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TWI349001B - Method of producing unsaturated acid from olefin - Google Patents

Method of producing unsaturated acid from olefin

Info

Publication number
TWI349001B
TWI349001B TW095108984A TW95108984A TWI349001B TW I349001 B TWI349001 B TW I349001B TW 095108984 A TW095108984 A TW 095108984A TW 95108984 A TW95108984 A TW 95108984A TW I349001 B TWI349001 B TW I349001B
Authority
TW
Taiwan
Prior art keywords
olefin
unsaturated acid
producing unsaturated
producing
acid
Prior art date
Application number
TW095108984A
Other languages
English (en)
Other versions
TW200700374A (en
Inventor
Boo Gon Woo
Jun Seok Ko
Kyoung Su Ha
Seong Pil Kang
Seok Hwan Choi
Young Bae Kim
Original Assignee
Lg Chemical Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Lg Chemical Ltd filed Critical Lg Chemical Ltd
Publication of TW200700374A publication Critical patent/TW200700374A/zh
Application granted granted Critical
Publication of TWI349001B publication Critical patent/TWI349001B/zh

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B09—DISPOSAL OF SOLID WASTE; RECLAMATION OF CONTAMINATED SOIL
    • B09B—DISPOSAL OF SOLID WASTE NOT OTHERWISE PROVIDED FOR
    • B09B3/00—Destroying solid waste or transforming solid waste into something useful or harmless
    • B09B3/40—Destroying solid waste or transforming solid waste into something useful or harmless involving thermal treatment, e.g. evaporation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/114—Helically shaped stirrers, i.e. stirrers comprising a helically shaped band or helically shaped band sections
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
    • B01F27/05—Stirrers
    • B01F27/11—Stirrers characterised by the configuration of the stirrers
    • B01F27/17—Stirrers with additional elements mounted on the stirrer, for purposes other than mixing
    • B01F27/172—Stirrers with additional elements mounted on the stirrer, for purposes other than mixing for cutting, e.g. with knives
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/04—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds
    • B01J8/0446—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical
    • B01J8/0449—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds
    • B01J8/0453—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds the fluid passing successively through two or more beds the flow within the beds being predominantly vertical in two or more cylindrical beds the beds being superimposed one above the other
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/215—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of saturated hydrocarbyl groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02—Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B01J2208/023—Details
    • B01J2208/024—Particulate material
    • B01J2208/025—Two or more types of catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/06—Details of tube reactors containing solid particles
    • B01J2208/065—Heating or cooling the reactor

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
TW095108984A 2005-03-18 2006-03-16 Method of producing unsaturated acid from olefin TWI349001B (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
KR20050022723 2005-03-18

Publications (2)

Publication Number Publication Date
TW200700374A TW200700374A (en) 2007-01-01
TWI349001B true TWI349001B (en) 2011-09-21

Family

ID=36991930

Family Applications (1)

Application Number Title Priority Date Filing Date
TW095108984A TWI349001B (en) 2005-03-18 2006-03-16 Method of producing unsaturated acid from olefin

Country Status (7)

Country Link
US (2) US7816559B2 (zh)
EP (1) EP1858833B1 (zh)
JP (1) JP4659881B2 (zh)
KR (1) KR100677051B1 (zh)
CN (1) CN101142163B (zh)
TW (1) TWI349001B (zh)
WO (1) WO2006098601A1 (zh)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
BRPI0906766A2 (pt) * 2008-01-17 2015-07-14 Lg Chemical Ltd Sistema do catalisador, reator de oxidação contendo o mesmo, e método de preparação para acroleíne e ácido acrílico empregando o mesmo
US9149781B2 (en) 2009-12-28 2015-10-06 Shell Oil Company Reactor with gas distribution system in bottom
CN102160981B (zh) * 2010-02-24 2015-01-07 杭州林达化工技术工程有限公司 一种催化反应设备
GB201506572D0 (en) 2015-04-17 2015-06-03 Johnson Matthey Davy Technologies Ltd Process
WO2017144584A1 (en) 2016-02-26 2017-08-31 Shell Internationale Research Maatschappij B.V. Alkane oxidative dehydrogenation (odh)
EP3360611B1 (en) 2017-02-10 2021-04-28 Technobell D.O.O. Koper Improved double zone tubular reactor and method for carrying out maleic anhydride production by n-butane oxidation
EP3892367A1 (en) * 2020-04-09 2021-10-13 Röhm GmbH A tube bundle reactor and method for the production of methacrylic acid through the partial oxidation of methacrolein

