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SU630225A1 - Method of purifying aqueous solution of sodium sulfate from metal ions and organic admixtures - Google Patents

Method of purifying aqueous solution of sodium sulfate from metal ions and organic admixtures

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Publication number
SU630225A1
SU630225A1 SU742045056A SU2045056A SU630225A1 SU 630225 A1 SU630225 A1 SU 630225A1 SU 742045056 A SU742045056 A SU 742045056A SU 2045056 A SU2045056 A SU 2045056A SU 630225 A1 SU630225 A1 SU 630225A1
Authority
SU
USSR - Soviet Union
Prior art keywords
aqueous solution
metal ions
sodium sulfate
purifying aqueous
organic admixtures
Prior art date
Application number
SU742045056A
Other languages
Russian (ru)
Inventor
Лем Матвеевич Рабинович
Владимир Александрович Смирнов
Сергей Сергеевич Крамаренко
Нелли Аркадьевна Нивикова
Original Assignee
Волгоградский Филиал Всесоюзного Научно-Исследовательского И Проектного Института Синтетических Жирозаменителей
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
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Application filed by Волгоградский Филиал Всесоюзного Научно-Исследовательского И Проектного Института Синтетических Жирозаменителей filed Critical Волгоградский Филиал Всесоюзного Научно-Исследовательского И Проектного Института Синтетических Жирозаменителей
Priority to SU742045056A priority Critical patent/SU630225A1/en
Application granted granted Critical
Publication of SU630225A1 publication Critical patent/SU630225A1/en

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Description

33

к о н ц бМт р а ц и   с у л ь ф а т аto about nts bmt r and c and s u lf f a t a

«атрн , г:л1 Ь"Atrn, g: l1 b

КОИцеИТ-раци  железа, г/,10,02KOITsIT-iron of iron, g /, 10.02

чонцеитрацл  марганца. г-.;0.02 Концентраци  органическихmanganese chonzeitrazl. Mr. - .0.02 Concentration of organic

сосди-нений, г/л2sundry, g / l2

Начальное значение рН5Initial pH5

подают насосем (0,5 л:ч} в лологрезател;,, где темнературу воды ноднилипот до 250 С. Вода с темнературон 250° С лроходнг через смеситс,ль, куда нодают воздух в количестве 25 лч. Врем  пребыва.ни  газожидксстiiofi смеси i автоклаве 1 ч. Жидкость :-:е 1рерЫ (В:Но вывод т из автоклава через дросселирующее устройство и теллообмеки ;. з рсзерзуар-сгустите.ть. ВОЗДУХ вывод т через дроеселирую цее устройство з атмосф еру . Далее зоду фильтруют.they are pumped (0.5 l: h} to a lolo-cutter ;, where the temperature of the water is up to 250 ° C. Water with the temperature of 250 ° C is distributed through the mixture, or where the air is supplied in the amount of 25 hl. The residence time and gas-liquid mixture i autoclave 1 hour. Liquid: -: e 1Repy (B: But withdrawn from the autoclave through a throttling device and body smear; z rzzerzuar-thicken. AIR is output through the air dowel circuit device from the atmosphere. Then the zod is filtered.

После фильтрации вода имеет следую1Ц ло характеристик}:After filtration, the water has the following characteristics:

Концепт-ради  сулы)атConcept for sula) at

и а три  , г/л158 Содержатше железа Отс тстлуегand a three, g / l 158 Contains iron Ots tstlueg

Содержание марга нца. г .:О.ООС.. Концентраци  органическихThe content of marga natz. G.: O.O.S .. Concentration of organic

соединений, г/лIcompounds g / l

Конечное значение рН6Final pH6

Концентраци  су.тьфатаConcentration of succinate

натри , г/лsodium, g / l

Концентраци  железа, г/л Концентраци  марганца, гл Конце1гпраци  органическихIron concentration, g / l Concentration of manganese, hl Concentration of organic

нри.месей, г/л З начеиие рНNom.mesey, g / l 3 Nacheee rn

иодают иасосом в иодогреватель, где темиературу воды иодним.ают до . Под воздействием температуры в ирисутстзин растворимого кислорода основна  часть лтета ,ллов пере.ходит з окислы. Воду зывОлТ, гIodine and pump into the iodine heater, where the temoturture of water is iodim. Under the influence of temperature, soluble oxygen irisststzin forms the main part of the summer, but it transfers from oxides. Cold water, g

4four

:; i нодогреватс.т  ;: ох,1:жлают епед гюдачеи ,; .|5-с:устител:,.:; i nodogrevats.t;: oh, 1: they want to eat this,; . | 5-s: tired:,.

