TW201521781A - Seaweed polysaccharides mask and manufacturing method thereof - Google Patents
Seaweed polysaccharides mask and manufacturing method thereof Download PDFInfo
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- TW201521781A TW201521781A TW103145918A TW103145918A TW201521781A TW 201521781 A TW201521781 A TW 201521781A TW 103145918 A TW103145918 A TW 103145918A TW 103145918 A TW103145918 A TW 103145918A TW 201521781 A TW201521781 A TW 201521781A
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- 150000004676 glycans Chemical class 0.000 title claims abstract description 33
- 229920001282 polysaccharide Polymers 0.000 title claims abstract description 33
- 239000005017 polysaccharide Substances 0.000 title claims abstract description 33
- 241001474374 Blennius Species 0.000 title claims abstract description 30
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- CDQSJQSWAWPGKG-UHFFFAOYSA-N butane-1,1-diol Chemical compound CCCC(O)O CDQSJQSWAWPGKG-UHFFFAOYSA-N 0.000 claims abstract description 22
- OKHHGHGGPDJQHR-YMOPUZKJSA-L calcium;(2s,3s,4s,5s,6r)-6-[(2r,3s,4r,5s,6r)-2-carboxy-6-[(2r,3s,4r,5s,6r)-2-carboxylato-4,5,6-trihydroxyoxan-3-yl]oxy-4,5-dihydroxyoxan-3-yl]oxy-3,4,5-trihydroxyoxane-2-carboxylate Chemical compound [Ca+2].O[C@@H]1[C@H](O)[C@H](O)O[C@@H](C([O-])=O)[C@H]1O[C@H]1[C@@H](O)[C@@H](O)[C@H](O[C@H]2[C@H]([C@@H](O)[C@H](O)[C@H](O2)C([O-])=O)O)[C@H](C(O)=O)O1 OKHHGHGGPDJQHR-YMOPUZKJSA-L 0.000 claims abstract description 20
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 claims abstract description 19
- 235000010410 calcium alginate Nutrition 0.000 claims abstract description 19
- 239000000648 calcium alginate Substances 0.000 claims abstract description 19
- 229960002681 calcium alginate Drugs 0.000 claims abstract description 19
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 18
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 claims abstract description 18
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 18
- 239000000661 sodium alginate Substances 0.000 claims abstract description 18
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 18
- 241000195493 Cryptophyta Species 0.000 claims abstract description 17
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 claims abstract description 16
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims abstract description 12
- 239000011734 sodium Substances 0.000 claims abstract description 12
- 229910052708 sodium Inorganic materials 0.000 claims abstract description 12
- 239000011265 semifinished product Substances 0.000 claims description 16
- 238000001125 extrusion Methods 0.000 claims description 13
- 239000002994 raw material Substances 0.000 claims description 11
- 229940033631 carrageenan sodium Drugs 0.000 claims description 10
- 238000002156 mixing Methods 0.000 claims description 9
- 238000000034 method Methods 0.000 claims description 8
- 241000037488 Coccoloba pubescens Species 0.000 claims description 7
- 238000003825 pressing Methods 0.000 claims description 4
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 claims description 3
- 239000008367 deionised water Substances 0.000 claims description 3
- 229910021641 deionized water Inorganic materials 0.000 claims description 3
- 239000003755 preservative agent Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 2
- 230000002335 preservative effect Effects 0.000 claims description 2
- 235000010418 carrageenan Nutrition 0.000 abstract description 12
- 239000000679 carrageenan Substances 0.000 abstract description 12
- 229940113118 carrageenan Drugs 0.000 abstract description 12
- 229920001525 carrageenan Polymers 0.000 abstract description 12
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 abstract description 12
- 229960002160 maltose Drugs 0.000 abstract description 9
- 239000003607 modifier Substances 0.000 abstract description 6
- 230000000694 effects Effects 0.000 abstract description 5
- 241001148683 Zostera marina Species 0.000 abstract description 3
- 239000004615 ingredient Substances 0.000 abstract description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 abstract 1
- 239000011575 calcium Substances 0.000 abstract 1
- 229910052791 calcium Inorganic materials 0.000 abstract 1
- 239000000499 gel Substances 0.000 description 7
- 238000010438 heat treatment Methods 0.000 description 6
- 239000002904 solvent Substances 0.000 description 5
- 230000001914 calming effect Effects 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 description 4
