TWM605507U - High performance vacuum furnace - Google Patents
High performance vacuum furnace Download PDFInfo
- Publication number
- TWM605507U TWM605507U TW109207467U TW109207467U TWM605507U TW M605507 U TWM605507 U TW M605507U TW 109207467 U TW109207467 U TW 109207467U TW 109207467 U TW109207467 U TW 109207467U TW M605507 U TWM605507 U TW M605507U
- Authority
- TW
- Taiwan
- Prior art keywords
- evaporation tray
- tray
- chamber space
- collecting
- vacuum furnace
- Prior art date
Links
- 238000001704 evaporation Methods 0.000 claims abstract description 101
- 230000008020 evaporation Effects 0.000 claims abstract description 100
- 238000010438 heat treatment Methods 0.000 claims abstract description 45
- 230000008018 melting Effects 0.000 claims abstract description 21
- 238000002844 melting Methods 0.000 claims abstract description 21
- 230000007246 mechanism Effects 0.000 claims abstract description 12
- 238000000605 extraction Methods 0.000 claims abstract description 6
- 125000006850 spacer group Chemical group 0.000 claims description 7
- 238000009833 condensation Methods 0.000 abstract description 13
- 230000005494 condensation Effects 0.000 abstract description 13
- 229910052751 metal Inorganic materials 0.000 description 33
- 239000002184 metal Substances 0.000 description 31
- 239000000463 material Substances 0.000 description 27
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 25
- 238000010586 diagram Methods 0.000 description 24
- 229910001174 tin-lead alloy Inorganic materials 0.000 description 18
- 239000012535 impurity Substances 0.000 description 14
- 238000000926 separation method Methods 0.000 description 12
- WABPQHHGFIMREM-UHFFFAOYSA-N lead(0) Chemical compound [Pb] WABPQHHGFIMREM-UHFFFAOYSA-N 0.000 description 10
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 7
- 238000010248 power generation Methods 0.000 description 7
- 238000005292 vacuum distillation Methods 0.000 description 7
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 238000005516 engineering process Methods 0.000 description 5
- 239000003923 scrap metal Substances 0.000 description 5
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 4
- 229910052802 copper Inorganic materials 0.000 description 4
- 239000010949 copper Substances 0.000 description 4
- 238000001514 detection method Methods 0.000 description 4
- 239000007787 solid Substances 0.000 description 4
- 229910045601 alloy Inorganic materials 0.000 description 3
- 239000000956 alloy Substances 0.000 description 3
- 229910052787 antimony Inorganic materials 0.000 description 3
- 229910010293 ceramic material Inorganic materials 0.000 description 3
- 229910052742 iron Inorganic materials 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 238000012806 monitoring device Methods 0.000 description 3
- 229910052759 nickel Inorganic materials 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- 230000009471 action Effects 0.000 description 2
- WATWJIUSRGPENY-UHFFFAOYSA-N antimony atom Chemical compound [Sb] WATWJIUSRGPENY-UHFFFAOYSA-N 0.000 description 2
- 229910052785 arsenic Inorganic materials 0.000 description 2
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 description 2
- JCXGWMGPZLAOME-UHFFFAOYSA-N bismuth atom Chemical compound [Bi] JCXGWMGPZLAOME-UHFFFAOYSA-N 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000007770 graphite material Substances 0.000 description 2
- 239000007791 liquid phase Substances 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000007769 metal material Substances 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 230000008520 organization Effects 0.000 description 2
- 239000012071 phase Substances 0.000 description 2
- 238000011084 recovery Methods 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- -1 antimony metals Chemical class 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 239000003779 heat-resistant material Substances 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000011344 liquid material Substances 0.000 description 1
- 229910001338 liquidmetal Inorganic materials 0.000 description 1
- 238000010310 metallurgical process Methods 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 230000001360 synchronised effect Effects 0.000 description 1
Images
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Waste-Gas Treatment And Other Accessory Devices For Furnaces (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
一種高效能真空爐,包括:本體、冷凝罩、進料裝置、第一集料盤、第二集料盤與熔化裝置;本體內部包含第一腔室空間、頂端有抽氣裝置;冷凝罩設於第一腔室空間內,包含加熱裝置、第一蒸發盤、第二蒸發盤、第三蒸發盤,第一蒸發盤設於加熱裝置頂端,第二蒸發盤與第三蒸發盤設於加熱裝置上;進料裝置包含進料管及進料容器,進料管一端連接進料容器,一端連接第一蒸發盤;第一集料盤設於冷凝罩下方,與第一出料管連接;第二集料盤設於第三蒸發盤下方,與第二出料管連接;熔化裝置包含給料機構,給料機構一端連接熔化裝置,一端連接進料容器。A high-efficiency vacuum furnace, comprising: a main body, a condensing hood, a feeding device, a first collecting pan, a second collecting pan, and a melting device; the body contains a first chamber space and an air extraction device at the top; the condensing cover It is arranged in the first chamber space and includes a heating device, a first evaporation tray, a second evaporation tray, and a third evaporation tray. The first evaporation tray is arranged at the top of the heating device, and the second evaporation tray and the third evaporation tray are arranged for heating On the device; the feeding device includes a feeding pipe and a feeding container, one end of the feeding pipe is connected to the feeding container, and one end is connected to the first evaporation tray; the first collecting tray is arranged under the condensation hood and connected to the first discharge pipe; The second collecting tray is arranged under the third evaporation tray and connected with the second discharge pipe; the melting device includes a feeding mechanism, one end of the feeding mechanism is connected with the melting device, and one end is connected with the feeding container.
