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US1946332A - Dressing, sizing, and softening oil - Google Patents

Dressing, sizing, and softening oil Download PDF

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Publication number
US1946332A
US1946332A US445230A US44523030A US1946332A US 1946332 A US1946332 A US 1946332A US 445230 A US445230 A US 445230A US 44523030 A US44523030 A US 44523030A US 1946332 A US1946332 A US 1946332A
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United States
Prior art keywords
oil
phosphatides
dressing
sizing
water
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Expired - Lifetime
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US445230A
Inventor
Rewald Bruno
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HANSEATISCHE MUHLENWERKE AG
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HANSEATISCHE MUHLENWERKE AG
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Publication of US1946332A publication Critical patent/US1946332A/en
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Expired - Lifetime legal-status Critical Current

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Classifications

    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/244—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus
    • D06M13/282—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing sulfur or phosphorus with compounds containing phosphorus
    • D06M13/292—Mono-, di- or triesters of phosphoric or phosphorous acids; Salts thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/44—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen containing nitrogen and phosphorus
    • D06M13/453—Phosphates or phosphites containing nitrogen atoms
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M7/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made of other substances with subsequent freeing of the treated goods from the treating medium, e.g. swelling, e.g. polyolefins
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
    • C10M2201/02—Water
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/125—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of eight up to twenty-nine carbon atoms, i.e. fatty acids
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/10—Carboxylix acids; Neutral salts thereof
    • C10M2207/12—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms
    • C10M2207/129—Carboxylix acids; Neutral salts thereof having carboxyl groups bound to acyclic or cycloaliphatic carbon atoms having hydrocarbon chains of thirty or more carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2207/00—Organic non-macromolecular hydrocarbon compounds containing hydrogen, carbon and oxygen as ingredients in lubricant compositions
    • C10M2207/40—Fatty vegetable or animal oils
    • C10M2207/404—Fatty vegetable or animal oils obtained from genetically modified species
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2219/00—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions
    • C10M2219/04—Organic non-macromolecular compounds containing sulfur, selenium or tellurium as ingredients in lubricant compositions containing sulfur-to-oxygen bonds, i.e. sulfones, sulfoxides
    • C10M2219/044—Sulfonic acids, Derivatives thereof, e.g. neutral salts
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
    • C10M2223/00—Organic non-macromolecular compounds containing phosphorus as ingredients in lubricant compositions
    • C10M2223/10—Phosphatides, e.g. lecithin, cephalin
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
    • C10N2040/00—Specified use or application for which the lubricating composition is intended
    • C10N2040/46—Textile oils
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/40—Reduced friction resistance, lubricant properties; Sizing compositions
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions

Definitions

  • My invention relates to an oil for use in textile manufactures.
  • oils are used for treating the fibres, threads or fabrics (i. e. textile materials) and aqueous emulsions of fatty oils and fatty acids are often required as dressing, sizing and softening oils. These emulsionsmust be capable of keeping a long time (i. e. must be quite stable) and should contain no substances which have harmful effects on the fibres.
  • these aqueous emulsions may be made in an advantageous manner by using the phosphatides which are contained in vegetable seeds in abundant quantities, particularly in soya beans from which these emulsions may be obtained very cheaply.
  • soya-bean slush which is obtained by separation from the soya bean oil extracted by means This slush is purified in well known manner with acetone or acetic ether. Moreover the components separating out during this purification are also capable of further use as they consist for the main part of decomposition products of the phosphatides with organically combined phosphorus.
  • the extraction medium used for the hot or cold extraction of the oil and the phosphatides from the soya beans comprises a mixture consisting chiefly of benzol with an addition of 10-20% alcohol. After the evaporation of the solvent leaving a mixture containing oil and phosphatides, steam is then passed into the mixture thus causing the phosphatides to,
  • phosphatides are melted together with suitable fatty acids or oils by heating at a moderate temperature and are emulsified by the'simultaneous addition of small quantities of diluted alkali or soap and vigorous mixing with water. In this way it is possible to obtain emulsions which keep very well. These emulsions will mix with water. in any desired ratio and may be regulated in the desired manner according to the purpose for which intended. They may be completely washed out of the finished product by means of the usual detergents.
  • the emulsions obtained in this way from fatty oils and fatty acids with vegetable phosphatides and water may also be mixed with Turkey-red oil and products thereof and when rendered necessary by the particular purpose for which intended, they may also be prepared with an addition of mineral oils.
  • a fatty acid emulsion suitable for the textile industry for example, one may melt together at a temperature of 50-60 deg. 0. equal parts of olein and dried phosphatides which have a soya bean oil content of 30% and are obtained by extraction with parts of benzol and 10 parts of 96% alcohol. Then by adding an equal quantity of water, keeping the temperature at 50-60 deg. C. and adding 85 small quantities of dilute soda lye, the mixture is emulsified under vigorous stirring.- When re-' quired for use, this emulsion is diluted with further quantities of water in the desired manner.
  • Textile oils may be produced not only from 9.0 the phosphatides derived from soya beans but also from vegetable lecithines which are obtained for instance from peas, lupins as well as grains such as wheat, and rye.
  • a dressing, sizing and softening oil for tex tiles consisting of an emulsion of .vegetable phosphatides in extracted condition and chemically uncombined, fatty oil, fatty acid and water and: substantially free from the remaining constitu- 100 ents of the vegetable material other than the oil.
  • a dressing, sizing and softening oil fortextiles comprising an emulsion of vegetable phosphatides in extracted condition and chemically uncombined, fatty oil and water.
  • a dressing, sizing and softening oil for textiles comprising an emulsion of soya bean phosphatides in extracted condition and chemically uncombined, fatty oil, fatty acid and water and substantially free from the remaining constitu- 9 ents of the vegetable material other than the oil.
  • a dressing, sizing and softening oil for textiles comprising an'emulsion of soya bean'phosphatides in extracted condition and chemically uncombined, fatty oil and'water.
  • a dressing, sizing andsoftening oil for textiles comprising an emulsion of soya bean phosphatides in extracted condition and chemically uncombined, fattyoil, fatty acid, Turkey-red oil and water and substantially free from the remaining constituentsof the vegetable material other than the oil.
  • a dressing, sizing and softening oil for textiles consisting of an emulsion of soya bean phosphatides in extracted condition and chemically