- FHVDTGUDJYJELY-UHFFFAOYSA-N 6-{[2-carboxy-4,5-dihydroxy-6-(phosphanyloxy)oxan-3-yl]oxy}-4,5-dihydroxy-3-phosphanyloxane-2-carboxylic acid Chemical compound O1C(C(O)=O)C(P)C(O)C(O)C1OC1C(C(O)=O)OC(OP)C(O)C1O FHVDTGUDJYJELY-UHFFFAOYSA-N 0.000 description 3
- 229940072056 alginate Drugs 0.000 description 3
- 235000010443 alginic acid Nutrition 0.000 description 3
- 229920000615 alginic acid Polymers 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 239000004744 fabric Substances 0.000 description 3
- 235000015110 jellies Nutrition 0.000 description 3
- 239000008274 jelly Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- BDOYKFSQFYNPKF-UHFFFAOYSA-N 2-[2-[bis(carboxymethyl)amino]ethyl-(carboxymethyl)amino]acetic acid;sodium Chemical compound [Na].[Na].OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O BDOYKFSQFYNPKF-UHFFFAOYSA-N 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 230000003796 beauty Effects 0.000 description 2
- -1 eucalyptus extract Chemical compound 0.000 description 2
- 229940007062 eucalyptus extract Drugs 0.000 description 2
- 235000010270 methyl p-hydroxybenzoate Nutrition 0.000 description 2
- 239000004292 methyl p-hydroxybenzoate Substances 0.000 description 2
- 229960002216 methylparaben Drugs 0.000 description 2
- 235000015424 sodium Nutrition 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 description 1
- 244000166124 Eucalyptus globulus Species 0.000 description 1
- 206010067482 No adverse event Diseases 0.000 description 1
- 206010040880 Skin irritation Diseases 0.000 description 1
- 206010052428 Wound Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 230000003110 anti-inflammatory effect Effects 0.000 description 1
- 230000002421 anti-septic effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 description 1
- 230000001815 facial effect Effects 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 230000009969 flowable effect Effects 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 239000008233 hard water Substances 0.000 description 1
- 239000006210 lotion Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- RECVMTHOQWMYFX-UHFFFAOYSA-N oxygen(1+) dihydride Chemical compound [OH2+] RECVMTHOQWMYFX-UHFFFAOYSA-N 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000002861 polymer material Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 210000002966 serum Anatomy 0.000 description 1
- 230000036556 skin irritation Effects 0.000 description 1
- 231100000475 skin irritation Toxicity 0.000 description 1
- 229940083542 sodium Drugs 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
- 235000011152 sodium sulphate Nutrition 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Cosmetics (AREA)
- Medicinal Preparation (AREA)
Abstract
Description
本發明是有關於一種面膜及其製法,特別是指一種包含有海藻多醣體之面膜,以及該面膜的製法。 The invention relates to a mask and a preparation method thereof, in particular to a mask comprising a seaweed polysaccharide body, and a method for preparing the mask.
傳統面膜包含一層以棉花或化學纖維等材料所製得的布層,以及塗布在該布層中的美容液或精華液。此種傳統面膜的缺點是該布層難以和肌膚貼合,故使用時存有相當多位於肌膚與該布層間的空隙,因此,肌膚吸收美容液或精華液的效果較差。為了改善此一問題,市面上有所謂的果凍面膜或膠體面膜。此類型面膜較傳統面膜柔軟,並具有較佳的服貼性。然而不論是傳統面膜、果凍面膜或膠體面膜,如果要產生例如鎮靜、舒緩等保養肌膚的功效,都需要額外添加美容液或精華液。此外,習知果凍面膜或膠體面膜,需要加入增進硬度的塑料改質劑,此塑料改質劑雖然可以使製造出來的面膜不易變形,但卻會使面膜的韌性變差,也容易因為拉扯而碎裂,並可能引起消費者皮膚過敏,不可不慎。 The conventional mask comprises a layer of cloth made of materials such as cotton or chemical fibers, and a cosmetic liquid or serum applied to the layer. The disadvantage of such a conventional mask is that the cloth layer is difficult to adhere to the skin, so that there are a considerable amount of space between the skin and the cloth layer when used, and therefore, the skin absorbs the beauty liquid or the essence liquid is inferior. In order to improve this problem, there are so-called jelly masks or gel masks on the market. This type of mask is softer than conventional masks and has better conformability. However, whether it is a traditional mask, a jelly mask or a gel mask, if you want to maintain the skin, such as calming, soothing, etc., you need to add a beauty lotion or essence. In addition, the conventional jelly mask or colloidal mask needs to be added with a plastic modifier for improving the hardness. Although the plastic modifier can make the manufactured mask not easily deformed, the toughness of the mask is deteriorated, and it is easy to pull. Fragmentation, and may cause skin irritation to consumers, not to be careless.