Description
本新型揭示一種真空分離技術,尤指一種真空分離技術在冶金領域之運用。This model discloses a vacuum separation technology, especially the application of a vacuum separation technology in the field of metallurgy.
廢五金,如:廢銅、廢鋁、廢鐵、廢錫等,隨著經濟高度發展,廢五金的數量每年都以驚人的數量成長,如今隨著世界各地自然資源與物質的短缺,各國也開始重視金屬的再生,從廢五金中提煉純金屬,生產成本不僅較一般比原生金屬低廉,還可以充分利用的二次資源以補充金屬礦產資源的不足的現況,並免於環境受污染。Scrap hardware, such as: scrap copper, scrap aluminum, scrap iron, scrap tin, etc. With the rapid economic development, the amount of scrap hardware has grown in an astonishing amount every year. Nowadays, with the shortage of natural resources and materials around the world, countries are also Begin to pay attention to metal recycling, and extract pure metal from scrap metal. The production cost is not only lower than that of primary metal, but also can make full use of secondary resources to supplement the current situation of insufficient metal mineral resources and avoid environmental pollution.
在各類廢五金的資源回收處理作業上,然而,鉛金屬、鉍金屬於錫鉛合金中佔的比例往往很高,利用真空蒸餾機去除鉛金屬、鉍金屬為目前習知的技術,目前,冶金業者實現合金真空蒸餾分離所使用的主要設備為真空蒸餾爐,其廢金屬進料方式分為固態進料和液態進料兩種,但固態進料的方式缺點在於倒入真空蒸餾爐時,一次只能倒入固定的進料量,必須等該批倒入的物料處理完畢後,真空蒸餾爐才能處理下一批的物料,反觀液態進料的方式,藉由調控物料進入量與進料時間,即能達到連續生產的目的。In the resource recovery and processing operations of various scrap hardware, however, the proportion of lead metal and bismuth metal in the tin-lead alloy is often high. The use of a vacuum distillation machine to remove lead metal and bismuth metal is currently known technology. At present, The main equipment used by metallurgists to realize the vacuum distillation and separation of alloys is the vacuum distillation furnace. The scrap metal feeding method is divided into solid feeding and liquid feeding. However, the disadvantage of the solid feeding method is that when it is poured into the vacuum distillation furnace, Only a fixed amount of material can be poured at a time. The vacuum distillation furnace can only process the next batch of materials after the batch of materials are processed. In contrast to the way of liquid feeding, by adjusting the amount of material and the input Time can achieve the goal of continuous production.
因此,如何創作一種設備,在冶金過程中可以兼顧連續生產、製程簡單、金屬回收率高等特點,且該設備應用於廢錫時,能提高錫金屬和其他廢金屬分離程度,更純化錫金屬、為目前相關業者所亟欲解決之問題。Therefore, how to create a device that can take into account the characteristics of continuous production, simple manufacturing process, and high metal recovery rate in the metallurgical process, and when the device is used in scrap tin, it can improve the separation of tin metal and other scrap metals, and more purify tin metal, It is a problem that the related industry urgently wants to solve.
