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US1390676A - Apparatus for evaporating liquids - Google Patents

Apparatus for evaporating liquids Download PDF

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US1390676A
US1390676A US144650A US14465017A US1390676A US 1390676 A US1390676 A US 1390676A US 144650 A US144650 A US 144650A US 14465017 A US14465017 A US 14465017A US 1390676 A US1390676 A US 1390676A
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shell
vapor
liquid
evaporating
valve
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US144650A
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Baufre William L De
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/28Evaporating with vapour compression
    • B01D1/284Special features relating to the compressed vapour
    • B01D1/2843The compressed vapour is divided in at least two streams

Definitions

  • My invention relates to the evaporation of liquids, including solutions of salt, sugar, etc., and has for its object'a reduction in the extent of heating surface required for the evaporation of a given quantity of vapor or the concentration of a given quantity of solution.
  • a further object of my invention is an improvement in the economy of the operation, especially in connection with the employment of a compressor to compress vapor from the liquid undergoing evapora tion for the purpose of using the compressed va or to heat the liquid.
  • the drawing shows the combination regenerative and multiple-efl'ect plant proposed to accomplish the object specified above,
  • the several evaporator shells are numbered 1, 2, 3, 4, respectively; 5 is a preheater and 6 a condenser.
  • An ejector 7 is connected to withdraw through valve 8 from the evaporating chamber of shell 1 the vapor produced therein.
  • the steam to operate ejector 7 is supplied through valve 9 from steam main 10, and the commingled steam and compressed vapor passes ,through valve 15 into the.
  • evaporator tubes 11 which comprise the condensing chamber of shell 1.
  • Shell 3 with tubes 13 thus constitutes the second-enact of a multiple-effect arrangement, in which shell 2 with tubes 12 constitutes the first effect and shell 4 with tubes 14 constitutes the third-effect.
  • Shell 1 with. tubes 11 may be called the regenerative eflect of the plant. lVhile more than three effects can be provided, the drawing shows the vapor from shell 4 passing through pipe 19 I to condenser 6.
  • valves 22 and 23 With valv 23 open, a part of the vapor from shell 4 will pass through pipes 20 and 21 to preheater 5., Reversing the positions of valves 22 and 23 so that the feed heater is supplied with steam from the first efi'ect rather than from the last effect results in "a higher temperature of the liquid fed to shell 1.
  • the commingled steam andvapor supplled tubes 11 may be augmented by exhaust steam through valve 29 from exhaust main 28-.
  • Valve 30 is provided in order to allow the regenerative effect? (shell 1) to become a part of the first effect (shell 2) should it be desired at times to operate the plant with valve 8 closed.
  • the condensed steam and vapor intubesv 11, 12, 13,14, and in preheater 5, are discharged by traps 31, 32, 33, 34, and 35, respectively, through drain main 36 to tank 37 or through drain main 38 to condenser 6 as shown in the drawing.
  • the vapor condensed in condenser 6 and the condensate discharged therein are removed by pump 24 together with any non-condensable gases present, and the condensate may be stored in tank 39.
  • the above arrangement is suitable when the last two effects are worked under i single chamber.
  • shells 1 and 2 may be. combined to simplify the construction, two evaporating chambers and one condensing chamber being provided in a single shell.
  • shells 1, 2, 3, 4 are filled to the working level with the liquid to be evaporated, drawn by pump 26 from storage tank 48 and forced through preheater 5 and through valve 41 into shell 1, thence through valve 42 into shell 2, thence through valve 43 into shell 3, and thence through valve 44 into shell 4, valve 45 being closed. Pump 24 and condenser 6 are next put into operation.
  • valve 29 If exhaust steam is available, the system may be heated by opening valve 29. Other- Wise, valves 15 and 9 should be opened to admit live steam from main 10.
  • the liquid in shells 1 and 2 will be heated by the condensation of the live or exhaust steam within tubes 11 and 12, which practically form a
  • the vapor from shells 1 and 2, valve 30 being open, will heat the liquid in shell 3 by condensation within tubes 13, and the liquid in shell 4 will be heated by the condensation within tubes 14 of vapor from shell 3.
