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US1653390A - Process of and means for flaking soap - Google Patents

Process of and means for flaking soap Download PDF

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US1653390A
US1653390A US492214A US49221421A US1653390A US 1653390 A US1653390 A US 1653390A US 492214 A US492214 A US 492214A US 49221421 A US49221421 A US 49221421A US 1653390 A US1653390 A US 1653390A
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soap
liquid
apron
flakes
flaking
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Coltman Bertram Wm
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/14Shaping
    • C11D13/20Shaping in the form of small particles, e.g. powder or flakes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S159/00Concentrating evaporators
    • Y10S159/23Cooling

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  • Myinvention relates to the process of and means for flaking soap.
  • the invention is particularly concerned with producing flaked soap foruse in the ture a high rade ofs'oap inflaked condition at a reasona 1y low cost has been due chiefly to the necessity of needless repetition of several steps in the process.
  • flaked soap has been merely the cake soap cut up again into shreds in order to place it in a condition more suitable for use. resulted in increased cost in production.
  • this soap is not flaked, but shaved, which of course must necessarily be of greater thickness.
  • shreds are placed upon delivery apron isprovi to aprons, and a 1 ed to receive the dried chipped -soap from the last of the series of drying aprons, It is then thor-' oughly mixed with the requisite colors and scent, and again massed or kneaded in order to form it into rolls which are out according to weight. These pieces are lastly placed in automatic stamping machines for caking or barring.
  • a thin flake is pr uced, being practicallytransparcut and in a-state next to powder.
  • the field for the use of flaked soap is greatly extended.
  • The' flakes are in a perfect condition to obtain; the-desired solubility in the washing fluid.
  • the theory involved includes spraying liquid soap. in fine clouds upon a traveling apron, which results in the formation of a fine sheet of soap.
  • This sheet of soap is'then carried by the aprons throu h an evaporating zone, such as a" hot 'or co d air blower directing currents against the apron, or such as a warm air oven or chamber housing a portion of the apron.
  • the soap is thoroughly desiccated and is in a frozen or friable condition when reaching thefend of the apron, so that it breaks up in fine' flakes as the apron travels around the end roller.
  • Figure 1 is a layout of apparatus for producing a flake embodying my invention
  • Figure 2 is an alternative lay out of apparatus embod ing my invention
  • Figure 3 il ustrates a form similar to Figure 2; but showing the use of a hot air oven and cooling chamber;
  • Figure 4 illustrates an alternative means for removing the soap from the apron after it is desiccated.
  • liquid soap is fed into the vat 2 through the supply pi pfiel3 containing the supply control valve 4.
  • e supply pipe 3 may lead direct: 1y from the large vat wherein the necessary constituents are thoroughly mixed and prepared into soap.
  • the solution taken from such a vat may contain about 25% moisture.
  • the volume of liquid soap is increased by I being mixed with water or other suitable fluid, such as alcohol or acetone, which reduces its density to permit freer flow, besides bein thinned out considerably.
  • the thinning uid is fed into the vat 2 through the valve 5 and pipe 6.
  • This fluid is mixed with the soapy solution b means of an ordinary wire stirrer 7 usual y employed where a mixing action is preferable over an ebulliting or kneading action.
  • the stirrer 7 is carried u on a shaft 8 which. is driven by any suita lc means, as for instance by a belt 9.
  • a hot air jacket 10 surrounds the mixing vat 2 to keep the contents thereof at a certain temperature.
  • the liquid soap of reduced consistency is fed through the valve 11 into the whipping vat 12, which, as shown, is of the ordinary type.
  • the whi per comprises simply the be t driven sha 13 carrying wires or rods 14, which stir and aerate the material.
  • the construction is such that the stirring instrumentalities, i. e. wires or rods, ass through the viscid mass with a smoot -cutting as again distinguished from either an ebullitin or kneading action, whereby there is o tained indefinitely repeated cutting of the occluded air into smaller and smaller subdivisions with comparatively small levitation or expulsion thereof,
  • the liquid soap is brou ht into a foaming mass.