有鑒於此,本創作即在提供一種高效能真空爐,係包括:本體、冷凝罩、進料裝置、第一集料盤、第二集料盤與熔化裝置;本體,其內部包含有第一腔室空間,本體之頂端包含有抽氣裝置;冷凝罩,設於第一腔室空間內,並包含有加熱裝置、第一蒸發盤、複數個第二蒸發盤、第三蒸發盤,冷凝罩界定出第二腔室空間,第一蒸發盤係設於加熱裝置之頂端,第二蒸發盤與第三蒸發盤固設於加熱裝置上,且第一蒸發盤、第二蒸發盤及第三蒸發盤彼此為同心圓態樣,並以固定間距垂直堆疊設置於加熱裝置上;進料裝置,包含進料管及進料容器,進料管一端連接進料容器,另一端連接第一蒸發盤;至少一第一集料盤,設於冷凝罩下方,與第一出料管連接;至少第二集料盤,設於第三蒸發盤下方,與第二出料管連接;熔化裝置,包含給料機構,給料機構一端連接熔化裝置,另一端連接進料容器。In view of this, this creation is to provide a high-efficiency vacuum furnace, which includes: a main body, a condensing hood, a feeding device, a first collecting pan, a second collecting pan, and a melting device; the main body contains the first The chamber space, the top of the body contains an air extraction device; the condensation cover is arranged in the first chamber space and contains a heating device, a first evaporation tray, a plurality of second evaporation trays, a third evaporation tray, and a condensation cover The second chamber space is defined, the first evaporation tray is arranged on the top of the heating device, the second evaporation tray and the third evaporation tray are fixed on the heating device, and the first evaporation tray, the second evaporation tray and the third evaporation tray The discs are concentric with each other and are vertically stacked on the heating device at a fixed interval; the feeding device includes a feeding pipe and a feeding container, one end of the feeding pipe is connected to the feeding container, and the other end is connected to the first evaporation tray; At least one first collecting pan is arranged under the condensing hood and connected to the first discharge pipe; at least a second collecting disc is arranged under the third evaporating pan and connected to the second discharge pipe; a melting device including a feeder Mechanism, one end of the feeding mechanism is connected with the melting device, and the other end is connected with the feeding container.
所述之高效能真空爐,其中,第二腔室空間更包含蒸發盤蓋,係連接第一蒸發盤上,蒸發盤蓋更包含開孔,藉由開孔使第一腔室空間與第二腔室空間彼此連通。In the high-efficiency vacuum furnace, the second chamber space further includes an evaporation pan cover, which is connected to the first evaporation pan, and the evaporation pan cover further includes an opening. The opening allows the first chamber space and the second The chamber spaces communicate with each other.
所述之高效能真空爐,其中,第二蒸發盤及第三蒸發盤設置有穿孔。In the high-efficiency vacuum furnace, the second evaporation tray and the third evaporation tray are provided with perforations.
所述之高效能真空爐,其中,第二蒸發盤設置有至少透孔。In the high-efficiency vacuum furnace, the second evaporation tray is provided with at least through holes.
所述之高效能真空爐,其中,加熱裝置更進一步連接法蘭,藉由法蘭俾使第一腔室空間與第二腔室空間產生出空間區隔。In the high-efficiency vacuum furnace, the heating device is further connected to a flange, and the flange is used to create a space separation between the first chamber space and the second chamber space.
所述之高效能真空爐,其中,第一集料盤及第二集料盤中包含有複數間隔島,藉由間隔島使第一集料盤及第二集料盤間隔出複數間隙。In the high-efficiency vacuum furnace, the first collecting tray and the second collecting tray include a plurality of spacer islands, and the first collecting tray and the second collecting tray are separated by a plurality of gaps by the spacer islands.
所述之高效能真空爐,其中,第一腔室空間與第二腔室空間內溫度範圍係介於攝氏900度至攝氏1100度之間。In the high-efficiency vacuum furnace, the temperature range in the first chamber space and the second chamber space is between 900 degrees Celsius and 1100 degrees Celsius.
所述之高效能真空爐,其中,冷凝罩一側裝設有複數個集料管,集料管為傾斜設置。In the high-efficiency vacuum furnace, a plurality of collecting pipes are installed on one side of the condensing cover, and the collecting pipes are arranged obliquely.
所述之高效能真空爐,其中,集料管上設置有封蓋。In the high-efficiency vacuum furnace, a cover is provided on the collecting pipe.
所述之高效能真空爐,其中,給料機構包含控制裝置。In the high-efficiency vacuum furnace, the feeding mechanism includes a control device.
有關本創作之前述及其他技術內容、特點與功效,在以下配合參考圖式之較佳實施例的詳細說明中,將可清楚的呈現。在本創作被詳細描述之前,要注意的是,在以下的說明內容中,類似的元件是以相同的編號來表示。The aforementioned and other technical content, features, and effects of this creation will be clearly presented in the following detailed description of the preferred embodiment with reference to the drawings. Before this creation is described in detail, it should be noted that in the following description, similar elements are represented by the same numbers.