因此,本發明之目的,即在提供一種海藻多醣體面膜,以及用來製造所述海藻多醣體面膜的製法,該海 藻多醣體面膜可以在不需要添加改質劑的情況下,具有柔軟、韌性佳、摺疊時不易脆裂,以及鎮靜舒緩肌膚等功效。 Accordingly, it is an object of the present invention to provide a seaweed polysaccharide body mask, and a method for producing the seaweed polysaccharide body mask, the sea The algal polysaccharide body mask can be soft, tough, foldable, and soothing and soothing, without the need to add a modifier.
於是,本發明海藻多醣體面膜,包含1.1~1.8重量份的角叉菜膠鈉、0.3~0.8重量份的藻酸鈉、0.03~0.15重量份的麥芽糖、0.03~0.15重量份的大葉藻提取物、0.01~0.08重量份的藻酸鈣、8~10重量份的丁二醇,以及與前述成分合計共100重量份的水。 Therefore, the seaweed polysaccharide body mask of the present invention comprises 1.1 to 1.8 parts by weight of carrageenan sodium, 0.3 to 0.8 parts by weight of sodium alginate, 0.03 to 0.15 parts by weight of maltose, and 0.03 to 0.15 parts by weight of large leaf algae extract. 0.01 to 0.08 parts by weight of calcium alginate, 8 to 10 parts by weight of butanediol, and 100 parts by weight of water in total together with the above components.
所述的藻酸鈉(sodium alginate,CAS No.9005-38-3;57606-04-9)及藻酸鈣(calcium alginate,CAS No.9005-35-0)分別為一種藻酸鹽。所述的藻酸鹽為具有黏性的高分子材料,有形成凝膠或薄膜的功能,舉例來說可應用為傷口的敷料。 The sodium alginate (CAS No. 9005-38-3; 57606-04-9) and calcium alginate (CAS No. 9005-35-0) are each an alginate. The alginate is a viscous polymer material having a function of forming a gel or a film, for example, a dressing for wounds.
所述的角叉菜膠鈉(sodium carrageenan,CAS No.9601-82-9,606166-95-7),又可稱為鹿角菜膠鈉或卡拉膠鈉,並可協同前述的藻酸鹽,以及大葉藻提取物(zostera marina extract,及麥芽糖(malose,CAS No.69-79-4,16984-36-4)等五種可成膜的成份,形成本發明之海藻多醣體面膜的主要成分。此外,由於藻酸鈉、藻酸鈣、角叉菜膠鈉、大葉藻提取物及麥芽糖均屬於多醣體材料,施用於肌膚時,能產生鎮靜、疏緩、抗發炎的功效,且由於藻酸鈉、藻酸鈣、角叉菜膠鈉及大葉藻提取物,分別是由取自大自然的藻類加工或提取而製得,除相當天然外也相當環保,更不會對人體產生不良影響。 The sodium carrageenan (CAS No. 9601-82-9, 606166-95-7), which may also be called sodium carrageenan or carrageenan, may cooperate with the aforementioned alginate. And five film-forming components such as zostera marina extract and malose (CAS No. 69-79-4, 16984-36-4) form the main component of the seaweed polysaccharide mask of the present invention. In addition, since sodium alginate, calcium alginate, sodium carrageenan, large leaf algae extract and maltose are all polysaccharide materials, when applied to the skin, it can produce calming, relieving, anti-inflammatory effects, and Sodium sulphate, calcium alginate, sodium carrageenan and extract of eucalyptus are produced by processing or extracting algae from nature. They are quite environmentally friendly and have no adverse effects on the human body. .