  • the vapor from shell 4 will be condensed in condenser 6.
  • Valve 22 or valve 23 may now be opened as desired to supply vapor for preheating the solution fed to shell 1.
  • the vapor condensed in preheater' 5 and shells 1 and 2 Will be automatically discharged into tank 37 by traps 35, 31 and 32, respectively. Th condensation in tubes 13 and 14 will be discharged by traps 33 and 34 into condenser 6, from which it and the vapor condensed therein will be removed by pump 24 and discharged into tank 39.
  • valve 30 When the liquid in shell 1 becomes sufficiently heated, valve 30 may be closed and valve 8 opened. The vapor produced in shell 1 will then be entrained in the live steam in ejector 7, compressed and forced into tubes 11.
  • valves 41, 42, 43, 44 As soon as an appreciable evaporation takes place, it becomes necessary to regulate valves 41, 42, 43, 44, to maintain the proper liquid levels in shells 1, 2, 3, 4, respectively.
  • the speed ot pump 24 will be regulated by means o l throttle valve 25 to maintain the proper vacuum in condenser (i and remove the condenser vapor therein; the speed ol pump 46 will be regulated by throttle valve 47 to remove the concentrated liquid from shell 4 and thus maintain the proper concentration therein; and the speed of feed pump 26 will be regu lated by throttle valve 27 to maintain the proper rate of feed.
  • Feed valves 41, 42, 43, 44 must be adjusted to preserve the proper working levels of the liquid undergoing col1- centration or evaporation within shells 1, 2, 3, 4, respectively.
  • the difference between the temperature of the condensing steam or vapor and that of the vapor produced may be made larger within shell 2 than within shell 1, within shell 3 than within shell 2, and so on,.increasing as the liquid becomes denser and more viscous.
  • This is especially advantageous for shells 1 and 2, particularly when no additional shells are used, and a greater temperature difference may readily be obtained in shell 2 than available within shell 1 with reasonable economy of the ejector 7; thus, after the liquid has been partially concentrated within shell 1, the final concentration may be carried out within shell 2 under a greater temperature difierence.
  • a vapor operated compressor for Withdrawing and compressing vapor from the first oi the said evaporating chambers and discharg ing the compressed vapor commingled with the operating vapor into the communicating condensing chambers, means to discharge liquid from the first to the second evaporat ing chamber,-n1eans for discharging "vapor from the second of the said evaporating chambers at a lower temperature than that in the first evapo 'ating chamber independent of the first evaporating chamber.
  • two evaporating chambers containing the said liquid non-communicating above the liquid level and separated by heating surfaces from communicating condensing chambers under substantially the same pressure, means for discharging liquid from the first to the second evaporating chamber, a vapor operated compressor for Withdrawing and compressing vapor from the first of the said evaporating chambers and discharging the compressed vapor commingled with the operating vapor into the communicating condensing chambers, and means for discharging vapor from the other of said evaporating chambers independent of the first evaporating chamber.
  • tvvo evaporating chambers contain ingthe said liquid non-communicating above the liquid ievel and so by heat-- ingsuriaces irons communio sting condens ing chambers under subs itiali v the same pressure, means ior disch liquid irom the iirst to the s cond evapo chamber, means tor Wit dravvi and compressing vapor from the oi 1 chambers l evaporating and ior introducing com-- pressed vapor into the communicating con-- densing chambers, means tor discharging vapor from the other oi the said evaporating chambers independent oi the iirst evapcrating chamber, and means ior introducing additional vapor into the communicating condensing chambers,
  • an evaporating chamber containing the said liquid separated by a heating surface from a condensing chamber means for Withdrawing and compressing vapor from the said evaporating chamber and of intro ducing the compressed vapor into the said condensing chamber, a second evaporating chamber separated by a heating surface from. a second condensing chamber, means for discharging the said liquid from the first evaporating chamber into the second evaporating chamber, means for discharging vapor irom the first condensing chamber into the second condensing chamber, and means for discharging vapor from the second evaporating chamber independent of the first evaporating chamber,

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Description

W. L. DE BAUFHE. APPARATUS FOR EVAPORATING LIQUIDS. APPLECATION FILED mzzs, 1917.
1,390,676. Patented Sept. 13,1921.