首先,請先參閱圖1,係顯示本創作之高效能真空爐1的示意圖。本創作之高效能真空爐1,係包括:一個本體2、一個冷凝罩3、一個進料裝置4、至少一個第一集料盤5與至少一個第二集料盤6。本體2,其內部包含有一第一腔室空間21,本體2之頂端包含有一抽氣裝置22,使用材料上,本體2較佳為金屬或陶瓷材料製成,外觀上,可為一圓柱體、正方體、長方體等任一構型所自由搭配組成,在一較佳實施例中,本體2為一鐘罩型構型;抽氣裝置22為一馬達,可分為直流馬達和交流馬達,若為直流馬達,可為有刷馬達、無刷馬達、步進馬達等任一者;若為交流馬達,可為誘導馬達、同步馬達等任一者。First of all, please refer to Figure 1, which is a schematic diagram showing the high-
請參閱圖2,係顯示本創作之高效能真空爐1的另一示意圖,另外,為了便於操作人員監控本創作之高效能真空爐1爐內反應情況,據此,本體2還另包含一監控裝置23,監控裝置23可實施態樣為:一影像擷取裝置、一觀察孔,若為一影像擷取裝置,其電性連接一顯示螢幕(未圖示),用以錄製本體2內的畫面,並於顯示螢幕播放監控影像;若為一觀察孔,其與本體2之間還連接一握持部231,以提供操作者或相關人士觀察握持,且握持部231使用材料為耐高溫材料,如:陶瓷材料、金屬材質等,在此,並不以為限。Please refer to Figure 2, which shows another schematic diagram of the high-
請參閱圖1配合參閱圖2及圖8,係分別顯示本創作之高效能真空爐1的示意圖、另一示意圖、及加熱裝置31立體示意圖。本新型之高效能真空爐1還包含一冷凝罩3,冷凝罩3設於第一腔室空間21內,並包含有一個加熱裝置31、一個第一蒸發盤32、複數個第二蒸發盤33、一個第三蒸發盤34,冷凝罩3界定出一第二腔室空間35,加熱裝置31係設計為一電柱,其電性連接一發電設備9,發電設備9提供電能於加熱裝置31,加熱裝置31係將電能轉變為熱能,用以加熱,在此,會因應所欲處理物料的特性而透過發電設備9調整加熱裝置31的溫度。而發電設備9更進一步包含一變壓器(未圖示),用以將來自外部電源透過變壓器降低其電流大小,其中,變壓器可採用單相供電、三相供電或星型供電等方式,在此,並不以為限。其中,單次執行本新型之高效能真空爐所消耗的電量較佳為500至600度/噸入爐原料。值得一提的是,加熱裝置31更進一步包含一個溫度偵測裝置(未圖示),藉由溫度偵測裝置得知目前第二腔室空間35內的溫度,進而與發電設備9連動,進行溫控動作。冷凝罩3與加熱裝置31使用材料上較佳為一石墨材料;外觀上,加熱裝置31為一圓柱體、正方體、長方體等任一構型所自由搭配組成;而冷凝罩3較佳為一鍾罩外觀。Please refer to Fig. 1 in conjunction with Figs. 2 and 8, which respectively show a schematic diagram of the high-
接續,請參閱圖1搭配參閱圖3、圖4與圖5,為本創作之高效能真空爐1的示意圖與第一蒸發盤32、第二蒸發盤33、及第三蒸發盤34的立體示意圖。第一蒸發盤32係設於加熱裝置31之頂端,第二蒸發盤33與第三蒸發盤34固設於加熱裝置31上,且第一蒸發盤32、第二蒸發盤33及第三蒸發盤34彼此為同心圓態樣,並以一固定間距垂直堆疊設置於加熱裝置31上。更進一步說明:第二蒸發盤33及第三蒸發盤34設置有一穿孔37,藉由穿孔37使第二蒸發盤33與第三蒸發盤34能穿過加熱裝置31並套接於上,且第二蒸發盤33設置有透孔331,且透孔331的數量可為一個或複數個,在此,並不以為限;形狀上,透孔331可為一圓型、一方形、一長方形等任一態樣,此外,第一蒸發盤32、第二蒸發盤33及第三蒸發盤34使用材料上較佳為一石墨材料;外觀上,為一圓體、橢圓體、長方體、方體等任一構型所自由搭配組成。更值得一提的是,本新型之高效能真空爐1能依據處理物料的不同及蒸餾速度,對應增設第二蒸發盤33及調控加熱裝置31的溫度,在此,不加以限制,在一較佳實施例中,第二蒸發盤33的數量為5至1個,較佳為3至1個,最佳為2個;第一腔室空間21與第二腔室空間35內溫度範圍係介於攝氏900度至攝氏1100度之間,較佳第一腔室空間21與第二腔室空間35內溫度係調控至攝氏1000度。For continuation, please refer to Figure 1 in conjunction with Figures 3, 4 and 5, which are a schematic diagram of the high-
請參閱圖1及圖2,係分別顯示本創作之高效能真空爐1的示意圖及另一示意圖。本創作之高效能真空爐1還包含一進料裝置4與一熔化裝置8,進料裝置4,包含一進料管41及一進料容器42,進料管41一端連接進料容器42,另一端連接第一蒸發盤32;外觀材質上,進料管41及進料容器42較佳為耐熱材質,如:陶瓷材料、金屬材質等,在此,並不以為限。熔化裝置8,包含一給料機構81,給料機構81一端連接熔化裝置8,另一端連接進料容器42。優選地,熔化裝置8為一熔化爐,用以將固態的物料加熱成液態金屬,其中,熔化裝置8單次倒入的物料量較佳為8至12噸;給料機構81包含一控制裝置(未圖示),控制裝置包含一電磁閥及一控制開關,藉由控制開關控制電磁閥工作,調節電磁閥的流量及啓停,實現物料自熔化裝置8流入至進料容器42的時間及流量的調節,其中,電磁閥可為直動式電磁閥、分布直動式電磁閥、先導式電磁閥或其他類似裝置。Please refer to Figures 1 and 2, which respectively show a schematic diagram and another schematic diagram of the high-
