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US1718334A - Method and apparatus for atomizing sulphur - Google Patents

Method and apparatus for atomizing sulphur Download PDF

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Publication number
US1718334A
US1718334A US203794A US20379427A US1718334A US 1718334 A US1718334 A US 1718334A US 203794 A US203794 A US 203794A US 20379427 A US20379427 A US 20379427A US 1718334 A US1718334 A US 1718334A
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United States
Prior art keywords
sulphur
atomizer
tank
thru
atomizing
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US203794A
Inventor
Arthur J Crowley
Charles S Haley
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
HUMBOLDT SULPHUR Co
Original Assignee
HUMBOLDT SULPHUR Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by HUMBOLDT SULPHUR Co filed Critical HUMBOLDT SULPHUR Co
Priority to US203794A priority Critical patent/US1718334A/en
Application granted granted Critical
Publication of US1718334A publication Critical patent/US1718334A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B17/00Sulfur; Compounds thereof
    • C01B17/02Preparation of sulfur; Purification
    • C01B17/10Finely divided sulfur, e.g. sublimed sulfur, flowers of sulfur

Definitions

  • Our invention relates to an apparatus and method for atomizing sulphur.
  • One of the objects of the invent-ion is to spray molten sulphur thru an atomizer in a manner which will prevent the freezing of the sulphur around the nozzle tip of the atomizer.
  • Another object of the invention is to maintain a bath of molten sulphur about the atomizer so as to prevent the chilling thereof.
  • Another object of the invention is to maintain the sulphur bath at a level approximately even with the tip of the atomizer.
  • the figure is a vertical sectional view of the tank in which the molten sulphur is held and from which it is sprayed.
  • our invention comprises the immersion of an atomizer within a bath of molten sulphur with the tip of the atomizer approximately even with the level of the sul hur bath, which is always maintained at t e same level within a tank.
  • Air from an outside source is forced thru the sulphur bath and thru the spraying chamber of the atomizer.
  • the air which is under pressure draws sulphur from the bath into the spraying chamber from which it escapes at a high velocity and due to the sudden expansion, the sulphur is atomized.
  • Thefparticular type of atomizer is not a part 0 the presient invention, since any atomizer may be use
  • our invention comprises a steam jacketed tank 1, having a pipe 2, for the in- FOB ATOMIZING SULPHUR.
  • a sulphur inlet pipe 4 for the introduction of molten sulphur and a sulphur outlet pipe 6 pass thru the walls of the tank near the top thereof and at the same distance from the bottom of the tank, so as to maintain the molten sulphur within the tank at the same level. Circulation of sulphur thru the inlet and outlet pipes of the tank is maintained at a rate which is about the same at which the sulphur is sprayed from the tank. Drain pipes 7 are located in the bottom ofthe tank for permitting the draining thereof.
  • the atomizer 8 Immersed within the bath of molten sulphur is the atomizer 8, which comprises a spraying chamber 9 with passages 11 leading into the bath of sulphur, and the air nozzle 12.
  • the tip of the atomizer is a proximately even with the surface of the bat preferably a trifle above the bath.
  • An air pipe 13 leads from the air nozzle 12, thru the bath of sulphur and thru the tank, to an air compressor.
  • the above described process may be carried on by having a plurality'of atomizers within the tank.
  • a method of atomizing sulphur which comprises melting the sulphur, maintainingmeans for maintaining the mass of sulphur at a constant level, and an atomizer immersed within the mass of molten sulphur.
  • the herein described apparatus for atomizing sulphur comprising a chamber, a
  • the herein described apparatus for atomizing sulphur comprising a chamber, a
  • An apparatus for atomizing sulphur comprising a chamber, a mass of molten sulphur within the chamber, means for heating the sulphur, means for maintaining the sulphur at a constant level, an atomizer within the mass of sulphur and an air passage leading thru the wall of the chamber and thru the bath of molten sulphur to the atomizer.