Ill" ll" lmwnfor WMM 1 WM f 4% @w UNITED STATES.
PATENT OFFICE.
WILLIAM L. DE BAUFRE, 0F ANNAPOLIS, MARYLAND.
AIPARATUS FOR EVAPORATING LIQUIDS.
To all whom it may concern:
Be it known that 1, WILLIAM L. DE BAU- rnn, a citizen of the United States, residing at Annapolis, in the county of Anne Arundel and State of Maryland, have invented a cer tain new and useful Apparatus for Evaporating Liquids, of which the following is a specification.
My invention relates to the evaporation of liquids, including solutions of salt, sugar, etc., and has for its object'a reduction in the extent of heating surface required for the evaporation of a given quantity of vapor or the concentration of a given quantity of solution. A further object of my invention is an improvement in the economy of the operation, especially in connection with the employment of a compressor to compress vapor from the liquid undergoing evapora tion for the purpose of using the compressed va or to heat the liquid.
Vith the foregoing and other objects in view, my invention consists of the novel construction, combination and arrangement of parts as hereinafter specifically described and illustrated in the accompanying drawing, wherein is shown the preferred embodiment of my invention, but it is understood that changes; variations and modifications can be resorted to which come within the scope of the claims hereunto appended.
The drawing shows the combination regenerative and multiple-efl'ect plant proposed to accomplish the object specified above, The several evaporator shells are numbered 1, 2, 3, 4, respectively; 5 is a preheater and 6 a condenser. An ejector 7 is connected to withdraw through valve 8 from the evaporating chamber of shell 1 the vapor produced therein. The steam to operate ejector 7 is supplied through valve 9 from steam main 10, and the commingled steam and compressed vapor passes ,through valve 15 into the. evaporator tubes 11 which comprise the condensing chamber of shell 1.
Since there is discharged from shell 1 onl the vapor which is compressed in ejector and returned to tubes 11, all the commingled steam and compressed vapor will not be condensed therein. In fact, there must be discharged through connecting pipe 16 into tubes 12 of shell 2 nearly one pound of commingled steam and vapor for each pound of steam supplied ejector 7 through valve 9. The condensation of the commingled Steam Specification of Letters Patent. P t hmd Sept 13, 1921 Application filed January 26, 1917.
Serial No. 144,650.
and vapor in this second condensing chamber (tubes 12) will produce nearly an equal quantity of vapor in the second evaporating chamber (shell 2).
With yalve 22 closed, this vapor from shell w1ll all pass through connecting pipe 17 to the tubes 13 of shell 3. Shell 3 with tubes 13 thus constitutes the second-enact of a multiple-effect arrangement, in which shell 2 with tubes 12 constitutes the first effect and shell 4 with tubes 14 constitutes the third-effect. Shell 1 with. tubes 11 may be called the regenerative eflect of the plant. lVhile more than three effects can be provided, the drawing shows the vapor from shell 4 passing through pipe 19 I to condenser 6.
With valv 23 open, a part of the vapor from shell 4 will pass through pipes 20 and 21 to preheater 5., Reversing the positions of valves 22 and 23 so that the feed heater is supplied with steam from the first efi'ect rather than from the last effect results in "a higher temperature of the liquid fed to shell 1.
The commingled steam andvapor supplled tubes 11 may be augmented by exhaust steam through valve 29 from exhaust main 28-. Valve 30 is provided in order to allow the regenerative effect? (shell 1) to become a part of the first effect (shell 2) should it be desired at times to operate the plant with valve 8 closed.