請繼續參閱圖1及圖2,透過馬達高速運轉,將第一腔室空間21內的空氣抽走,使本體2內部第一腔室空間21形成一真空狀態,使進料管41產生一虹吸作用,將進料容器42中的液態物料自進料管41吸至第一蒸發盤32上,在一較佳實施中,本體2內部壓力會降至1毫米汞柱(1mmHg)以下,較佳為降至0.6毫米汞柱(1mmHg)。Please continue to refer to Figures 1 and 2, the motor is running at high speed to draw out the air in the
請繼續參閱圖1配合參閱圖6及圖7,為本創作之高效能真空爐1的示意圖、第一集料盤5及第二集料盤6立體示意圖。本創作之高效能真空爐1包含一第一集料盤5,設於冷凝罩3下方,與一第一出料管51連接;以及一第二集料盤6,設於第三蒸發盤34下方,與一第二出料管61連接,結構設計上不僅可藉由卡環來讓第一集料盤5與第一出料管51和第二集料盤6與第二出料管61做套接卡固結合,亦可利用磁吸的方式,或增設凸點及凹點等態樣來達成相同的連結效果,其目的都是使集料盤和出料管彼此可以更穩固的連接,在此僅說明集料盤和出料管可實施樣式,並不以上述範例做為限制。再者,第一集料盤5及第二集料盤6中包含有複數間隔島7,藉由該等間隔島7使第一集料盤6及第二集料盤6間隔出複數間隙,使物料沿著間隔島7流動,用以集中將提煉出的物料集中自集料盤流至出料管內。Please continue to refer to Figure 1 in conjunction with Figures 6 and 7, which are a schematic diagram of the high-
接續,請參閱圖1配合參閱圖10,為本創作之高效能真空爐1的示意圖及冷凝罩3側面示意圖。由於本創作係利用真空蒸餾技術,透過廢金屬在不同溫度條件下的飽和蒸汽壓的差異進行真空分離,據此,為避免物料之間的露點相近,而無法有效分離各雜質,第二腔室空間35更包含一蒸發盤蓋36,係連接第一蒸發盤32上,蒸發盤蓋36更包含一開孔361,藉由開孔361使第一腔室空間21與第二腔室空間35彼此連通,透過加熱裝置31緩慢提高溫度,用以使蒸氣壓大的金屬元素優先揮發冷凝於冷凝罩3上,蒸氣壓小的金屬元素殘留於第一蒸發盤32上,且藉由蒸發盤蓋36可以降低物料的揮發面積,以達到更好的分離效果。For continuation, please refer to Figure 1 in conjunction with Figure 10, which is a schematic diagram of the high-
另外地,請參閱圖1配合參閱圖9,為本創作之高效能真空爐1的示意圖及法蘭311立體示意圖。在一較佳實施例中,加熱裝置31係設於一基座(未圖示)上面,加熱裝置31更進一步包含一法蘭311,法蘭311銜接基座與加熱裝置31,用以固定加熱裝置31於基座上,且法蘭311和基座上設置有複數個孔洞,且該等孔洞彼此相對,藉由法蘭311俾使第一腔室空間23與第二腔室空間35產生出空間區隔,使第一腔室空間23與第二腔室空間35彼此氣道流通、壓力可以快速調整一致。Additionally, please refer to FIG. 1 in conjunction with FIG. 9, which is a schematic diagram of the high-
請繼續參閱圖1,冷凝罩3一側裝設有複數個集料管41,當所欲處理的物料內所含的金屬彼此之間露點相差甚遠時,透過增設第二蒸發盤33,延長物料從第一蒸發盤32流至集料盤的距離,用以增加物料蒸餾分離的時間,據此,加熱裝置31能緩慢增加其溫度,擴大本體2內部溫度區間,藉此,能將物料中露點較低的雜質先分離出來,而露點較低的雜質會揮發於冷凝罩3上,並沿著冷凝罩3上的壁面緩慢流至集料管41內,且由於集料管41為傾斜設置,因此,能更集中收集雜質,且該等集料管41還另連接一導管(未圖示),用以將該等雜質透過導管收集至容器內呈裝。另外,集料管41上設置有一封蓋(未圖示)及一電磁閥,藉由電磁閥控制集料管41上封蓋的開關,其中,電磁閥可為直動式電磁閥、分布直動式電磁閥、先導式電磁閥或其他類似裝置。隨著加熱裝置31升高溫度,達到欲蒐集的金屬的露點溫度時,將集料管41上的封蓋關閉,避免金屬流至集料管41內。Please continue to refer to Figure 1. A plurality of collecting
本創作將就下面的實施例來做進一步說明,但應瞭解的是,該等實施例僅是供例示說明用,而不應被解釋為本創作的實施上的限制。This creation will further illustrate the following embodiments, but it should be understood that these embodiments are only for illustrative purposes and should not be interpreted as limitations on the implementation of this creation.