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Description

June 25, 1929. A. J. CROWLEY in AL 1.718.334
IETHOD AND APPARATUS FOR ATONIZING SULPHUR Filed July 6, 1927 a l I} INVE/VTQES Jeni 0P1 (EMU CHARLES S. HALEY THE/A? ATTOE/YEY.
Patented June 25, 1929.
UNITED STATES 1,718,334 PATENT- OFFICE.
ARTHUR J. CROWLEY, 0F SULPHUR, NEVADA, AND CHARLES S. HALEY, OF SAN FRAN- CISGO, CALIFORNIA, ASSIGNOBS TO HUMBOLDT SULPHUR COMPANY, OF SULPHUR,
NEVADA, A OOB'PORATION OI DELAWARE.
METHOD AND APPARATUS Application filed July 6,
Our invention relates to an apparatus and method for atomizing sulphur.
One of the objects of the invent-ion is to spray molten sulphur thru an atomizer in a manner which will prevent the freezing of the sulphur around the nozzle tip of the atomizer.
Another object of the invention 'is to maintain a bath of molten sulphur about the atomizer so as to prevent the chilling thereof.
Another object of the invention is to maintain the sulphur bath at a level approximately even with the tip of the atomizer.
The invention possesses many other objects and valuable features, some of which will be set forth in the following-description of the invention which is illustrated in the drawings forming part of the specification. It is to be understood that we do not limit ourselves to the showing made by the said description and drawings, as we may adopt varying forms of our invention wlthin the scope of the claims.
The figure is a vertical sectional view of the tank in which the molten sulphur is held and from which it is sprayed.
Efforts have been made to atomize molten sul hur by s raying it thru a nozzle but the difficulty in t is process is that upon the sudden expansion of the sulphur, it becomes chilled and solidifiesaround the ti of the nozzle, thus clogging the nozzle. is difficulty is overcome by the method described in our invention.
In terms of broad inclusion, our invention comprises the immersion of an atomizer within a bath of molten sulphur with the tip of the atomizer approximately even with the level of the sul hur bath, which is always maintained at t e same level within a tank. Air from an outside source is forced thru the sulphur bath and thru the spraying chamber of the atomizer. The air which is under pressure draws sulphur from the bath into the spraying chamber from which it escapes at a high velocity and due to the sudden expansion, the sulphur is atomized. Thefparticular type of atomizer is not a part 0 the presient invention, since any atomizer may be use In detail, our invention comprises a steam jacketed tank 1, having a pipe 2, for the in- FOB ATOMIZING SULPHUR.
1927. Serial No. 208,794.
troduction of steam into the jacket and which is located near the top of the tank, and a steam outlet and drain pipe 3 located in the bottom of the tank for draining the condensate and steam from the jacket. A sulphur inlet pipe 4 for the introduction of molten sulphur and a sulphur outlet pipe 6 pass thru the walls of the tank near the top thereof and at the same distance from the bottom of the tank, so as to maintain the molten sulphur within the tank at the same level. Circulation of sulphur thru the inlet and outlet pipes of the tank is maintained at a rate which is about the same at which the sulphur is sprayed from the tank. Drain pipes 7 are located in the bottom ofthe tank for permitting the draining thereof.
Immersed within the bath of molten sulphur is the atomizer 8, which comprises a spraying chamber 9 with passages 11 leading into the bath of sulphur, and the air nozzle 12. The tip of the atomizer is a proximately even with the surface of the bat preferably a trifle above the bath. An air pipe 13 leads from the air nozzle 12, thru the bath of sulphur and thru the tank, to an air compressor.
. It will be thus seen that as the air is forced thru the pipe and nozzle it draws the sulphur from the ath thru passages 11, into the spraying chamber from which it is 'spra ed into' the atmosphere. The atomized sulp ur which is in a very finely divided state is then collectedby suitable collecting means 14.
The above described process may be carried on by having a plurality'of atomizers within the tank.
As a result of the above recited process an atomized sulphur is produced which is much finer than the usual ade of atomized sulphur,'inasmuch as it Wlll pass thru a 300 mesh screen.
We claim:
1. A method of atomizing sulphur which comprises melting the sulphur, maintainingmeans for maintaining the mass of sulphur at a constant level, and an atomizer immersed within the mass of molten sulphur.
3. The herein described apparatus for atomizing sulphur comprising a chamber, a
mass of molten sulphur within the chamber, means for heating the sulphur, means for mass of sulphur.
5. The herein described apparatus for atomizing sulphur comprising a chamber, a
mass of molten sul hur within the chamber, means for maintainlng the mass of sulphur at a constant level, and an atomizer immersed within the mass of molten sulphur so that the tip of the atomizer is approximately even with the level of the mass of sulphur.w
6. An apparatus for atomizing sulphur comprising a chamber, a mass of molten sulphur within the chamber, means for heating the sulphur, means for maintaining the sulphur at a constant level, an atomizer within the mass of sulphur and an air passage leading thru the wall of the chamber and thru the bath of molten sulphur to the atomizer.
In testimony whereof, we have hereunto set our hands.
ARTHUR J. CROWLEY. CHARLES S. HALEY.
US203794A 1927-07-06 1927-07-06 Method and apparatus for atomizing sulphur Expired - Lifetime US1718334A (en)

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Application Number Priority Date Filing Date Title
US203794A US1718334A (en) 1927-07-06 1927-07-06 Method and apparatus for atomizing sulphur

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US203794A US1718334A (en) 1927-07-06 1927-07-06 Method and apparatus for atomizing sulphur

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2629133A (en) * 1950-06-06 1953-02-24 Olin Mathieson Production of noncaking finely ground sulfur
US2972169A (en) * 1957-09-13 1961-02-21 Owens Corning Fiberglass Corp Method and apparatus for producing fibers
US3083405A (en) * 1958-10-03 1963-04-02 Heinz Erich Sommer Process and apparatus for the manufacture of fibres from fusible mineral materials, more particularly glass and its derivatives
US3355259A (en) * 1964-02-03 1967-11-28 Freeport Sulphur Co Process for melting sulfur

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2629133A (en) * 1950-06-06 1953-02-24 Olin Mathieson Production of noncaking finely ground sulfur
US2972169A (en) * 1957-09-13 1961-02-21 Owens Corning Fiberglass Corp Method and apparatus for producing fibers
US3083405A (en) * 1958-10-03 1963-04-02 Heinz Erich Sommer Process and apparatus for the manufacture of fibres from fusible mineral materials, more particularly glass and its derivatives
US3355259A (en) * 1964-02-03 1967-11-28 Freeport Sulphur Co Process for melting sulfur

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