Landscapes

  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)
  • Cosmetics (AREA)
  • Fats And Perfumes (AREA)

Description

" of benzine.
Patented Feb. 6, 1934 PATENT OFFICE 1,946,332 DRESSING, SIZING, AND' SOFTENIN'G OIL Bruno Rewald, Hamburg, Germany, assignor to Hanseatische Muhlenwerke Aktiengesellschaft, Hamburg, Germany, a joint-stock company of Germany No Drawing. Application April 1'1, 1930, Serial No. 445,230, and in Germany April 20, 1929 7 Claims.
My invention relates to an oil for use in textile manufactures.
In the textile industry, oils are used for treating the fibres, threads or fabrics (i. e. textile materials) and aqueous emulsions of fatty oils and fatty acids are often required as dressing, sizing and softening oils. These emulsionsmust be capable of keeping a long time (i. e. must be quite stable) and should contain no substances which have harmful effects on the fibres.
I Now it has been found that these aqueous emulsions may be made in an advantageous manner by using the phosphatides which are contained in vegetable seeds in abundant quantities, particularly in soya beans from which these emulsions may be obtained very cheaply.
When using emulsions prepared with the aid of vegetable phosphatides, no crusts are formed as isthe case with the media generally used for this purpose; consequently the fibres and the fabric remain quite soft. If they are used during the printing of fabrics the print comes out particularly sharp and clear and the dye does not penetrate. In place of tragacanth which is expensive, it is then possible to use starch which is much cheaper. Furthermore, the dye does not harden in the depressions existing in the fabric, but remains uniformly distributed. Furthermore, the rolls and cutting knives used in the processes are also spared.
For the purpose of making the aqueous emulsions with fatty acids or oils, it is possible to use the soya-bean slush which is obtained by separation from the soya bean oil extracted by means This slush is purified in well known manner with acetone or acetic ether. Moreover the components separating out during this purification are also capable of further use as they consist for the main part of decomposition products of the phosphatides with organically combined phosphorus.
Much purer and therefore much more efficient phosphatides are obtained if the extraction medium used for the hot or cold extraction of the oil and the phosphatides from the soya beans, comprises a mixture consisting chiefly of benzol with an addition of 10-20% alcohol. After the evaporation of the solvent leaving a mixture containing oil and phosphatides, steam is then passed into the mixture thus causing the phosphatides to,
separate out and settle on the bottom. After removal they are then freed from a part of the entrained oil by centrifugal separation and are dried under diminished air pressure by distilling off the water present. This may leave a mixture of about 40-50% phosphatides and -60% oil.
These phosphatides are melted together with suitable fatty acids or oils by heating at a moderate temperature and are emulsified by the'simultaneous addition of small quantities of diluted alkali or soap and vigorous mixing with water. In this way it is possible to obtain emulsions which keep very well. These emulsions will mix with water. in any desired ratio and may be regulated in the desired manner according to the purpose for which intended. They may be completely washed out of the finished product by means of the usual detergents.
The emulsions obtained in this way from fatty oils and fatty acids with vegetable phosphatides and water, may also be mixed with Turkey-red oil and products thereof and when rendered necessary by the particular purpose for which intended, they may also be prepared with an addition of mineral oils.
In order to obtain a fatty acid emulsion suitable for the textile industry, for example, one may melt together at a temperature of 50-60 deg. 0. equal parts of olein and dried phosphatides which have a soya bean oil content of 30% and are obtained by extraction with parts of benzol and 10 parts of 96% alcohol. Then by adding an equal quantity of water, keeping the temperature at 50-60 deg. C. and adding 85 small quantities of dilute soda lye, the mixture is emulsified under vigorous stirring.- When re-' quired for use, this emulsion is diluted with further quantities of water in the desired manner.
Textile oils may be produced not only from 9.0 the phosphatides derived from soya beans but also from vegetable lecithines which are obtained for instance from peas, lupins as well as grains such as wheat, and rye.
I claim:
l. A dressing, sizing and softening oil for tex tiles consisting of an emulsion of .vegetable phosphatides in extracted condition and chemically uncombined, fatty oil, fatty acid and water and: substantially free from the remaining constitu- 100 ents of the vegetable material other than the oil.
2. A dressing, sizing and softening oil fortextiles comprising an emulsion of vegetable phosphatides in extracted condition and chemically uncombined, fatty oil and water.
3. A dressing, sizing and softening oil for textiles comprising an emulsion of soya bean phosphatides in extracted condition and chemically uncombined, fatty oil, fatty acid and water and substantially free from the remaining constitu- 9 ents of the vegetable material other than the oil.
4. A dressing, sizing and softening oil for textiles comprising an'emulsion of soya bean'phosphatides in extracted condition and chemically uncombined, fatty oil and'water.
4 5. A dressing, sizing andsoftening oil for textiles comprising an emulsion of soya bean phosphatides in extracted condition and chemically uncombined, fattyoil, fatty acid, Turkey-red oil and water and substantially free from the remaining constituentsof the vegetable material other than the oil.
6. A dressing, sizing and softening oil for textiles consisting of an emulsion of soya bean phosphatides in extracted condition and chemically
US445230A 1929-04-20 1930-04-17 Dressing, sizing, and softening oil Expired - Lifetime US1946332A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE348783X 1929-04-20

