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US1770725A - Bubble tower - Google Patents

Bubble tower Download PDF

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Publication number
US1770725A
US1770725A US222620A US22262027A US1770725A US 1770725 A US1770725 A US 1770725A US 222620 A US222620 A US 222620A US 22262027 A US22262027 A US 22262027A US 1770725 A US1770725 A US 1770725A
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US
United States
Prior art keywords
liquid
bubble
well
bubble tower
pipe
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
US222620A
Inventor
Edward E Bartels
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Standard Oil Co
Original Assignee
Standard Oil Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Standard Oil Co filed Critical Standard Oil Co
Priority to US222620A priority Critical patent/US1770725A/en
Application granted granted Critical
Publication of US1770725A publication Critical patent/US1770725A/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D3/00Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14Fractional distillation or use of a fractionation or rectification column
    • B01D3/16Fractionating columns in which vapour bubbles through liquid
    • B01D3/18Fractionating columns in which vapour bubbles through liquid with horizontal bubble plates
    • B01D3/20Bubble caps; Risers for vapour; Discharge pipes for liquid

Definitions

  • the uquid seal or well poaion 21 0f the This invention relates to improvements in fractionating columns, and particularly to columns of the bubble cap type.
  • Figure 1 is an elevational view of a column
  • Fig. 2 is a sectional view of the overiiow pipe ⁇ on an enlarged scale
  • Fig. 3 is a similar view of a modilied for-m of overflow pipe.
  • 10 is a fractionating column provided with bubble 4 plates 11 of the ordinary type.
  • the column is provided at its lower end with avapor supply pipe 12 and a liquid draw-off p1pe 13, and at its upper end with a liquid supply pipe 14 and a-vapor-outlet 15.
  • the overflow pipes 16 are provided with a liquid seal or trap, and with an outlet located above the liquid level of the plate next below.
  • each of the overflow pipes 16 preferably comprises an upstanding nipple 17, a flange 18 therebeneath for attachment to a bubble cap plate, and a lower body portion constituted by sides 19.and a wall portion 2O which extends,
  • a septum 23 extends. between the Asides 19 and from the flange 18, into. the well 21 s o as to establish a liquidseal therein..
  • overflow pipe 16 is provided with a hole or orilice 24, at a low portion thereof and preferably at its lowest point.
  • the orifice 24 is of such a size that itpermits only a part of the down-coming liquid to pass therethrough so that sealing liquid is maintained in the well 21 and a substantial part of the flow passes over the spout 22. Since the size of the orifice depends upon the volumeof the flow, it is impossible to state definitely what size it should be in any particular case. By way of illustration, however, it may be stated that in bubble towers used forfractionating petroleum distillates an orifice of about one inch diameter has been found suitable for overiowpipes in which the nipple 17 is about six lnches in diameter.
  • the overflow pipe y16 may be in the form of a pipe of uniform diameter having a bend which constitutes a liquid sealtherein.
  • the orifice 24 is proy vided in the lowest point of thisy bend.
  • the down-flowing liquid passes into the overliow pipe through the nipple 17 and lills the liquid seal or well 21, so
  • An overflow pipe for bubble cap towers comprising ⁇ a nipple adapted to project above a bubble plate to which it is to be attached, a.
  • a bubble tower comprising a plurality of superimposed plates, a bubble plate, an overflow pipe therefor, ingprovided with a liquid seal portion, a discharge 'above the liquid level of the next inferior plate, and a normally unclosed perforation at a low point of said seal portion and adapted to discharge liquid continuously.
  • a bubble tower comprising a plurality of superimposed plates, a bubble plate, an overflow pipe, therefore said overow-pipe being provided with means constituting a receptacle vided with a normally unclosed orifice at the lowest point of said receptacle and adapted to discharge liquid continuously upon the plate therebeneath.l
  • said overflow pipe be-l for sealing liquid therein and pro-

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Extraction Or Liquid Replacement (AREA)