  • the li uid soap is kept main upon the belt and will spread evenly thereover by its own action.
  • warm air of sufficient avidity to remove the moisture is directed against the soap by'means of the blower 18 and manifold 19 having any number of jets 20 from which the air is emitted.
  • the soap By the time the soap reaches the end of the belts horizontal run, it will be of a spongy and friable nature, that is, there will be a tendency for it to crumble into fine flakes as soon as it is disturbed.
  • the comparatively small diameter roller 21 serves this purpose, while, if so desired, an auxiliary means may be used to remove soa which persists in clinging to the belt.
  • This auxiliary means is in the form of one or more blades 22,which lightly bear against the belt ing the same. It is to be noted that the flakes are permitted to drop practically untouched into the receptacle 23, which prevents lumping. It is further to be noted that the use of this particular process will produce a flake, which is very spongy in character, and which is friable, so that it will immediately break or crumble into bits when disturbed; the flake having a great avidity to dissolve instantly upon mixing with a washing fluid.
  • FIG. 2 An alternative process for flaking soap is shown in Figure 2.
  • the liquid soap is taken from the cooking vat (not shown) with a consistency of about 25% moisture, and fed through the supply pipe 25", the flow being controlled by the va ve 26, to the vat 27.
  • the liquid soap while in this vat 27, is kept at a certain temperature to prevent cooling oif which is apt to result in crusting, but this has been found provide such disturbance by crewithout wearing or destrovnot necessary. With the soap in such state,
  • the sheet of soap is advanced under the streams of warm air emitted from the jets of the manifold 19.
  • the length of the belts horizontal run is such as will permit a manifold of sufiicient capacity to be used to desiccate the soap film, and also permit adequate cooling of the soap film before it is disturbed and crumbled into flakes;
  • FIG. 3 By referringi to Figure 3, an alternate suggestion for esieeating the soap filmfupon the traveling surface will beseen. It is considered a matter of ordinary mechanical skill to propose a different method fordesiccating the soap upon the surface 30, as the scope of the present invention should extend to any method of desiccation.
  • the particular construction shown in Figure 3 comprises a warm air oven 33 through which the surface is led. Freely rotating rollers may be mounted within this warm air oven 33 and adjusted so as to engage lightly the pellicle of soap on the belt. Thiswill, more or less,
  • the invention is not to be limited to aerating to cause frothing of-the liquid soap before it is spread upon'the belt.
  • the invention will, however, produce a flake which is very desirable, being spongy, friable, and of a very soluble character.
  • the feature of spraymg a thin film of soapy solution upon a traveling (horizontal) surface, against which is directed currents of warm an, and then disturbing the desiccated soap by changing the direction of travel of the surface, is considered of importance.
  • the method of flaking soap which comprises first laying a layer of liquid soap upon a surface, next, conditioning said soap while upon the surface by desiccation to rei an move substantially the entire moisture thereinfand finally, breaking said soap into pieces by changing the contour of said surface after said conditioning has taken place.
  • the method of flaking soap which comprises first spraying liquid soap upon a moving surface, next, passing said surface through a desiccation zone to remove the moisture in the soap, and finally, removing the soap in flaked condition from said surface.
  • the methodfof flaking soap which comprises, first spraying a thin film-of liquid soap upon a traveling surface, next, passing said surface through a hot air zone to re move the moisture contained in the soap,
  • a source of liquid soap means for converting'the liquid soap into a froth, a sprayer for spraying said froth upon an a ion, a desiccating zone for rendering said roth in a friable condition, and means for disturbing the friably conditioned froth so as to remove it from the apron in form of flakes.
  • a source of liquid soap a converter for converting said liquid soap into a froth, a sprayer for spraying the froth upon an apron, a warm air zone for removing moisture from said froth, a cool air zone for removing heat from said froth, and means at the end of the apron to disturb said froth.