The condensed steam and vapor intubesv 11, 12, 13,14, and in preheater 5, are discharged by traps 31, 32, 33, 34, and 35, respectively, through drain main 36 to tank 37 or through drain main 38 to condenser 6 as shown in the drawing. "The vapor condensed in condenser 6 and the condensate discharged therein are removed by pump 24 together with any non-condensable gases present, and the condensate may be stored in tank 39. The above arrangement is suitable when the last two effects are worked under i single chamber.
lated either by pump throttle valve 27 or by feed valve 41. From shell 1 the partially concentrated liquid passes to shell 2 through valve 42 Where it is further concentrated, through valve 43 to shell 3 where it is still further concentrated, and finally to shell 4 through valve 44, and from thence the completely concentrated liquid is drawn by pump 46 through valve 45 and discharged into storage tank 40.
It should be noted that the system is operative With a greater number than three effects, or with the regenerative effect and first effect only. Also, shells 1 and 2 may be. combined to simplify the construction, two evaporating chambers and one condensing chamber being provided in a single shell.
The operationof this apparatus for evaporating liquids is carried out as follows:
First, shells 1, 2, 3, 4, are filled to the working level with the liquid to be evaporated, drawn by pump 26 from storage tank 48 and forced through preheater 5 and through valve 41 into shell 1, thence through valve 42 into shell 2, thence through valve 43 into shell 3, and thence through valve 44 into shell 4, valve 45 being closed. Pump 24 and condenser 6 are next put into operation.
If exhaust steam is available, the system may be heated by opening valve 29. Other- Wise, valves 15 and 9 should be opened to admit live steam from main 10. The liquid in shells 1 and 2 will be heated by the condensation of the live or exhaust steam within tubes 11 and 12, which practically form a The vapor from shells 1 and 2, valve 30 being open, will heat the liquid in shell 3 by condensation within tubes 13, and the liquid in shell 4 will be heated by the condensation within tubes 14 of vapor from shell 3. The vapor from shell 4 will be condensed in condenser 6. Valve 22 or valve 23 may now be opened as desired to supply vapor for preheating the solution fed to shell 1.
The vapor condensed in preheater' 5 and shells 1 and 2 Will be automatically discharged into tank 37 by traps 35, 31 and 32, respectively. Th condensation in tubes 13 and 14 will be discharged by traps 33 and 34 into condenser 6, from which it and the vapor condensed therein will be removed by pump 24 and discharged into tank 39.
When the liquid in shell 1 becomes sufficiently heated, valve 30 may be closed and valve 8 opened. The vapor produced in shell 1 will then be entrained in the live steam in ejector 7, compressed and forced into tubes 11.
As soon as an appreciable evaporation takes place, it becomes necessary to regulate valves 41, 42, 43, 44, to maintain the proper liquid levels in shells 1, 2, 3, 4, respectively.
This may be done manually, or automatically by well known devices for this purpose.
It now becomes necessary to observe the concentration oi" the liquid in the last eil'cct, shell 4, and when this concentration reaches the maximum desired, to start pump 46 and open valve 45, to withdraw the concentrated liquid for storage in tank 40.
During normal operation, the speed ot pump 24 will be regulated by means o l throttle valve 25 to maintain the proper vacuum in condenser (i and remove the condenser vapor therein; the speed ol pump 46 will be regulated by throttle valve 47 to remove the concentrated liquid from shell 4 and thus maintain the proper concentration therein; and the speed of feed pump 26 will be regu lated by throttle valve 27 to maintain the proper rate of feed. Feed valves 41, 42, 43, 44 must be adjusted to preserve the proper working levels of the liquid undergoing col1- centration or evaporation within shells 1, 2, 3, 4, respectively.
\Vith a given vacuum maintained in shell 4 by condenser (5 and a given initial steam pressure at valve S), the several intermediate pressures and temperatures in shells l, 2, 3, 4, will be determined by the physical properties of the liquid undergoing evaporation and the liberality of design of the several effects. In fact, the conditions within shells 2, 3, and 4, will be but slightly dill'erent from those obtaining in an ordinary tripleefiect plant of the same dimensions using the same quantity of steam as supplied this combination plant. In shell 1, the pressure dilterence will be determined by .the etliciency of ejector 7 and the ellicacy of the heating surface in tubes 11.