本案之發明人在研發過程中發現,當前述的五種可成膜成分之各別使用量太少時,混合在一起的半成品呈現可流動的凝膠態,無法形成面膜,當前述的五種可成膜成分之各別使用量太多時,雖可形成面膜,但所形成的面膜會因溶劑含量不足,而變得太硬且韌性不足,除無法折疊外,還容易因拉扯而斷裂,在敷臉的過程中相當不便。為了使面膜成品能維持一定的形狀,且柔軟有韌性,前述的五種可成膜的成分的使用量應限定在如前所述的範圍。此外,本發明所使用的水,以去離子水為佳,因為去離子水可以避免製得的成品物性受硬水離子濃度影響,使面膜成品品質穩定。 The inventor of the present invention found in the development process that when the respective amounts of the five kinds of film-forming components mentioned above are too small, the mixed semi-finished products exhibit a flowable gel state and cannot form a mask, when the aforementioned five kinds When the amount of each of the film-forming components is too large, a mask may be formed, but the formed mask may be too hard and insufficient in toughness due to insufficient solvent content, and may be easily broken by pulling, in addition to being unfoldable. It is quite inconvenient in the process of applying the face. In order to maintain a certain shape of the finished mask, and to be soft and tough, the amount of the above-mentioned five film-forming components to be used should be limited to the range as described above. In addition, the water used in the present invention is preferably deionized water, because the deionized water can prevent the finished product property from being affected by the hard water ion concentration, so that the quality of the finished film product is stable.
本發明海藻多醣體面膜的製法包含混合原料步驟、靜置步驟,以及擠壓成形步驟。該混合原料步驟是將預定比例的角叉菜膠鈉、藻酸鈉、麥芽糖、大葉藻提取物、藻酸鈣、丁二醇以及水,混合成半成品。該靜置步驟是將半成品靜置2~3小時。該擠壓成形步驟是將半成品加溫至70~80℃,並快速攪拌後擠壓成形,再冷卻至室溫定形,即可製得前述的海藻多醣體面膜。 The method for preparing a seaweed polysaccharide body mask of the present invention comprises a mixing raw material step, a standing step, and an extrusion forming step. The mixed raw material step is to mix a predetermined ratio of sodium carrageenan, sodium alginate, maltose, eucalyptus extract, calcium alginate, butylene glycol, and water into a semi-finished product. The rest step is to leave the semi-finished product for 2 to 3 hours. The extrusion forming step is to heat the semi-finished product to 70-80 ° C, and rapidly extrude and then extrude, and then cooled to room temperature to form the aforementioned seaweed polysaccharide body mask.
在該混合原料步驟中,較佳地,是先將丁二醇加熱至75~85℃後,再與水混合,並加入角叉菜膠鈉、藻酸鈉、麥芽糖、大葉藻提取物,以及藻酸鈣。當丁二醇的加熱溫度高於85℃時,丁二醇容易過度揮發,而當丁二醇的加熱溫度低於75℃,不利各成分間的互溶。為了取得平衡,丁二醇以加熱至75~85℃為佳。此外,在本步驟中, 如果要延長產品的保存期限,還可在丁二醇中加入防腐劑,並在水中加入可增加防腐效果的乙二胺四乙酸二鈉(disodium EDTA,EDTA-2Na)。所述的防腐劑舉例來說可為對羥苯甲酸甲酯(methylparaben),以角叉菜膠鈉、藻酸鈉、麥芽糖、大葉藻提取物、藻酸鈣、丁二醇及水的總重為100重量份當基準,使用量為0.15重量份,且可省略不添加。乙二胺四乙酸二鈉,以角叉菜膠鈉、藻酸鈉、麥芽糖、大葉藻提取物、藻酸鈣、丁二醇及水的總重為100重量份當基準,使用量為0.1重量份,且同樣可省略不添加。在水中加入乙二胺四乙酸二鈉時,可先取少部分的水溶解乙二胺四乙酸二鈉,再與剩餘的水混合均勻。 In the step of mixing the raw materials, preferably, the butanediol is heated to 75 to 85 ° C, and then mixed with water, and added sodium carrageenan, sodium alginate, maltose, and large leaf algae extract, and Calcium alginate. When the heating temperature of the butanediol is higher than 85 ° C, the butanediol is easily excessively volatilized, and when the heating temperature of the butanediol is lower than 75 ° C, the mutual solubility between the components is disadvantageous. In order to achieve equilibrium, the butanediol is preferably heated to 75 to 85 °C. In addition, in this step, If you want to extend the shelf life of the product, you can also add preservatives to the butanediol and add disodium EDTA (EDTA-2Na) to the water to increase the antiseptic effect. The preservative may be, for example, methylparaben, the total weight of sodium carrageenan, sodium alginate, maltose, big leaf algae extract, calcium alginate, butanediol and water. When the amount is 100 parts by weight, the amount used is 0.15 parts by weight, and may be omitted. Ethylenediaminetetraacetic acid disodium, based on 100 parts by weight of carrageenan sodium, sodium alginate, maltose, big leaf algae extract, calcium alginate, butanediol and water, the amount used is 0.1 weight Share, and the same can be omitted without adding. When disodium edetate is added to water, a small portion of water can be used to dissolve disodium edetate, and then mixed with the remaining water.