>實施例一>>Example One>
請參閱圖1及圖2,首先,操作人員將固態的錫鉛合金倒入至熔化裝置8內,優選的,係倒入8至12噸的錫鉛合金,且錫鉛合金為錫含量佔3%至95%、銻佔20%至25%、銅佔0.01%至0.1%、鐵佔0.01%至0.1%、鎳佔0.01%至0.1%、砷佔0.01%至0.1%、及鉛佔50%至75%的合金,更值的一提的是,對於任何進合倒入熔化裝置8內的物料,需滿足:鉛金屬÷銻金屬≧2;錫含量÷銅雜質含料≧50;錫含量÷雜質(鐵、鎳)含量之和≧1000。透過熔化裝置8將固態的錫鉛合金液化,液化的錫鉛合金經給料機構81流至進料容器42內,藉由抽氣裝置22將第一腔室空間21內的空氣抽走,使本體2內部第一腔室空間21形成一真空狀態,用以加快錫鉛合金自進料容器42流入至第一蒸發盤32的速度。Please refer to Figure 1 and Figure 2. First, the operator pours the solid tin-lead alloy into the
當第一蒸發盤32上的錫鉛合金液體盛滿後,錫鉛合金會沿著第一蒸發盤32盤緣流到第二蒸發盤33中,且透過第二蒸發盤33中的透孔331流至第三蒸發盤34中,如此一來,錫鉛合金液體從加熱裝置31頂層由下逐盤流至底層的過程中,藉由加熱裝置31逐漸加溫的過程中,進行物料中各金屬的分離,由於砷等雜質和錫金屬與鉛金屬之間的飽和蒸汽壓相差甚遠,藉由在冷凝罩3上增設集料管41,而露點較低的雜質會揮發於冷凝罩3上,並沿著冷凝罩3上的壁面緩慢流至集料管41內,用以分離出露點較低的雜質,隨著加熱裝置31升高溫度,達到鉛金屬的露點時,藉由電磁閥將集料管41上封蓋的關閉,避免鉛金屬揮發冷凝於冷凝罩3上時留至集料管41內,而是讓鉛金屬沿著冷凝罩3牆體流至第一集料盤5內,透過第一出料管51排出,然後,露點較高的錫金屬會保持液相並留在蒸發盤上並流至下方第二集料盤6上,並透過第二出料管61排出,從而實現錫鉛分離,以提煉出純錫金屬及純鉛金屬,其中,錫含量佔純錫金屬≧99.3%、銻金屬佔純錫金屬≦0.2%、鉛金屬佔純錫金屬≦0.5%;鉛含量佔純鉛金屬≧99.7%、雜質含量佔純鉛金屬≦0.3%;第一腔室空間21與第二腔室空間35內溫度範圍控制在攝氏200度至攝氏500度之間,較佳地,第一腔室空間21與第二腔室空間35內溫度範圍控制在攝氏300度至攝氏500度之間,最佳,第一腔室空間21與第二腔室空間35內溫度係為攝氏400度;第二蒸發盤33的數量為5至1個,較佳為3至1個,最佳為2個。When the tin-lead alloy liquid on the
更值得一提的是,為因應所欲處理得物料金屬含量不同,本創作之分離結晶裝置1還有第二實施態樣,其係延續第一實施例,其重複之處在此就不再加以贅述,What’s more worth mentioning is that in response to the different metal content of the materials to be processed, the separation and
>實施例二>>Example 2>
操作人員在執行本新型之高效能真空爐1操作作業前,可先將錫鉛合金液化倒入一低溫真空爐,其中,錫鉛合金為錫含量佔60%至70%及鉛含量佔30%至35%的合金,同樣的利用真空蒸餾技術分離錫鉛合金,透過廢金屬在不同溫度條件下的飽和蒸汽壓的差異進行真空分離,使錫鉛合金可以達到深度脫鉛的效果,此時,取得一錫鉛合金,其錫含量佔純錫金屬91%、鉛含量佔純錫金屬8%至9%,之後,操作人員將含有91%的純錫金屬倒入至熔化裝置8內。The operator can liquefy the tin-lead alloy into a low-temperature vacuum furnace before performing the operation of the high-
當第一蒸發盤32上的錫鉛合金液體盛滿後,錫鉛合金會沿著第一蒸發盤32盤緣流到第二蒸發盤33中,且透過第二蒸發盤33中的透孔331流至第三蒸發盤34中,如此一來,錫鉛合金液體從加熱裝置31頂層由下逐盤流至底層的過程中,藉由加熱裝置31逐漸加溫的過程中,進行錫鉛分離,飽和蒸氣壓大的錫金屬會揮發並冷凝於冷凝罩3上並沿著冷凝罩3牆體流至第一集料盤5內,透過第一出料管51排出,飽和蒸氣壓小雜質金屬(如: 銅金屬、鐵金屬、或鎳金屬)會保持液相並留在蒸發盤上流至下方第二集料盤6上,並透過第二出料管61排出,從而實現精錫提煉,其中,錫含量佔純錫金屬99.99%、雜質佔純錫金屬0.01%;第一腔室空間21與第二腔室空間35內溫度範圍係介於攝氏900度至攝氏1100度之間,較佳第一腔室空間21與第二腔室空間35內溫度係調控至攝氏1000度;第二蒸發盤33的數量為5至1個,較佳為3至1個,最佳為2個。When the tin-lead alloy liquid on the
綜上所述,本創作之高效能真空爐1優點如下:In summary, the advantages of the high-
1. 電性連接一監控裝置23,便於操作人員監控爐內反應情況。1. A
2.電性連接一溫度偵測裝置,藉由溫度偵測裝置得知目前第二腔室空間35內的溫度,進而與發電模組連動,進行溫控動作。2. It is electrically connected to a temperature detection device, and the current temperature in the
3. 藉由蒸發盤蓋36可以降低物料的揮發面積,以達到更好的分離效果。3. The evaporation pan cover 36 can reduce the evaporation area of the material to achieve a better separation effect.
4.藉由法蘭311使第一腔室空間21與第二腔室空間35彼此氣道流通、壓力可以快速調整一致,且加熱裝置31能固設於基座上。4. The