  • the method ofproducing soap flakes having a high degree of porosity and easily soluble in water which comprises spraying in fine clouds a liquid soa of a bi h air content upon a moving sur ace where the air may be readily released during the ardening of the soap, and finally disturbing the soap so that it will crumble into flakes of crystalline appearance upon being removed from said surface.
  • the method of producing soap flakes having a high degree of porosity an easily soluble in water which comprises taking li uid soa of any density and adding a thinning uid thereto whereby the liquid soap may be given a desired volume of air by subsequent agitation, then applying the soap to a surface in a manner to continue the agitation and the admixture of air with the soap but upon being spread upon said surface to effect a release of the air during a subsequent drying or hardening step, and
  • the method of producing soap flakes easily soluble in water which comprises sprayingliquid soap of a high air content upon a moving surface in a substantially thin layer whereby upon hardening of the soap the walls thlereof confining the air therein will contract'and release the air, and 10 finally removing the hardened air-freed soap from said surface for disintegration into separate flakes or particles. 7

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Description

Dec. 20, 1927.
B. W. COLTMAN PROCESS OF AND MEANS FOR FLAKING sou Filed Aug. 15, 1921 2 Sheets-Sheet 1 DecQZO, 1927. 1,653,390 a. w. COLTMAN PROCESS OF AND MEANS FOR FLAKING SOAP Filed Auz. 15. 1921- 2 Sheets-Sheet 2 Patented Dec. 20, 192 7.
' UNITED' STATES,
PATENT- OFFICE.
,mm'rm COLTMAN, 'or cm onqo, mm I8.
o I rnoonss' or AND 1mm iron amino son. I
Application filed August 15,1921. Serial no. 492,214.-
Myinventionrelates to the process of and means for flaking soap.
The invention is particularly concerned with producing flaked soap foruse in the ture a high rade ofs'oap inflaked condition at a reasona 1y low cost has been due chiefly to the necessity of needless repetition of several steps in the process. Heretofore, flaked soap has been merely the cake soap cut up again into shreds in order to place it in a condition more suitable for use. resulted in increased cost in production. In reality, this soap is not flaked, but shaved, which of course must necessarily be of greater thickness. i
From actual experience it has been foundthat shaved soap must be instantly soluble in the washing fluid, and as a re uisite thereto, the shavings must be light an very thin, bu tsuch as will prevent massing or' pastingtogether while in packages. Us1 1allysoap flakes are used where a saving in time and in labor is desired, and hence, if the.
flakes mass before bein used, due to moisture, heat, or lack-of t orough desiccation,
" the advantage ordinarily obtained by their use will be'lost.
Practically all soap isflaked while in some stage of its making. This is particularly true of the higher grades of toilet soap, whose external appearance in bar form is greatly taken into account and considered as" animportant factor in marketing. In the manufacture of such soap, theliquid is usually poured into a. trough, into WhlCh projects a rotary laminating roller, which wipes a thin layer'of liquid soap on its periphery. The pellicle of soap is then passed between and onto a second-laminating roller, and so on, until it is pressed mto This has a thin sheet'forshredding or chipping. The
shreds are placed upon delivery apron isprovi to aprons, and a 1 ed to receive the dried chipped -soap from the last of the series of drying aprons, It is then thor-' oughly mixed with the requisite colors and scent, and again massed or kneaded in order to form it into rolls which are out according to weight. These pieces are lastly placed in automatic stamping machines for caking or barring.
Obviously this process is tedious and expensive, particularly so when the soap thus produced is again shredded. These shreds usually'are not of afine' texture, being too coarse to. permit instant solubility.
Accordm tothe present invention, a thin flake is pr uced, being practicallytransparcut and in a-state next to powder. With theflakes inthis condition, the field for the use of flaked soap is greatly extended. The' flakes are in a perfect condition to obtain; the-desired solubility in the washing fluid.