在該混合原料步驟後,由於所述的五種可成膜的成分加入水與丁二醇的溶劑中,需要時間分散在溶劑當中,並吸取足夠的水及丁二醇來改變為黏稠的狀態。當經過2~3個小時的靜置後,所述的半成品將可呈現高黏度但仍可勉強流動的水膠狀態。當靜置的時間太短,可成膜的成分無法吸收足夠的溶劑,而當靜置的時間太長,會使整個製造過程過度冗長。因此,在面膜之成膜性及時間效益的考量下,該靜置步驟的較佳靜置時間為2~3個小時。 After the mixing raw material step, since the five film-forming components are added to the solvent of water and butanediol, it takes time to disperse in the solvent, and sufficient water and butanediol are taken to change to a viscous state. . After 2 to 3 hours of standing, the semi-finished product will exhibit a high viscosity but still barely flowing water gel state. When the standing time is too short, the film-forming component cannot absorb enough solvent, and when it is left for too long, the entire manufacturing process is excessively long. Therefore, the preferred rest time of the rest step is 2 to 3 hours under consideration of the film formation property and time benefit of the mask.
在該擠壓成形步驟中,之所以要加熱並攪拌半成品,是為了確保所有原料妥善地溶解與分散,使半成品再次呈現流動性較佳的狀態,以利注入模具中擠壓成形。在攪拌時,以每分鐘750~850轉的轉速為佳。當加熱溫度低於70℃時,半成品的流動性不佳,不易灌注至模具當中 ,而當加熱溫度高於80℃時,會使溶劑過度揮發,使製得的海藻多醣體面膜過硬易脆裂。因此,該半成品的加熱溫度應以70~80℃為佳。所製得的海藻多醣體面膜,因經過擠壓冷卻定形,可使得各成分間較為緊密地結合在一起,而可維持住面膜的外形,不會再次回到水膠狀態。較佳地,在擠壓成形步驟中,擠壓時間宜控制在1.5~2.5秒,當擠壓時間太長,組成物可能沾黏在模具上,如果擠壓時間太短,無法使面膜具有良好的外觀。 In the extrusion forming step, the reason why the semi-finished product is heated and stirred is to ensure that all the raw materials are properly dissolved and dispersed, so that the semi-finished product is again in a state of better fluidity for extrusion molding into the mold. When stirring, it is preferably 750 to 850 rpm. When the heating temperature is lower than 70 ° C, the fluidity of the semi-finished product is not good, and it is not easy to be poured into the mold. When the heating temperature is higher than 80 ° C, the solvent is excessively volatilized, so that the prepared seaweed polysaccharide body mask is too hard and brittle. Therefore, the heating temperature of the semi-finished product should preferably be 70 to 80 ° C. The prepared seaweed polysaccharide body mask is shaped and cooled by extrusion, so that the components can be tightly combined to maintain the shape of the mask and will not return to the state of water gel. Preferably, in the extrusion forming step, the pressing time is preferably controlled to 1.5 to 2.5 seconds. When the pressing time is too long, the composition may stick to the mold. If the pressing time is too short, the mask may not be good. Appearance.
本發明之功效在於:利用特定比例的角叉菜膠鈉、藻酸鈉、麥芽糖、大葉藻提取物、藻酸鈣,以及丁二醇及水的配合,以及加工條件的限制,可以在不必使用改質劑的情況下,使製造的面膜具有柔軟、韌性佳、摺疊時不易脆裂,以及鎮靜舒緩肌膚等功效。 The effect of the invention is that the specific ratio of carrageenan sodium, sodium alginate, maltose, big leaf algae extract, calcium alginate, and the combination of butanediol and water, as well as the limitation of processing conditions, can be used without In the case of a modifier, the manufactured mask has the effects of being soft, tough, not brittle when folded, and calming and soothing the skin.