Description

July l5, 1930. E. E. BARTELS BUBBLE TOWER Filed sept; 28, 1927 Patented July 15, 1930 I' UNITED sTArE's'A-PATENT OFFICE EDWARD E. BARIELS, OF 'WHITIN G, INDIANA, ASSIGNOR TO STANDARD OIL CO]ll[I.A.'l\1'Y,l OIE'.'WI-IICLING, INDIANA, CORPORATION OF INDIANA BUBBLE TOWER Application led September 28, 1927. Serial No. 222,620.
The uquid seal or well poaion 21 0f the This invention relates to improvements in fractionating columns, and particularly to columns of the bubble cap type.
In co-pending application Serial No. v1,91,250,filed Ma 13, 1927, Perry J. Sweeney has described a ubble tower provided with' overflow pipes having'liquid seals therein, and adapted to discharge liquid at a point above the level of the liquid on the plate therebeneath.
The present invention relates particularly ltiq ap improvement in overiow pipes of this The invention will be readily understood from the following description taken in conjunction with the drawings, in which:
Figure 1 is an elevational view of a column,
partly broken away to show plates and asso ciated parts. 4
Fig. 2 is a sectional view of the overiiow pipe `on an enlarged scale; and
Fig. 3 is a similar view of a modilied for-m of overflow pipe.
Referring to the drawings, 10 is a fractionating column provided with bubble 4 plates 11 of the ordinary type. The column is provided at its lower end with avapor supply pipe 12 and a liquid draw-off p1pe 13, and at its upper end with a liquid supply pipe 14 and a-vapor-outlet 15. The overflow pipes 16 are provided with a liquid seal or trap, and with an outlet located above the liquid level of the plate next below.
As shown in Figs. 1 and 2, each of the overflow pipes 16 preferably comprises an upstanding nipple 17, a flange 18 therebeneath for attachment to a bubble cap plate, and a lower body portion constituted by sides 19.and a wall portion 2O which extends,
downwardly from said flange, closes the bottom-ofthe nipple 17 and then proceeds upwardly forming with-the sides 19 a well 21. The'wall 20 then bends downwardly again and, together with extensions of the sides 19, formsa spout 22 which terminates somewhat above the .level of the liquid maintained in the..nextinferiorvplate A septum 23 extends. between the Asides 19 and from the flange 18, into. the well 21 s o as to establish a liquidseal therein..
overflow pipe 16 is provided with a hole or orilice 24, at a low portion thereof and preferably at its lowest point. y The orifice 24 is of such a size that itpermits only a part of the down-coming liquid to pass therethrough so that sealing liquid is maintained in the well 21 and a substantial part of the flow passes over the spout 22. Since the size of the orifice depends upon the volumeof the flow, it is impossible to state definitely what size it should be in any particular case. By way of illustration, however, it may be stated that in bubble towers used forfractionating petroleum distillates an orifice of about one inch diameter has been found suitable for overiowpipes in which the nipple 17 is about six lnches in diameter.
Asshown in Fig. 3, the overflow pipe y16 may be in the form of a pipe of uniform diameter having a bend which constitutes a liquid sealtherein. The orifice 24 is proy vided in the lowest point of thisy bend.
In operation, the down-flowing liquid passes into the overliow pipe through the nipple 17 and lills the liquid seal or well 21, so
as to prevent upward passage ofthe vapors therethrough. A stream of the liquid issues from the orilice 24, carrying withit solid matter which might otherwise collect in the well 21. As previously indicated,this stream ordinarily constitutes only a part of the down-llowing liquid, the remainder passing out over the spout 22. i
Although the present invention has *been described in connection with the details of a,
said well and adapted to discharge liquid continuously therefrom.
2. An overflow pipe for bubble cap towers comprising` a nipple adapted to project above a bubble plate to which it is to be attached, a.
t extending therefrom,
well'portion, a spou` l and a wail extending into saldwell portion to constitute a liquid seal therein, saidlpipe being provided with a relatively small nor-l mally unclosed orifice at a low point of said well.
3. A bubble tower, comprising a plurality of superimposed plates, a bubble plate, an overflow pipe therefor, ingprovided with a liquid seal portion, a discharge 'above the liquid level of the next inferior plate, and a normally unclosed perforation at a low point of said seal portion and adapted to discharge liquid continuously.
4:. A bubble tower comprising a plurality of superimposed plates, a bubble plate, an overflow pipe, therefore said overow-pipe being provided with means constituting a receptacle vided with a normally unclosed orifice at the lowest point of said receptacle and adapted to discharge liquid continuously upon the plate therebeneath.l
In witness whereof, I have hereunto set my hand, this Sth day of September, 1927.
EDWARD E. BARTELS.
said overflow pipe be-l for sealing liquid therein and pro-
US222620A 1927-09-28 1927-09-28 Bubble tower Expired - Lifetime US1770725A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
US222620A US1770725A (en) 1927-09-28 1927-09-28 Bubble tower

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2792070A (en) * 1952-02-25 1957-05-14 Phillips Petroleum Co Refinery blowdown and relief system
US4184857A (en) * 1976-04-05 1980-01-22 Jgc Corporation Stripping column and process for removal of volatile matter
US4381974A (en) * 1981-09-08 1983-05-03 Furzer Ian A Distillation columns

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2792070A (en) * 1952-02-25 1957-05-14 Phillips Petroleum Co Refinery blowdown and relief system
US4184857A (en) * 1976-04-05 1980-01-22 Jgc Corporation Stripping column and process for removal of volatile matter
US4381974A (en) * 1981-09-08 1983-05-03 Furzer Ian A Distillation columns

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