Briefly, the theory involved includes spraying liquid soap. in fine clouds upon a traveling apron, which results in the formation of a fine sheet of soap. This sheet of soap is'then carried by the aprons throu h an evaporating zone, such as a" hot 'or co d air blower directing currents against the apron, or such as a warm air oven or chamber housing a portion of the apron. The soap is thoroughly desiccated and is in a frozen or friable condition when reaching thefend of the apron, so that it breaks up in fine' flakes as the apron travels around the end roller. I means forremovmg the soap fromthe apron, and even contemplatin resorting to various 'forms of aprons,-whic will function to re-- movethe soap when reaching a certain Point.
I have found by reducin the density of the liquid soap before fee it through the s ra ers onto the apron, at the flakes will e ight and porous, which of course permits greater solubility.- This desired result is secured b first mixing the liquid soap, as it comes m the cooking vat, with propose employing various a thinning fluid which reduces its consistency, so that it may be worked with greater facility when aerated by whipping or blowing air through, or ot er suitable process, so as to convert it into a mass whose weight is considerably less than that of the same volume of ordinar liquid soap. After aerated, the soap W111 be frothy and very light and may be spra ed with reater facility upon the apron. hile a t ing fluid has been found desirable, its use is not essential to the aerating step, as liquid soap of any consistency may be whipped to increase its volume.
In the drawing: Figure 1 is a layout of apparatus for producing a flake embodying my invention;
Figure 2 is an alternative lay out of apparatus embod ing my invention;
Figure 3 il ustrates a form similar to Figure 2; but showing the use of a hot air oven and cooling chamber; and
Figure 4 illustrates an alternative means for removing the soap from the apron after it is desiccated.
Referring to the illustration in Figure 1, liquid soap is fed into the vat 2 through the supply pi pfiel3 containing the supply control valve 4. e supply pipe 3 may lead direct: 1y from the large vat wherein the necessary constituents are thoroughly mixed and prepared into soap. The solution taken from such a vat may contain about 25% moisture.
This, of course, may be varied. In the vat 2, the volume of liquid soap is increased by I being mixed with water or other suitable fluid, such as alcohol or acetone, which reduces its density to permit freer flow, besides bein thinned out considerably. The thinning uid is fed into the vat 2 through the valve 5 and pipe 6. This fluid is mixed with the soapy solution b means of an ordinary wire stirrer 7 usual y employed where a mixing action is preferable over an ebulliting or kneading action. The stirrer 7 is carried u on a shaft 8 which. is driven by any suita lc means, as for instance by a belt 9. A hot air jacket 10 surrounds the mixing vat 2 to keep the contents thereof at a certain temperature.
From the vat 2 the liquid soap of reduced consistency is fed through the valve 11 into the whipping vat 12, which, as shown, is of the ordinary type. The whi per comprises simply the be t driven sha 13 carrying wires or rods 14, which stir and aerate the material. The construction is such that the stirring instrumentalities, i. e. wires or rods, ass through the viscid mass with a smoot -cutting as again distinguished from either an ebullitin or kneading action, whereby there is o tained indefinitely repeated cutting of the occluded air into smaller and smaller subdivisions with comparatively small levitation or expulsion thereof,
' roundin or conversion of the mass throughout into froth or foam. In this machine, the liquid soap is brou ht into a foaming mass. During the aerating step, the li uid soap is kept main upon the belt and will spread evenly thereover by its own action. As the belt travels along its upper horizontal run, warm air of sufficient avidity to remove the moisture is directed against the soap by'means of the blower 18 and manifold 19 having any number of jets 20 from which the air is emitted. By the time the soap reaches the end of the belts horizontal run, it will be of a spongy and friable nature, that is, there will be a tendency for it to crumble into fine flakes as soon as it is disturbed. It is here proposed to ating an abrupt break in the straight run of the belt. The comparatively small diameter roller 21 serves this purpose, while, if so desired, an auxiliary means may be used to remove soa which persists in clinging to the belt. This auxiliary means is in the form of one or more blades 22,which lightly bear against the belt ing the same. It is to be noted that the flakes are permitted to drop practically untouched into the receptacle 23, which prevents lumping. It is further to be noted that the use of this particular process will produce a flake, which is very spongy in character, and which is friable, so that it will immediately break or crumble into bits when disturbed; the flake having a great avidity to dissolve instantly upon mixing with a washing fluid.
