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SU622869A1 - Coating for protection of aluminized articles against oxidation during heat treatment - Google Patents

Coating for protection of aluminized articles against oxidation during heat treatment

Info

Publication number
SU622869A1
SU622869A1 SU762428485A SU2428485A SU622869A1 SU 622869 A1 SU622869 A1 SU 622869A1 SU 762428485 A SU762428485 A SU 762428485A SU 2428485 A SU2428485 A SU 2428485A SU 622869 A1 SU622869 A1 SU 622869A1
Authority
SU
USSR - Soviet Union
Prior art keywords
coating
against oxidation
aluminized
protection
oxidation during
Prior art date
Application number
SU762428485A
Other languages
Russian (ru)
Inventor
Наталия Фридриховна Шур
Юрий Павлович Шкретов
Original Assignee
Предприятие П/Я Г-4696
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Предприятие П/Я Г-4696 filed Critical Предприятие П/Я Г-4696
Priority to SU762428485A priority Critical patent/SU622869A1/en
Application granted granted Critical
Publication of SU622869A1 publication Critical patent/SU622869A1/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C10/00Solid state diffusion of only metal elements or silicon into metallic material surfaces
    • C23C10/28Solid state diffusion of only metal elements or silicon into metallic material surfaces using solids, e.g. powders, pastes
    • C23C10/30Solid state diffusion of only metal elements or silicon into metallic material surfaces using solids, e.g. powders, pastes using a layer of powder or paste on the surface

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Preventing Corrosion Or Incrustation Of Metals (AREA)
  • Catalysts (AREA)
  • Anti-Oxidant Or Stabilizer Compositions (AREA)

Description

8eight

Эта цель достигаетс  тем, что предложенна  обмазка содержит в качестве наполнител  алюминий и окись алюмини , а в качестве св зующего коллоксилин , амилацетат и диэтилоксалат при следующем соотношении компонентов , вес.%:This goal is achieved by the fact that the proposed plaster contains aluminum and alumina as a filler, and colloxylin, amylacetate and diethyloxalate as a binder in the following ratio of components, wt.%:

5-105-10

1-3 40-45 15-20 Остальное1-3 40-45 15-20 Else

Пример. Дл  приготовлени  обмазки предложенного состава компоненты берут в указанном соотношении. Коллоксилин раствор ют в смеси амилацетата и диэтилоксалата) затем в по лученный раствор св зующего добавл ют наполнитель - смесь алюмини  в виде пудры и порошка окиси алюмини . В зкость обмазки должна составл ть от 20 до 25 сек по визкозиметру Example. To prepare the coating of the proposed composition, the components are taken in the specified ratio. The colloxylin is dissolved in a mixture of amyl acetate and diethyl oxalate) and then a filler — a mixture of aluminum in the form of powder and alumina powder — is added to the resulting binder solution. The viscosity of the coating should be from 20 to 25 seconds using a viscometer.

Состав предложенной The composition of the proposed

№№ обмазки, вес.% ппNumber of the coating, wt.% PP

228694228694

Приготовленную обмазку тщательно перемешивают и нанос т на поверхность металлических изделий с нанесенным слоем алюмини  пульверизатором (или окунанием); сушат на воздухе.The prepared coating is thoroughly mixed and applied to the surface of metal products with an aluminum layer applied with a spray gun (or dipping); air dried.

Издели  с нанесенной обмазкой подвергают диффузионному отжигу при температуре 700-950 С в течение 2-3 час. Несгоревшие частицы обмазки удал ют щеткой.The coated products are subjected to diffusion annealing at a temperature of 700-950 C for 2-3 hours. The unburned smear particles are removed with a brush.

Предложенна  обмазка полностью.The proposed coating completely.

10 предохран ет алитированные издели  от выгорани  алюмини  при диффузионном отжиге и обеспечивает получение изделий с хорошим товарным видом и высоким качеством поверхности ( отсутствуют дефекты в виде наплывов,10 prevents aluminized products from burning aluminum during diffusion annealing and provides products with a good presentation and high surface quality (there are no defects in the form of sagging,

оплавлени , неравномерного сцеплени  обмазки с покрытием).melting, uneven adhesion of the coating with the coating).