11‧‧‧混合原料步驟 11‧‧‧ mixed raw material steps
12‧‧‧靜置步驟 12‧‧‧Standing steps
13‧‧‧擠壓成形步驟 13‧‧‧Extrusion step
本發明之其他的特徵及功效,將於參照圖式的實施方式中清楚地呈現,其中:圖1是一個流程示意圖,說明本發明海藻多醣體面膜之製法的一個實施例。 Other features and effects of the present invention will be apparent from the following description of the drawings, wherein: Figure 1 is a flow diagram illustrating one embodiment of the method of making a seaweed polysaccharide body mask of the present invention.
參閱圖1,本發明海藻多醣體面膜之實施例1,包含1.5kg的角叉菜膠鈉、0.6kg的藻酸鈉、0.1kg的麥芽糖、0.1kg的大葉藻提取物(購自滿凌實業有限公司)、0.04kg 的藻酸鈣、9kg的丁二醇,以及88.66kg的水,並以包含一個混合原料步驟、一個靜置步驟及一個擠壓成形步驟的製法製成。 Referring to Figure 1, Example 1 of the seaweed polysaccharide facial mask of the present invention comprises 1.5 kg of sodium carrageenan, 0.6 kg of sodium alginate, 0.1 kg of maltose, and 0.1 kg of large leaf algae extract (purchased from Manling Industrial Co., Ltd.). Company), 0.04kg Calcium alginate, 9 kg of butanediol, and 88.66 kg of water were prepared in a process comprising a mixing raw material step, a standing step, and an extrusion forming step.
該混合原料步驟是先取9kg的丁二醇,加入150g的對羥苯甲酸甲酯並加熱至80℃備用,再取88.66kg的水,先取其中1kg的水加入100g的EDTA-2Na,再連同剩下的水,並與前述的丁二醇、1.5kg的角叉菜膠鈉、0.6kg的藻酸鈉、0.1公斤的麥芽糖、0.1公斤的大葉藻提取物、0.04公斤的藻酸鈣混合而成為一個半成品。 The mixing raw material step is to first take 9kg of butanediol, add 150g of methylparaben and heat to 80 ° C for use, and then take 88.66kg of water, first take 1kg of water and add 100g of EDTA-2Na, together with the remaining The water is mixed with the aforementioned butanediol, 1.5 kg of sodium carrageenan, 0.6 kg of sodium alginate, 0.1 kg of maltose, 0.1 kg of large leaf algae extract, and 0.04 kg of calcium alginate. A semi-finished product.
該靜置步驟是將該半成品靜置2.5小時。 The standing step is to leave the semi-finished product for 2.5 hours.
該擠壓成形步驟是將該半成品以每分鐘800轉的轉速攪拌,並加溫至75℃後注入模具擠壓2秒後成形。成形之後冷卻至室溫取出,即可製得海造多醣體面膜。 The extrusion molding step was carried out by stirring the semi-finished product at a rotation speed of 800 rpm and heating it to 75 ° C and then injecting it into the mold for 2 seconds to form. After forming, it is cooled to room temperature and taken out to obtain a sea-made polysaccharide mask.
實施例2~3與實施例1類似,不同的地方在於角叉菜膠鈉、藻酸鈉、麥芽糖、大葉藻提取物、藻酸鈣、丁二醇及水的用量有所不同。各成分的使用量及所製得的海藻多醣體面膜之物性記錄於表1中。 Examples 2 to 3 are similar to Example 1, except that the amounts of carrageenan sodium, sodium alginate, maltose, big leaf algae extract, calcium alginate, butanediol, and water are different. The amount of each component used and the physical properties of the prepared seaweed polysaccharide mask are shown in Table 1.
比較例1~2與實施例1類似,不同的地方在於角叉菜膠鈉、藻酸鈉、麥芽糖、大葉藻提取物、藻酸鈣、丁二醇及水的用量有所不同。各成分的使用量記錄於表1中。 Comparative Examples 1 and 2 were similar to Example 1, except that the amounts of carrageenan sodium, sodium alginate, maltose, eucalyptus extract, calcium alginate, butanediol, and water were different. The amount of each component used is reported in Table 1.