An alternative process for flaking soap is shown in Figure 2. In this instance, the liquid soap is taken from the cooking vat (not shown) with a consistency of about 25% moisture, and fed through the supply pipe 25", the flow being controlled by the va ve 26, to the vat 27. The liquid soap, while in this vat 27, is kept at a certain temperature to prevent cooling oif which is apt to result in crusting, but this has been found provide such disturbance by crewithout wearing or destrovnot necessary. With the soap in such state,
gtraveling surface 30 in a thin sheet. This flake from the traveling surface.
.tion of the belt run horizontal.
sheet of soap is advanced under the streams of warm air emitted from the jets of the manifold 19. The length of the belts horizontal run is such as will permit a manifold of sufiicient capacity to be used to desiccate the soap film, and also permit adequate cooling of the soap film before it is disturbed and crumbled into flakes;
By referringi to Figure 3, an alternate suggestion for esieeating the soap filmfupon the traveling surface will beseen. It is considered a matter of ordinary mechanical skill to propose a different method fordesiccating the soap upon the surface 30, as the scope of the present invention should extend to any method of desiccation. The particular construction shown in Figure 3 comprises a warm air oven 33 through which the surface is led. Freely rotating rollers may be mounted within this warm air oven 33 and adjusted so as to engage lightly the pellicle of soap on the belt. Thiswill, more or less,
roll out the pellicle soap in a positive fashion, the purpose being print rily to remove the gloss and to prevent crusting of the surface, which causes uneven drying.
From experience it-has been found that soap flakes will remain in a very much better condition if thoroughly cooled before lacing in packages; while oftentimes a finer quality of flake is obtained by removing the heat' before itis crumbled. A cool air chamber 34 is provided for this purpose and 'the soap,'interposed therebetween. Thus, no
element comes into contact with the soap,
.afterit has been desiccated, to crumble it.
Without further elaboration, the foregoing will so fully explain the gist of my invention', that others may, by applying current knowledge, readily adapt the same for use under varying conditions of service. The invention is not to be limited to aerating to cause frothing of-the liquid soap before it is spread upon'the belt. The invention will, however, produce a flake which is very desirable, being spongy, friable, and of a very soluble character. The feature of spraymg a thin film of soapy solution upon a traveling (horizontal) surface, against which is directed currents of warm an, and then disturbing the desiccated soap by changing the direction of travel of the surface, is considered of importance. However. the
general mode of operation may obviously be changed without eliminating important parts, which may properly be said to con-. stitute the essential featuresof novelty involved in my invention.
' The invention aims to produce a soap flake Jf higher quality over what has heretofore been made. To this end, a process is suggested, the nature of which is such that various steps maybe omitted without deviating from the invention with respect to chang ing the nature of flake produced, as is contemplated within the limits of the present case. Of the steps that may be omitted or interchanged, that of aerating to increase the volume per unit of weight is mentioned. Variation of this latter step is possible within a wide range, and hence, it is the increased volume which issought. Laying the liquid soap on the belt by a sprayer may be omitted when the aeratingor other volume increasing means are employed.
I claim: I V
-1. The methodof flaking soap which comprises first spraying it wh1l 'e in liquid form into a thin fi m,next, operating upon the film to cause desiccation, and finally, disturbing the desiccated film to cause disintegration into flakes.