В-таблице приведены результаты испытаний алитированных изделий из стали 10 с нанесенной обмазкой приThe table shows the test results for alitized steel 10 products coated with a coating at

температуре 600 Сstemperature 600 Cs

Срок службы,Life time,

часhour

Окись алюмини  КоллоксилинAlumina Kolloksilin

Амилацетат ДиэтилоксалатAmilacetate Diethyloxalate

АЛЮ1иШНИЙALIUM AND LARGE

Окись алюмини Aluminum oxide

КоллоксилинKolloksilin

АмилацетатAmyl acetate

ДиэтилоксалатDiethyloxalate

АлюминийAluminum

Окись алюмини Aluminum oxide

КоллоксилинKolloksilin

АмилацетатAmyl acetate

ДиэтилоксалатDiethyloxalate

АлюминийAluminum

После указанного срока службы издели  были сн ты с йстдтаний, так как гарант рованный срок службы (10000 час) изделий был превышен боле ,е чем в 3 раза.After the specified service life, the products were removed from service, since the guaranteed service life (10,000 hours) of the products was exceeded by more than 3 times.

Claims (1)

Формула изобретени Invention Formula Обмазка защиты -алитированных изделий от окислени  при термической об31000Coating protection of a-catalyzed products against oxidation during thermal operation 31000 3100031,000 3100031,000 работке, содержаща  наполнитель и св зующее, отличающа с   тем, что, с целью улучшени  качества поверхности и увеличени  срока службы , в качестве наполнител  она содержит алюминий и окись алюмини , а в качестве св зующего - коллоксилин, амилацетат и дизтилоксалат при следующем соотнесении компонентов, вес.%| 5 Окись алюмини 5-10 Коллоксилин1-3 Амилацетат40-45 Диэтилоксалат15-20 дттичммомйл АлюминийОстальное 622869в Источники информации, прин тые во внимание при экспертизе: 1. Авторское свидетельство СССР 99463, С 23 С.,7/00, 1954. Минкевич А.Н. Химико-термичес обработка металлов и сплавов, м., МашиностроениеЧ с. 162-163.It contains filler and binder, characterized in that, in order to improve surface quality and increase service life, it contains aluminum and aluminum oxide as a filler, and colloxyline, amyl acetate and distiloxalate as a binder, wt.% | 5 Aluminum oxide 5-10 Kolloksilin1-3 Amilacetate40-45 Diethyloxalate15-20 dtichmmomyl AluminumOtherly 622869v Sources of information taken into account during the examination: 1. USSR Copyright Certificate 99463, C 23 S., 7/00, 1954. Minkevich AN . Chemical-thermal treatment of metals and alloys, m., MashinostroenieCh. 162-163.
SU762428485A 1976-12-13 1976-12-13 Coating for protection of aluminized articles against oxidation during heat treatment SU622869A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU762428485A SU622869A1 (en) 1976-12-13 1976-12-13 Coating for protection of aluminized articles against oxidation during heat treatment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU762428485A SU622869A1 (en) 1976-12-13 1976-12-13 Coating for protection of aluminized articles against oxidation during heat treatment

Publications (1)

Publication Number Publication Date
SU622869A1 true SU622869A1 (en) 1978-07-25

Family

ID=20686104

Family Applications (1)

Application Number Title Priority Date Filing Date
SU762428485A SU622869A1 (en) 1976-12-13 1976-12-13 Coating for protection of aluminized articles against oxidation during heat treatment

Country Status (1)

Country Link
SU (1) SU622869A1 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1998027245A1 (en) * 1996-12-17 1998-06-25 Yalestown Corporation N.V. Method for manufacturing parts with a reinforced working surface

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1998027245A1 (en) * 1996-12-17 1998-06-25 Yalestown Corporation N.V. Method for manufacturing parts with a reinforced working surface

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