參閱實施例1~3,可以發現,當角叉菜膠鈉、 藻酸鈉、麥芽糖、大葉藻提取物及藻酸鈣的用量分別在本發明的限定範圍內時,所製得的海藻多醣體面膜,除了可維持住面膜的外形外,還因柔軟度好而可折疊,韌性佳而在拉扯時不易脆裂。參閱比較例1及2則可以發現,當可成膜的五種成分之使用量低於本發明所限定的範圍時,所製得的半成品將無法形成並維持住面膜的外觀,而呈現可流動的凝膠狀態。當可成膜的五種成分之使用量高於本發明所限定的範圍時,所製得的海藻多醣體面膜又會過硬而無法摺疊且在拉扯時容易斷裂。 Referring to Examples 1 to 3, it can be found that when carrageenan sodium, When the amounts of sodium alginate, maltose, big leaf algae extract and calcium alginate are within the limits of the present invention, respectively, the prepared seaweed polysaccharide body mask can maintain the shape of the mask and is also soft. Foldable, good toughness and not brittle when pulled. Referring to Comparative Examples 1 and 2, it can be found that when the five components which can be formed into a film are used in a range lower than the range defined by the present invention, the obtained semi-finished product cannot form and maintain the appearance of the mask, and exhibits flowability. The gel state. When the amount of the five components which can be formed into a film is higher than the range defined by the present invention, the obtained seaweed polysaccharide body mask is too hard to be folded and is easily broken when pulled.
綜上所述,本發明海藻多醣體面膜的製法,能製造出海藻多醣體面膜,而該海藻多醣體面膜因含有特定比例的角叉菜膠鈉、藻酸鈉、麥芽糖、大葉藻提取物及藻酸鈣,故即使不含改質劑仍相當柔軟且韌性佳而可摺疊並不易因拉扯脆裂,且本發明所使用的成膜成分,為取自海藻具有多醣體的材料,所以無須添加其他成分即可有鎮靜舒緩肌膚之功效,故確實能達成本發明之目的。 In summary, the method for preparing a seaweed polysaccharide body mask of the present invention can produce a seaweed polysaccharide body mask, and the seaweed polysaccharide body mask contains a specific proportion of carrageenan sodium, sodium alginate, maltose, and big leaf algae extract and Calcium alginate, even if it does not contain a modifier, it is quite soft and has good toughness and can be folded and is not easily pulled by brittle fracture. The film-forming component used in the present invention is a material obtained from seaweed having a polysaccharide, so there is no need to add Other ingredients can have the effect of calming and soothing the skin, so that the object of the present invention can be achieved.
惟以上所述者,僅為本發明之實施例而已,當不能以此限定本發明實施之範圍,即大凡依本發明申請專利範圍及專利說明書內容所作之簡單的等效變化與修飾,皆仍屬本發明專利涵蓋之範圍內。 However, the above is only the embodiment of the present invention, and the scope of the present invention is not limited thereto, that is, the simple equivalent changes and modifications made by the patent application scope and the patent specification of the present invention are still It is within the scope of the patent of the present invention.
11‧‧‧原料混合步驟 11‧‧‧Material mixing steps
12‧‧‧靜置步驟 12‧‧‧Standing steps
13‧‧‧擠壓成形步驟 13‧‧‧Extrusion step
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2020133308A1 (en) * | 2018-12-29 | 2020-07-02 | L'oreal | Kit for caring for the skin |
| CN115363993A (en) * | 2022-09-22 | 2022-11-22 | 赵卫东 | A targeted mask containing algae particles |
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| US20060104931A1 (en) * | 2004-11-12 | 2006-05-18 | Takeshi Fukutome | Cosmetic treatment article comprising substrate and gel composition |
| CN103893028A (en) * | 2012-12-25 | 2014-07-02 | 青岛海芬海洋生物科技有限公司 | Seaweed facial mask |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2020133308A1 (en) * | 2018-12-29 | 2020-07-02 | L'oreal | Kit for caring for the skin |
| CN113194921A (en) * | 2018-12-29 | 2021-07-30 | 莱雅公司 | Set for caring skin |
| CN115363993A (en) * | 2022-09-22 | 2022-11-22 | 赵卫东 | A targeted mask containing algae particles |
| CN115363993B (en) * | 2022-09-22 | 2024-06-07 | 健泽(深圳)生物科技有限公司 | A targeted facial mask containing seaweed particles |
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