5.透過集料管41,將物料中露點較低的雜質先分離出來。5. Through the collecting
惟以上所述者,僅為本新型之較佳實施例而已,當不能以此限定本新型實施之範圍,即大凡依本新型申請專利範圍及新型說明內容所作之簡單等效變化與修飾,皆仍屬本新型專利涵蓋之範圍內。However, the above-mentioned are only the preferred embodiments of the present model, and should not be used to limit the scope of implementation of the present model, that is to say, all simple equivalent changes and modifications made in accordance with the scope of the patent application of the present model and the description of the model are all It still falls within the scope of this new patent.
1:高效能真空爐1: High-efficiency vacuum furnace
2:本體2: body
3:冷凝罩3: Condensation hood
4:進料裝置4: Feeding device
5:第一集料盤5: The first collecting tray
6:第二集料盤6: The second collecting tray
7:間隔島7: Space island
8:熔化裝置8: melting device
9:發電設備9: Power generation equipment
21:第一腔室空間21: The first chamber space
22:抽氣裝置22: Exhaust device
23:監控裝置23: Monitoring device
31:加熱裝置31: heating device
32:第一蒸發盤32: The first evaporation tray
33:第二蒸發盤33: The second evaporation tray
34:第三蒸發盤34: The third evaporation tray
35:第二腔室空間35: second chamber space
36:蒸發盤蓋36: Evaporation pan cover
37:穿孔37: Piercing
41:進料管41: feed pipe
42:進料容器42: feed container
51:第一出料管51: The first discharge tube
61:第二出料管61: The second discharge pipe
81:給料機構81: Feeding organization
231:握持部231: Grip
311:法蘭311: Flange
312:集料管312: Collecting pipe
331:透孔331: Through Hole
361:開孔361: hole
圖1係顯示本創作之高效能真空爐的示意圖;Figure 1 is a schematic diagram showing the high-efficiency vacuum furnace of this creation;
圖2係顯示本創作之高效能真空爐的另一示意圖;Figure 2 is another schematic diagram showing the high-efficiency vacuum furnace of this creation;
圖3係顯示本創作之第一蒸發盤立體示意圖;Figure 3 is a three-dimensional schematic diagram showing the first evaporation tray of this creation;
圖4係顯示本創作之第二蒸發盤立體示意圖;Figure 4 is a three-dimensional schematic diagram showing the second evaporation tray of this creation;
圖5係顯示本創作之第三蒸發盤立體示意圖;Figure 5 is a three-dimensional schematic diagram showing the third evaporation tray of this creation;
圖6係顯示本創作之第一集料盤立體示意圖;Figure 6 is a three-dimensional schematic diagram showing the first collecting tray of this creation;
圖7係顯示本創作之第二集料盤立體示意圖;Figure 7 is a three-dimensional schematic diagram showing the second collecting tray of this creation;
圖8係顯示本創作之加熱裝置立體示意圖;Figure 8 is a three-dimensional schematic diagram showing the heating device of this creation;
圖9係顯示本創作之法蘭立體示意圖;Figure 9 is a three-dimensional schematic diagram showing the flange of this creation;
圖10係顯示本創作之冷凝罩側面示意圖。Figure 10 shows the side view of the condensing cover of this creation.