By proper design, the difference between the temperature of the condensing steam or vapor and that of the vapor produced may be made larger within shell 2 than within shell 1, within shell 3 than within shell 2, and so on,.increasing as the liquid becomes denser and more viscous. This is especially advantageous for shells 1 and 2, particularly when no additional shells are used, and a greater temperature difference may readily be obtained in shell 2 than available within shell 1 with reasonable economy of the ejector 7; thus, after the liquid has been partially concentrated within shell 1, the final concentration may be carried out within shell 2 under a greater temperature difierence.
Having thus described my invention, I claim and desire to secure by Letters Patent, the following:
1. In an apparatus for e\ aporating a liquid, two evaporating chambers containing the said liquid non-cominunieating above the liquid level and separated by heating sur-v faces from communicating condensing sham:
camera here under substantially the same pressure, a vapor operated compressor for Withdrawing and compressing vapor from the first oi the said evaporating chambers and discharg ing the compressed vapor commingled with the operating vapor into the communicating condensing chambers, means to discharge liquid from the first to the second evaporat ing chamber,-n1eans for discharging "vapor from the second of the said evaporating chambers at a lower temperature than that in the first evapo 'ating chamber independent of the first evaporating chamber.
2. In an apparatus for evaporating" a liquid, two evaporating chambers containing the said liquid non-communicating above the liquid level and separated by heating surfaces from communicating condensing chambers under substantially the same pressure, means for discharging liquid from the first to the second evaporating chamber, a vapor operated compressor for Withdrawing and compressing vapor from the first of the said evaporating chambers and discharging the compressed vapor commingled with the operating vapor into the communicating condensing chambers, and means for discharging vapor from the other of said evaporating chambers independent of the first evaporating chamber.
3. In an apparatus for evaporating a liquid, two evaporating chambers containing the said liquid non-communicating above the liquid level and separated by heating surfaces from communicating condensing chambers under substantially the same pres sure, means for discharging liquid from the first to the second evaporating chamber, means for Withdrawing and compressing va por from the first of the said evaporating chambers and for introducing the compressed vapor into the communicating con (lensing chambers, and means for discharging vapor irom the other not aid evaporating chambers independent; oi the iirst evapora'h ing chamber,
l. in an apparatus t r evaporating a liquid, tvvo evaporating chambers contain ingthe said liquid non-communicating above the liquid ievel and so by heat-- ingsuriaces irons communio sting condens ing chambers under subs itiali v the same pressure, means ior disch liquid irom the iirst to the s cond evapo chamber, means tor Wit dravvi and compressing vapor from the oi 1 chambers l evaporating and ior introducing com-- pressed vapor into the communicating con-- densing chambers, means tor discharging vapor from the other oi the said evaporating chambers independent oi the iirst evapcrating chamber, and means ior introducing additional vapor into the communicating condensing chambers,
5, In an apparatus tor evaporating a liquid, an evaporating chamber containing the said liquid separated by a heating surface from a condensing chamber, means for Withdrawing and compressing vapor from the said evaporating chamber and of intro ducing the compressed vapor into the said condensing chamber, a second evaporating chamber separated by a heating surface from. a second condensing chamber, means for discharging the said liquid from the first evaporating chamber into the second evaporating chamber, means for discharging vapor irom the first condensing chamber into the second condensing chamber, and means for discharging vapor from the second evaporating chamber independent of the first evaporating chamber,
WILLIAM L. DE BAUFRE.
Witnesses:
GEORGE F. CRUIT, A. J. G, BABEL.
dill
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2440173A (en) * 1942-06-15 1948-04-20 Roy O Henszey Multiple effect still with thermocompression of vapors
US2793502A (en) * 1948-11-19 1957-05-28 Frederick W Riehl Method and apparatus for utilizing exhaust steam

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2440173A (en) * 1942-06-15 1948-04-20 Roy O Henszey Multiple effect still with thermocompression of vapors
US2793502A (en) * 1948-11-19 1957-05-28 Frederick W Riehl Method and apparatus for utilizing exhaust steam

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