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SU466238A1 - Trimethylgallium release method - Google Patents

Trimethylgallium release method

Info

Publication number
SU466238A1
SU466238A1 SU1904380A SU1904380A SU466238A1 SU 466238 A1 SU466238 A1 SU 466238A1 SU 1904380 A SU1904380 A SU 1904380A SU 1904380 A SU1904380 A SU 1904380A SU 466238 A1 SU466238 A1 SU 466238A1
Authority
SU
USSR - Soviet Union
Prior art keywords
trimethylgallium
release method
release
target product
etherate
Prior art date
Application number
SU1904380A
Other languages
Russian (ru)
Inventor
Борис Георгиевич Грибов
Борис Иванович Козыркин
Евгения Николаевна Зорина
Ирина Григорьевна Тоноян
Людмила Григорьевна Тоноян
Владимир Иосифович Брегадзе
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed filed Critical
Priority to SU1904380A priority Critical patent/SU466238A1/en
Application granted granted Critical
Publication of SU466238A1 publication Critical patent/SU466238A1/en

Links

Description

3 примеру 1 получают 19,6 г триметилгалли  (48% на вз тый и 95% на вступивший в реакцию диэтиловый эфират триметилгалли ). Предмет изобретени  1. Способ выделени  триметилгалли  из его эфирата путем термической обработки иоследнего с последуюшим выделением целевого продукта известными приемами, отличаю4 щ и и с   тем, что, с целью повышени  стеиени чистоты целевого продукта, термической обработке подвергают продукт взаимодействи  диэтилового эфирата триметилгалли  с более высококип шим эфиром. 2. Способ по п. 1, отличаюш;ийс  тем, что, с целью получени  триметилгалли  высокой степени чистоты, диэтиловый эфират триметилгалли  предварительно очишают.In Example 1, 19.6 g of trimethylgallium (48% for the taken and 95% for the reacted trimethylgallium diethyl ether) are obtained. The subject matter of the invention 1. The method for isolating trimethylgalli from its etherate by heat treatment and the latter followed by separation of the target product by known methods differs from that in order to increase the purity of the target product, trimethylgallium diethyl etherate shim ether. 2. The method according to claim 1, characterized by the fact that, in order to obtain high purity trimethyl gallium, trimethyl gallium diethyl ether is first purified.

SU1904380A 1973-04-04 1973-04-04 Trimethylgallium release method SU466238A1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
SU1904380A SU466238A1 (en) 1973-04-04 1973-04-04 Trimethylgallium release method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
SU1904380A SU466238A1 (en) 1973-04-04 1973-04-04 Trimethylgallium release method

Publications (1)

Publication Number Publication Date
SU466238A1 true SU466238A1 (en) 1975-04-05

Family

ID=20548566

Family Applications (1)

Application Number Title Priority Date Filing Date
SU1904380A SU466238A1 (en) 1973-04-04 1973-04-04 Trimethylgallium release method

Country Status (1)

Country Link
SU (1) SU466238A1 (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4604473A (en) * 1983-06-17 1986-08-05 The Secretary Of State For Defence In Her Britannic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland Preparation of metal alkyls
US4720561A (en) * 1984-03-26 1988-01-19 The Secretary Of State For Defence In Her Britannic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland Preparation of metal alkyls
US5288885A (en) * 1991-11-19 1994-02-22 Shell Research Limited Purification of tri-alkyl compounds of Group 3a metals

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4604473A (en) * 1983-06-17 1986-08-05 The Secretary Of State For Defence In Her Britannic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland Preparation of metal alkyls
US4720561A (en) * 1984-03-26 1988-01-19 The Secretary Of State For Defence In Her Britannic Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland Preparation of metal alkyls
USRE33292E (en) * 1984-03-26 1990-08-07 The Secretary Of State For Defence In Her Majesty's Government Of The United Kingdom Of Great Britain And Northern Ireland Preparation of metal alkyls
US5288885A (en) * 1991-11-19 1994-02-22 Shell Research Limited Purification of tri-alkyl compounds of Group 3a metals

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