Publications (1)

Publication Number Publication Date
US1946332A true US1946332A (en) 1934-02-06

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US445230A Expired - Lifetime US1946332A (en) 1929-04-20 1930-04-17 Dressing, sizing, and softening oil

Country Status (5)

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US (1) US1946332A (en)
BE (1) BE368926A (en)
FR (1) FR692528A (en)
GB (1) GB348783A (en)
NL (2) NL50792C (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2819496A (en) * 1950-12-28 1958-01-14 Hugh J Fairfield Process for oiling fabrics prior to reduction to fibre
FR2602803A1 (en) * 1986-08-14 1988-02-19 Colgate Palmolive Co LECITHIN-BASED FABRIC SOFTENING COMPOSITIONS, METHODS OF MAKING SAME AND THEIR USE

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3625905A (en) * 1967-11-22 1971-12-07 Purex Corp Ltd Detergent composition having softening properties

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2819496A (en) * 1950-12-28 1958-01-14 Hugh J Fairfield Process for oiling fabrics prior to reduction to fibre
FR2602803A1 (en) * 1986-08-14 1988-02-19 Colgate Palmolive Co LECITHIN-BASED FABRIC SOFTENING COMPOSITIONS, METHODS OF MAKING SAME AND THEIR USE
GB2194561A (en) * 1986-08-14 1988-03-09 Colgate Palmolive Co Fabric softening compositions
BE1000403A4 (en) * 1986-08-14 1988-11-22 Colgate Palmolive Co Easing of tissue compositions based lecithin, methods of production and use.
US4808320A (en) * 1986-08-14 1989-02-28 Colgate-Palmolive Company Fabric softening compositions based on lecithin and methods for making and using same
GB2194561B (en) * 1986-08-14 1990-12-19 Colgate Palmolive Co Fabric softening compositions

Also Published As

Publication number Publication date
FR692528A (en) 1930-11-06
NL25360C (en)
GB348783A (en) 1931-05-21
BE368926A (en)
NL50792C (en)

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