llcc/ie фильтрации те: л С-о5работа:-На  зода ИМеет следующую характеристику:llcc / ie filtering those: l C-o5work: -On the zod IMEet the following characteristics:

К С: i це н тр ац и   с ,i ь ф а т аK C: i cce n tr a c u s i i f a t а

натри , г л5Ssodium, g l5S

Содержание же.теза, г/л0,002Content same.tez, g / l0,002

Содержа«1 е маргаи-ца. г/л0,С02 Кондентраци  опганичс::-;ихContaining "1 e margai-tsa. g / l0, C02 Concentration opganichs :: -;

соединений, гл1.7compounds, ch1.7

Значен 1е рН8Value 1e pH8

Сток;, нрошедш ;е термообработку, ис: ользуюте  дл  выделени  сульфата каТрИЯ .Stoke; not hot; e heat treated, use: Use to give off KATRIUM sulphate.

Способ осуществлен i-:a опытной установке производительностью 40 л1ч. Очищагма  зода тгр а ктичеоки не содержит ионов металлов, возраетает скорость фильтрации, у 1рощаетс  технологи  очистки зоды за счет сокращени  числа стадий.The method is implemented i-: a pilot plant with a capacity of 40 l1h. The purification system of the zodiac does not contain metal ions, the filtration rate is restored, and the cleaning technology of the zod is reduced by reducing the number of stages.

Фор М у л а и 3 о б р е т е н н  Vor M u l a and 3 o b e te n n

1.Снособ очисткп водного раствора сульф:1та натри  от ИОНОЗ метал.тов и орга ничес: нх тгримесе, включающий HciVioa.:i;3au;; O :; фНльтраиию раствора, о т л и ч а ю щ и iс   тем. что. с целью упрощени  ироцессз С)ч;;ст1 и путем 1:с: лючс; ;:;: стад;:;: -тстаиван; и , перед ф гльтрацне : ;гСт:ю1 .гюдзе а К) т I е:} м о с:) б р а б о т к е.1. The method of purification of an aqueous solution of sulfon: 1 t sodium from IONOS metal.t and organic: nx term, including HciVioa.:ii3au ;; O:; fnltraiyu solution, about tl and h a y i and i with those. what. in order to simplify the processes C) h ;; st1 and by 1: s: luchs; ;::: herd;:;: -staivan; and, in front of the footer,: gSt: S1. Gyudze and K) t I e:} m o s :) b a b o to k.

2.C:ioco6 но ::. 1. от л и ч а ю Hi и и с   1ем, что термообработку ос и;ест1;;-т::о: гпи температуре 170-250° С.2.C: ioco6 but ::. 1. from Hi and Hi and and with 1, that the heat treatment of wasps and; est1 ;; - t :: o: gpi temperature 170-250 ° C.

Источники инфор.маЦИ ;, :прин тые во п:1имание при экспертизе:Sources informatsi;;: accepted in p: 1 name for examination:

1.Масл ницкий 11. Н. Авток.ла зньге процессы в цветной металлургии. М., 1969, с. 78-85.1. Oil Nikitsky 11. N. Avtok.la znge processes in non-ferrous metallurgy. M., 1969, p. 78-85.

2.Солодовников В. В. и др. Обеззрежиза1;ие сульфатных сточ.кых в-эд ироиз:юдства СЖК. М., «ЦНП ТЭНе:ЬтеХИМ, 1970, с. 40.2. Solodovnikov, V.V., et al. Decontamina1; no sulphate wastewater sources: the waters of SLC. M., “TSNP TENe: Laborer, 1970, p. 40

SU742045056A 1974-07-17 1974-07-17 Method of purifying aqueous solution of sodium sulfate from metal ions and organic admixtures SU630225A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU742045056A SU630225A1 (en) 1974-07-17 1974-07-17 Method of purifying aqueous solution of sodium sulfate from metal ions and organic admixtures

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
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Publications (1)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012065731A1 (en) * 2010-11-16 2012-05-24 Remondis Assets & Services Gmbh & Co. Kg Method for recovering potassium sulphate from biodiesel production
CN110759570A (en) * 2019-10-31 2020-02-07 广东闻扬环境科技有限公司 Treatment method and treatment system for dye intermediate wastewater

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012065731A1 (en) * 2010-11-16 2012-05-24 Remondis Assets & Services Gmbh & Co. Kg Method for recovering potassium sulphate from biodiesel production
US8968689B2 (en) 2010-11-16 2015-03-03 Remondis Production Gmbh Method for recovering potassium sulphate from biodiesel production
CN110759570A (en) * 2019-10-31 2020-02-07 广东闻扬环境科技有限公司 Treatment method and treatment system for dye intermediate wastewater

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