly 100 includes a fixed mounting at its center so that maximum thermal contraction is approximately ½ inch at each end. Because of differential temperatures,insulated auger trough 64 andauger drive shaft 7 expansions and contractions are not equal and must be compensated. Thus, the front end ofauger drive shaft 7 is free to float with thermal expansions within the frontend bearing assembly 600. This is illustrated by gap G. That is,rotating shaft 28 can move, due to thermal expansion, by a length G, as illustrated inFIG. 6 b. - Externally, the
insulated auger trough 24 is supported on multiple mounts. As illustrated inFIG. 12 , all but one of those mounts is provided byexpansion mount assembly 1000. Eachassembly 1000, as illustrated inFIG. 13 a, includes a pair ofsupport brackets 51 and abrace bracket strap 57 to connect thesupport brackets 51 for additional stability. Thesupport brackets 51 are fastened to theauger trough 24 portion of thechamber assembly 100, preferably by welding, providing expansion and contraction mobility. - Expansion and contraction capability of the
chamber assembly 100 is provided by thechamber support assembly 1000 and expansionjoint arrangement 1000 a. Expansionjoint subassembly 1000 a is depicted inFIGS. 13 a and 13 b. Eachsupport bracket 51, connected to theauger trough 24 portion ofchamber assembly 100, is free to move horizontally depending on the expansion and contraction of theassembly 100. Eachsupport bracket 51, is welded to apressure plate 53, which is bolted to anupper slip plate 54. Alower slip plate 55 is bolted tocross-mounting plate 56 which is bolted to a platform structural steel support. Vertical and lateral movement of thechamber assembly 100 is limited by a pair of “Z”brackets 52 affixed tocross-mounting plate 56. Horizontal movement ofbrackets 51 attached totrough 24, however, are permitted free movement between upper and 54 and 55. A fixed mountinglower slip plates support 58 is welded to apressure plate 53 which is bolted tocross-mounting plate 56, as shown inFIG. 13 c. Thecross mounting plate 56, affixed to platform structural steel support, restrains the center ofchamber assembly 100 allowing expansion and contraction to occur at either end. - The solid particles, entering the
chamber assembly 100 through rotaryvalve feeder assembly 400, are removed asfeedstock product 22, below its glass transition temperature, throughproduct discharge 21.Discharge device 21 is again preferably provided by flexible bellows. - The above description and embodiments are given to illustrate the scope and spirit of the present invention. These embodiments will make apparent, to those skilled in the art, other embodiments and examples. These other embodiments and examples are within the contemplation of the present invention. Therefore, the present invention should be limited only by the appended claims.
Claims (20)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/975,976 US20090100846A1 (en) | 2007-10-23 | 2007-10-23 | Cryogenic freeze chamber assembly |
| PCT/US2008/075334 WO2009055149A1 (en) | 2007-10-23 | 2008-09-05 | Cryogenic freeze chamber assembly |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11/975,976 US20090100846A1 (en) | 2007-10-23 | 2007-10-23 | Cryogenic freeze chamber assembly |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| US20090100846A1 true US20090100846A1 (en) | 2009-04-23 |
Family
ID=40562080
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| US11/975,976 Abandoned US20090100846A1 (en) | 2007-10-23 | 2007-10-23 | Cryogenic freeze chamber assembly |
Country Status (2)
| Country | Link |
|---|---|
| US (1) | US20090100846A1 (en) |
| WO (1) | WO2009055149A1 (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20240130288A1 (en) * | 2022-10-20 | 2024-04-25 | Cryomass Llc | Cryogenic separation systems and methods |
Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4048469A (en) * | 1973-12-12 | 1977-09-13 | Societa Italiana Vetro Siv S.P.A. | Automatic control system for a defogging circuit |
| US4428535A (en) * | 1981-07-06 | 1984-01-31 | Liquid Carbonic Corporation | Apparatus to cool particulate matter for grinding |
| US4429782A (en) * | 1981-10-16 | 1984-02-07 | Mcquay-Perfex Inc. | Screw conveyer with removable flighting |
| US4597672A (en) * | 1984-03-30 | 1986-07-01 | Stirco, Inc. | Center discharge mixer for fluent and nonfluent material |
| US5152889A (en) * | 1991-12-04 | 1992-10-06 | Exxon Research And Engineering Company | Drip pipe for application of wash liquid to filter surfaces |
| US5174122A (en) * | 1989-10-02 | 1992-12-29 | Applied Cryogenics, Inc. | Method and means of low temperature treatment of items and materials with cryogenic liquid |
| US5354345A (en) * | 1989-08-29 | 1994-10-11 | Minnesota Power And Light | Reactor arrangement for use in beneficiating carbonaceous solids; and process |
| US5408846A (en) * | 1994-02-17 | 1995-04-25 | Crumbrubber Technology Company, Inc. | Apparatus for preparing rubber and other materials for recycling |
| US6263833B1 (en) * | 2000-02-10 | 2001-07-24 | Clyde Runyan | Livestock feed dispenser |
| US20040156263A1 (en) * | 2000-04-07 | 2004-08-12 | Tmo Enterprises Limited | Method and apparatus for the distribution of ice |
| US20050107484A1 (en) * | 2003-11-17 | 2005-05-19 | Lehigh Technologies Llc | Process and apparatus for manufacturing crumb and powder rubber |
-
2007
- 2007-10-23 US US11/975,976 patent/US20090100846A1/en not_active Abandoned
-
2008
- 2008-09-05 WO PCT/US2008/075334 patent/WO2009055149A1/en not_active Ceased
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4048469A (en) * | 1973-12-12 | 1977-09-13 | Societa Italiana Vetro Siv S.P.A. | Automatic control system for a defogging circuit |
| US4428535A (en) * | 1981-07-06 | 1984-01-31 | Liquid Carbonic Corporation | Apparatus to cool particulate matter for grinding |
| US4429782A (en) * | 1981-10-16 | 1984-02-07 | Mcquay-Perfex Inc. | Screw conveyer with removable flighting |
| US4597672A (en) * | 1984-03-30 | 1986-07-01 | Stirco, Inc. | Center discharge mixer for fluent and nonfluent material |
| US5354345A (en) * | 1989-08-29 | 1994-10-11 | Minnesota Power And Light | Reactor arrangement for use in beneficiating carbonaceous solids; and process |
| US5174122A (en) * | 1989-10-02 | 1992-12-29 | Applied Cryogenics, Inc. | Method and means of low temperature treatment of items and materials with cryogenic liquid |
| US5152889A (en) * | 1991-12-04 | 1992-10-06 | Exxon Research And Engineering Company | Drip pipe for application of wash liquid to filter surfaces |
| US5408846A (en) * | 1994-02-17 | 1995-04-25 | Crumbrubber Technology Company, Inc. | Apparatus for preparing rubber and other materials for recycling |
| US6263833B1 (en) * | 2000-02-10 | 2001-07-24 | Clyde Runyan | Livestock feed dispenser |
| US20040156263A1 (en) * | 2000-04-07 | 2004-08-12 | Tmo Enterprises Limited | Method and apparatus for the distribution of ice |
| US20050107484A1 (en) * | 2003-11-17 | 2005-05-19 | Lehigh Technologies Llc | Process and apparatus for manufacturing crumb and powder rubber |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20240130288A1 (en) * | 2022-10-20 | 2024-04-25 | Cryomass Llc | Cryogenic separation systems and methods |
| US20240224868A9 (en) * | 2022-10-20 | 2024-07-11 | Cryomass Llc | Cryogenic separation systems and methods |
| US12193364B2 (en) * | 2022-10-20 | 2025-01-14 | Cryomass Llc | Cryogenic separation systems and methods |
| US20250176467A1 (en) * | 2022-10-20 | 2025-06-05 | Cryomass Llc | Cryogenic separation systems and methods |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2009055149A1 (en) | 2009-04-30 |
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