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3147084A (en) 1962-03-08 1964-09-01 Shell Oil Co Tubular catalytic reactor with cooler
DE2056614C3 (de) 1970-11-18 1981-04-16 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von Acrylsäure aus Propylen
BE793928A (fr) 1972-01-13 1973-05-02 Deggendorfer Werft Eisenbau Appareil pour la mise en oeuvre de processus chimiques exothermiques et endothermiques
US3907859A (en) * 1972-10-25 1975-09-23 Standard Oil Co Ohio Coproduction of acrylonitrile and acrylic acid
US3919257A (en) * 1973-02-09 1975-11-11 Standard Oil Co Ohio Catalytic vapor phase oxidation of n-butene to maleic anhydride using two different catalysts maintained in two distinct and separate portions of the reaction zone
AU529228B2 (en) 1977-07-13 1983-06-02 Nippon Shokubai Kagaku Kogyo Co. Ltd. Catalytic vapour phase oxidation
JPS55113730A (en) * 1979-02-26 1980-09-02 Mitsubishi Petrochem Co Ltd Preparation of acrolein and acrylic acid
EP0383224B1 (en) * 1989-02-17 1992-09-16 Jgc Corporation Shell-and-tube apparatus having an intermediate tube plate
JPH0783830B2 (ja) 1989-02-17 1995-09-13 日揮株式会社 中間管板を有する多管式装置
JP3287066B2 (ja) * 1993-06-28 2002-05-27 住友化学工業株式会社 アクリル酸の製造方法
KR100204729B1 (ko) 1997-03-17 1999-06-15 성재갑 아크롤레인 부분산화용 촉매의 제조 방법
KR100204728B1 (ko) 1997-03-17 1999-06-15 성재갑 아크롤레인 산화용 촉매의 제조 방법
KR100349602B1 (ko) 1997-08-30 2002-11-18 주식회사 엘지화학 아크롤레인 및 메타크롤레인 제조 촉매의 제법
JP3948798B2 (ja) * 1997-10-27 2007-07-25 株式会社日本触媒 アクリル酸の製造方法
JP4045693B2 (ja) * 1999-04-27 2008-02-13 住友化学株式会社 メタクリル酸の製造方法
JP3943284B2 (ja) * 1999-05-27 2007-07-11 株式会社日本触媒 アクリル酸の製造方法
JP4318367B2 (ja) 2000-02-16 2009-08-19 株式会社日本触媒 アクロレインおよびアクリル酸の製造方法
JP3943311B2 (ja) 2000-05-19 2007-07-11 株式会社日本触媒 不飽和アルデヒドおよび不飽和カルボン酸の製造方法
JP4426069B2 (ja) 2000-06-12 2010-03-03 株式会社日本触媒 アクリル酸の製造方法
CN1572772A (zh) * 2001-12-27 2005-02-02 三菱化学株式会社 （甲基）丙烯醛或（甲基）丙烯酸的制造方法
CN1277790C (zh) * 2002-01-11 2006-10-04 三菱化学株式会社 多管反应器,使用多管反应器的气相催化氧化法,和应用于多管反应器的启动方法
US7045657B2 (en) 2002-04-03 2006-05-16 Nippon Shokubai Co., Ltd. Catalytic gas phase oxidation process
KR100450234B1 (ko) 2002-07-10 2004-09-24 주식회사 엘지화학 개선된 열교환 시스템을 갖는 촉매 산화 반응기
DE10323461A1 (de) * 2003-05-23 2004-12-09 Basf Ag Herstellung von Aldehyden, Carbonsäuren und/oder Carbonsäureanhydriden mittels Vanadiumoxid, Titandioxid und Antimonoxid enthaltender Katalysatoren
JP4888876B2 (ja) 2003-06-13 2012-02-29 田平 武 アルツハイマー病の治療のための組換えアデノ随伴ウィルスベクター
TWI302147B (en) * 2003-09-01 2008-10-21 Lg Chemical Ltd Method of producing unsaturated aldehyde and unsaturated acid in fixed-bed catalytic partial oxidation reactor with enhanced heat control system

Also Published As

Publication number Publication date
JP4659881B2 (ja) 2011-03-30
EP1858833B1 (en) 2013-12-18
CN101142163A (zh) 2008-03-12
WO2006098601A1 (en) 2006-09-21
EP1858833A1 (en) 2007-11-28
US8142742B2 (en) 2012-03-27
JP2008535802A (ja) 2008-09-04
US20060211884A1 (en) 2006-09-21
CN101142163B (zh) 2011-01-26
TW200700374A (en) 2007-01-01
KR20060101323A (ko) 2006-09-22
EP1858833A4 (en) 2010-07-07
US20110008218A1 (en) 2011-01-13
KR100677051B1 (ko) 2007-02-01
US7816559B2 (en) 2010-10-19

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Legal Events

Date Code Title Description
MM4A Annulment or lapse of patent due to non-payment of fees