. 2. The method of flaking soap which comprises first laying a layer of liquid soap upon a surface, next, conditioning said soap while upon the surface by desiccation to rei an move substantially the entire moisture thereinfand finally, breaking said soap into pieces by changing the contour of said surface after said conditioning has taken place.
3. The method of flaking soap which comprises first spraying liquid soap upon a moving surface, next, passing said surface through a desiccation zone to remove the moisture in the soap, and finally, removing the soap in flaked condition from said surface.
4. The method of flaking soap whichcomprises first spraying a thin filmof liquid soap upon a traveling surface, next, passing said surface through a hotair zone to remove the moisture contained in the soap,
next, changing the travel of said surface to cause breaking .up of said soap, and finally, scraping said surface to remove whatever soap that remains thereon.
5. The methodfof flaking soap which comprises, first spraying a thin film-of liquid soap upon a traveling surface, next, passing said surface through a hot air zone to re move the moisture contained in the soap,
next, passing said surfacethrough a cooling zone to lower the temperature of the desiccated soap, and finally, changing the travel of said surface to cause breaking up of said soap.
- 6. The method of flaking soap which comsai prises first spraying a thin film of liquid soa upon a traveling surface, next, passing surface through a hotair zone to remove the moisture contained in the soap, and next, passing said surface through a cooling zone to lower the temperature of the desiccated soap before removing soap from said surface and finally removing the desiccated soap in the form of flakes.
7. In the method of flaking soap which comprises first reducing the density of a body of liquid soap so that it will be of a desired consistency, next, converting the body of liquid soap into an aerated and foamy mass, next, shaping said mass into a film of desired thickness, next, drying said sheet, and finally, producing flakes therefrom.
8. In the method of flaking soap which comprises first converting a body of liquid soap into a frothy or foamy mass, next, layin said mass upon a surface in form of a su stantially thin sheet, and finally, drying said sheet so as to render the same friable and crumbly, whereby to divide said sheet into flakes.
9. In the method of flaking soap which comprises first mixing a thinnmg fluid with a body of liquid soap, next, whipping said body of liquid soap into a froth, next, desiceating to any des'ired degree, the frothed soap to render it friable, and finally flaking the soap.
10. In the method of flaking soap which comprises first mixing a thinning fluid with a body of liquid soa next, frothing said body of liquid soap by whipping and admitting air thereinto, next, placing the soa upon an exposed surface, next, passing said surface through a. desiccating zone to dry said soap, and finally flaking the soap.
- 11. In the method of flaking soap which comprises first mixing a thinnin fluid with a body of liquid soap, next, a mitting air into said body of liquid soap by whipping, next, placing the aerated liquid soap 'uponh traveling surface, next, desiccating said aerated li uid soap, and finally, removing the aerate soap in form of crumbled flakes by disturbing said traveling surface.
12. In the method of flaking soap which comprises first aerating by whipping a body of liquid soap, next spraylng the aerated liquid soa upon a traveling surface, next, desiccating said aerated soap, and finally, removing the aerated soap in form of crumbled flakes by disturbing said traveling surface.
13. In combination, a source of liquid soap, 1!. vat for receiving said liquid soap an apron, means for removing said liquid soap from said vat to place it u on said apron in a thin sheet, means for currents of air of sufiicient avidity to remove moisture from said sheet of soap, and
irecting means substantially at the end of said apron to crumble and remove said soap.
1 1. In combination, a source of liquid soa a traveling apron, means for placing sai soap upon said apron in form of a thin sheet, means for desiccating said sheet of soap while on said apron, thedirection of travel of said apron being changed to crumble said soap into flakes, and additional means for assistlng in removing said soap from said apron.
15. In combination, a source of liquid soap, an apron, a sprayer for spraying said liquid soap upon said apron, a hot air zone through which said apron is passed, a cold air zone through which said apron also is passed, and means for disturbing said apron substantially at its end to crumble the soap into flakes.