1:高效能真空爐 1: High-efficiency vacuum furnace
2:本體 2: body
3:冷凝罩 3: Condensation hood
4:進料裝置 4: Feeding device
5:第一集料盤 5: The first collecting tray
6:第二集料盤 6: The second collecting tray
8:熔化裝置 8: melting device
21:第一腔室空間 21: The first chamber space
22:抽氣裝置 22: Exhaust device
31:加熱裝置 31: heating device
32:第一蒸發盤 32: The first evaporation tray
33:第二蒸發盤 33: The second evaporation tray
34:第三蒸發盤 34: The third evaporation tray
35:第二腔室空間 35: second chamber space
41:進料管 41: feed pipe
42:進料容器 42: feed container
51:第一出料管 51: The first discharge tube
61:第二出料管 61: The second discharge pipe
81:給料機構 81: Feeding organization
311:法蘭 311: Flange
312:集料管 312: Collecting pipe
Claims (10)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| TW109207467U TWM605507U (en) | 2020-06-14 | 2020-06-14 | High performance vacuum furnace |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| TW109207467U TWM605507U (en) | 2020-06-14 | 2020-06-14 | High performance vacuum furnace |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| TWM605507U true TWM605507U (en) | 2020-12-21 |
Family
ID=74671345
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| TW109207467U TWM605507U (en) | 2020-06-14 | 2020-06-14 | High performance vacuum furnace |
Country Status (1)
| Country | Link |
|---|---|
| TW (1) | TWM605507U (en) |
-
2020
- 2020-06-14 TW TW109207467U patent/TWM605507U/en unknown
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| US5582630A (en) | Ultra high purity magnesium vacuum distillation purification method | |
| CN105969997B (en) | Higher boiling alloy discontinuous vacuum distilled furnace for separating | |
| US20190284658A1 (en) | Device for fractional condensation of arsenic lead vapor mixture and application method thereof | |
| EP2770068B1 (en) | Vacuum refining furnace for nonferrous metal multicomponent alloys | |
| CN109055769B (en) | Multi-element alloy fractional distillation equipment | |
| CN111593211B (en) | A kind of high-purity indium purification method | |
| CN106756094B (en) | Zinc distillation furnace | |
| CN101565781A (en) | Method and device for producing high-purity antimony | |
| CN102706144A (en) | Fractional condensation vacuum furnace | |
| CN112195351A (en) | Method for producing high-purity magnesium from industrial magnesium ingot | |
| CN204434697U (en) | A kind of vacuum distillation furnace processing non-ferrous metal alloy slag charge | |
| TWM605507U (en) | High performance vacuum furnace | |
| CN205528963U (en) | Precious metals containing lead vacuum distillation stove | |
| CN102181655A (en) | Multistage distillation crucible made of tantalum material and distillation process | |
| CN211999859U (en) | A kind of distillation device for high-purity zinc production | |
| TWM600755U (en) | Low temperature vacuum furnace | |
| US11427885B2 (en) | Apparatus and process for separating and recovering the components of an alloy, particularly a noble alloy | |
| CN117987650A (en) | Condensing device and method for separating and recycling tin and antimony from tin-lead-antimony alloy | |
| US2430389A (en) | Apparatus for the condensation of metallic vapors | |
| CN107737895A (en) | A kind of oxygen-free copper bar preparation method | |
| CN111235398A (en) | Distillation plant is used in high-purity zinc production | |
| CN109207741B (en) | Refining method and device for metallic aluminum | |
| US3778044A (en) | Method and apparatus for recovery and refining of zinc | |
| CN103146933A (en) | Method for separating and recycling zinc from secondary zinc resource by using distilling-condensing device | |
| Zhang et al. | Sustainable and green removal of arsenic from crude tin via vacuum gasification–directional condensation |