16. In combination, a source of liquid soap, means for converting'the liquid soap into a froth, a sprayer for spraying said froth upon an a ion, a desiccating zone for rendering said roth in a friable condition, and means for disturbing the friably conditioned froth so as to remove it from the apron in form of flakes.
17 In combination, a source of liquid soap, a converter for converting said liquid soap into a froth, a sprayer for spraying the froth upon an apron, a warm air zone for removing moisture from said froth, a cool air zone for removing heat from said froth, and means at the end of the apron to disturb said froth.
18. The method of producing soap flakes having a high degree of porosity and easily soluble in water which comprises spraying liquid soap of a hi h air content upon a moving surface, an then. removing the moisture or hardening the soap whereupon the air is allowed to escape and the soap rendered friable and finally disintegrating the same into flakes.
19. The method ofproducing soap flakes having a high degree of porosity and easily soluble in water which comprises spraying in fine clouds a liquid soa of a bi h air content upon a moving sur ace where the air may be readily released during the ardening of the soap, and finally disturbing the soap so that it will crumble into flakes of crystalline appearance upon being removed from said surface.
20. The method of producing soap flakes having a high degree of porosity an easily soluble in water which comprises taking li uid soa of any density and adding a thinning uid thereto whereby the liquid soap may be given a desired volume of air by subsequent agitation, then applying the soap to a surface in a manner to continue the agitation and the admixture of air with the soap but upon being spread upon said surface to effect a release of the air during a subsequent drying or hardening step, and
finally removin the soap from said surface in the form of akes or like particles.
21. The method of producing soap flakes easily soluble in water which comprises sprayingliquid soap of a high air content upon a moving surface in a substantially thin layer whereby upon hardening of the soap the walls thlereof confining the air therein will contract'and release the air, and 10 finally removing the hardened air-freed soap from said surface for disintegration into separate flakes or particles. 7
In Witness whereof, I hereunto subscribe my name 11th day of August, 1921.
BERTRAM WM; COLTMAN.
US492214A 1921-08-15 1921-08-15 Process of and means for flaking soap Expired - Lifetime US1653390A (en)

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US18546D USRE18546E (en) 1921-08-15 Pbocess of and means fob flaking soap
US492214A US1653390A (en) 1921-08-15 1921-08-15 Process of and means for flaking soap
US241361A US1718778A (en) 1921-08-15 1927-12-20 Soap flakes

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Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2571459A (en) * 1945-11-05 1951-10-16 Fmc Corp Method of and apparatus for producing dried whole eggs
US2773753A (en) * 1953-01-06 1956-12-11 Commercial Solvents Corp Process for producing ammonium nitrate of any desired size particle
US2902719A (en) * 1955-01-07 1959-09-08 Diamond Alkali Co Preparation of easily friable crystalline substances by a melt casting process
US2946655A (en) * 1957-08-22 1960-07-26 Koppers Co Inc Production of diammonium phosphate
US2996114A (en) * 1957-04-11 1961-08-15 Lowe Edison Method and apparatus for vacuum dehydration
US3064722A (en) * 1960-01-11 1962-11-20 Jr Arthur I Morgan Production of carbohydrates in readily dispersible form

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2571459A (en) * 1945-11-05 1951-10-16 Fmc Corp Method of and apparatus for producing dried whole eggs
US2773753A (en) * 1953-01-06 1956-12-11 Commercial Solvents Corp Process for producing ammonium nitrate of any desired size particle
US2902719A (en) * 1955-01-07 1959-09-08 Diamond Alkali Co Preparation of easily friable crystalline substances by a melt casting process
US2996114A (en) * 1957-04-11 1961-08-15 Lowe Edison Method and apparatus for vacuum dehydration
US2946655A (en) * 1957-08-22 1960-07-26 Koppers Co Inc Production of diammonium phosphate
US3064722A (en) * 1960-01-11 1962-11-20 Jr Arthur I Morgan Production of carbohydrates in readily dispersible form

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